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S h a m s a e i | S e ifi S t r u c t u r a l I n t e g r i t y o f A d d i t i v e M ASTM INTERNATIONAL Selected Technical Papers a n u f Structural Integrity a c t u r e of Additive d M a t e Manufactured r i a l s a Materials and Parts n d P a r t s S T ASTM INTERNATIONAL P 1 6 Helping our world work better 3 STP 1631 1 Editors: Nima Shamsaei ISBN: 978-0-8031-7708-6 Mohsen Seifi Stock #: STP1631 www.astm.org . SELECTEDTECHNICALPAPERS STP1631 Editors:NimaShamsaeiandMohsenSeifi Structural Integrity of Additive Manufactured Materials and Parts ASTM STOCK #STP1631 DOI: 10.1520/STP1631-EB ASTMInternational,100BarrHarborDrive,POBoxC700,WestConshohocken,PA19428-2959 PrintedintheU.S.A. . LibraryofCongressCataloging-in-PublicationData Names:Shamsaei,Nima,editor.|Seifi,Mohsen,editor. Title:Structuralintegrityofadditivemanufacturedmaterialsandparts/ editors,NimaShamsaei,MohsenSeifi. Description:WestConshohocken,PA,USA:ASTMInternational,[2020]| Series:Selectedtechnicalpapers;STP1631|Includesbibliographical references.|Summary:“THISCOMPILATIONOFSelectedTechnicalPapers, STP1631,StructuralIntegrityofAdditiveManufacturedMaterials& Parts,containspeer-reviewedpapersthatwerepresentedatasymposium heldOctober7–10,2019,inNationalHarbor,MD,USA.Thesymposiumwas sponsoredbyASTMInternationalAdditiveManufacturingCenterof ExcellenceandadditionalASTMTechnicalCommittees”–Providedby publisher. Identifiers:LCCN2020032340(print)|LCCN2020032341(ebook)|ISBN 9780803177086|ISBN9780803177093(pdf) Subjects:LCSH:Strengthofmaterials.|Machineparts–Testing.| Structuralanalysis(Engineering)|Additivemanufacturing. Classification:LCCTA405.S7672020 (print)|LCCTA405 (ebook)|DDC 620.1/12–dc23 LCrecordavailableathttps://lccn.loc.gov/2020032340 LCebookrecordavailableathttps://lccn.loc.gov/2020032341 ISBN:978-0-8031-7708-6 CopyrightVC 2020ASTMINTERNATIONAL,WestConshohocken,PA.Allrightsreserved.Thismaterial maynotbereproducedorcopied,inwholeorinpart,inanyprinted,mechanical,electronic,film,orother distributionandstoragemedia,withoutthewrittenconsentofthepublisher. PhotocopyRights Authorizationtophotocopyitemsforinternal,personal,oreducationalclassroomuse,ortheinternal, personal,oreducationalclassroomuseofspecificclients,isgrantedbyASTMInternationalprovidedthat theappropriatefeeispaidtotheCopyrightClearanceCenter,222RosewoodDrive,Danvers,MA01923, Tel:(978)646-2600;http://www.copyright.com/ ASTMInternational isnot responsible, asa body, for the statementsand opinions expressed in this publication.ASTMInternationaldoesnotendorseanyproductsrepresentedinthispublication. PeerReviewPolicy Eachpaperpublishedinthisvolumewasevaluatedbytwopeerreviewersandatleastoneeditor.The authorsaddressedallofthereviewers’commentstothesatisfactionofboththetechnicaleditor(s)and theASTMInternationalCommitteeonPublications. Thequalityofthepapersinthispublicationreflectsnotonlytheobviouseffortsoftheauthorsandthe technical editor(s), but also the work of the peer reviewers. In keeping with long-standing publication practices, ASTM International maintains the anonymity of the peer reviewers. The ASTM International CommitteeonPublicationsacknowledgeswithappreciationtheirdedicationandcontributionoftime andeffortonbehalfofASTMInternational. CitationofPapers When citingpapers fromthispublication,the appropriate citationincludesthe paperauthors,“paper title,”inSTPtitle,bookeditor(s)(WestConshohocken,PA:ASTMInternational,year),pagerange,paper doi,listedinthefootnoteofthepaper.Acitationisprovidedonpageoneofeachpaper. PrintedinHanover,PA . September,2020 Foreword THIS COMPILATION OF Selected Technical Papers, STP1631, Structural Integrity of Additive Manufactured Materials and Parts, contains peer-reviewed papers that were presented at a symposium held October 7–10, 2019, in National Harbor, MD, USA.The symposium was sponsoredbyASTMInternational AdditiveManufactur- ingCenterofExcellenceandadditionalASTMTechnicalCommittees. Symposium Chairs and STP Editors: Nima Shamsaei Auburn University Auburn, AL, USA Mohsen Seifi ASTM International Washington, DC, USA . iii . Contents Overview ix DemonstrationofClosed-LoopControlforLaserPowderBedFusion(LPBF) 1 DavidMaass OntheChallengestowardRealizationofFunctionallyGradedStructuresby ElectronBeamMelting—Fe-BaseShapeMemoryAlloyandStainlessSteel 20 ChristofTorrent,Andre´Bauer,MalteVollmer,andThomasNiendorf ResidualStressFormationinLaser-BasedPowderBedFusion(PBF-LB)ofInvar36 34 MostafaYakoutandMohamedA.Elbestawi OriginofOxidesandOxide-RelatedPoresinLaserPowderBedFusionParts 45 TomioOhtsuki,LonnieSmith,MingTang,andP.ChrisPistorius TowardUnderstandingtheRoleofSurfaceTextureforAdditively ManufacturedMetalParts 61 AdamJ.Brooks,ArushiDhakad,AgustinDiaz,andDanielKowalik OptimizingX-RayComputedTomographySettingsforDimensionalMetrology Using2DImageAnalysis 88 YounesChahid,AndrewTownsend,AlexanderLiu,PaulBills, PhilipSperling,andRaduRacasan ChallengesinInspectingInternalFeaturesforSLMAdditiveManufactured BuildArtifacts 102 AhmedTawfik,RaduRacasan,DesiBacheva,LiamBlunt, Andre´Beerlink,andPaulBills ACriticalDiscussionontheDiffraction-BasedExperimentalDetermination ofResidualStressinAMParts 122 TatianaMishurova,ItziarSerrano-Mun˜oz,TobiasFritsch,AlexanderUlbricht, MaximilianSprengel,AlexanderEvans,ArneKromm,MauroMadia, andGiovanniBruno . v X-RayComputedTomographyInspectioninMetalAdditiveManufacturing: TheRoleofWitnessSpecimens 139 AntonduPlessis,JessM.Waller,StephanG.leRoux,InaYadroitsava, IgorYadroitsev,JohanEls,andJacobusPrinsloo PerspectiveonNondestructiveEvaluationofAdditiveManufacturedComponents 157 EricLindgrenandBryceJolley PredictionofResidualStressEvolutionforEnd-To-EndProcessChainof LaserPowderBedFusionProcessandDeterminationofFatigueS-NCurves 165 ShukriAfazov,JamieFrame,UtkarshaAnkalkhope,PrveenBidare, YijunLiu,WilsonVesga,andBenDutton DesignofCouponsandTestMethodologyforOrthotropicCharacterization ofFFF-ProcessedUltem9085 176 TommyHyatt,RichardMartin,andRichFields IntrinsicThresholdStressIntensityofAdditiveManufacturedMetals 188 R.Sunder,RameshKoraddi,andAndreiGorunov AMultiscaleMaterialModelingApproachtoPredicttheMechanical PropertiesofPowderBedFusion(PBF)Metal 203 YangLi,HongyiXu,Wei-JenLai,ZiangLi,andXumingSu AlternateMethodforDeterminingYieldStrengthofPolymerAdditiveManufacturing 214 ChulY.Park,KeithE.Rupel,ChelseyE.Henry,KevinF.Malik, SayataGhose,andUpulR.Palliyaguru EffectsofSurfaceRoughnessandPorosityonFatigueBehaviorofAlSi10Mg ProducedbyLaserPowderBedFusionProcess 229 Wei-JenLai,ZiangLi,AvineshOjha,YangLi,JoyForsmark, CarlosEngler,andXumingSu CharacterizationofFunctionallyGradedMaterialsBasedonInconel718 andStainlessSteel316LManufacturedbyDEDProcess 247 JanDˇzugan,DanielMelzer,MartinaKoukol´ıkova´,JaroslavVavˇr´ık,andMohsenSeifi FrettingFatigueCharacterizationinPress-FitJointsofAMPartsby X-RayTomographyandDigitalImageCorrelation 257 InigoBacaicoa,SaschaHorn,AngelikaBrueckner-Foit, JuliaRichter,andThomasNiendorf EffectofMicrostructureandInternalDefectsontheMechanical PropertiesofTi6Al4VGyroidLatticeStructuresforBiomedicalImplants 271 DaliaMahmoud,MohamedA.Elbestawi,andKassimS.Al-Rubaie Full-ScaleHigh-Load,Thermal,andFatigueTestingofAdditive ManufacturedPowderBedFusionComponentforOilFieldApplications 289 MatthewWayneSanders,AdamRowe,andSureshDivi . vi DynamicCompressionResponseofPorousZirconium-BasedBulk MetallicGlass(Zr Ti Cu Ni Be )Honeycomb:ANumericalStudy 308 41 14 12.5 10 22.5 NandKishoreSingh,ShashiKantKumar,SatishK.S.N.Idury, K.K.Singh,andRatneshwarJha PreclinicalTestingofaNovel,Additive-Manufactured,Three-Dimensional PorousTitaniumStructure 322 ErikWoodard,ZachPost,andMarkMorrison InvestigationofMicrostructureandMechanicalPropertiesofSLM-Produced Inconel718andHastelloy-XAlloys 340 GuneyMertBilgin,CansinemTuzemen,CemreTigli,andYesimNurGulcan AnalysisofDataStreamsforQualificationandCertificationofInconel738LC AirfoilsProcessedthroughElectronBeamMelting 352 MichaelKirka,DerekRose,WilliamHalsey,AmirkoushyarZiabari,VincentPaquit, DanielRyan,andPaulBrackman . vii . Overview Toensurethestructuralintegrityofadditivelymanufactured(AM)parts,thereisa need for establishing feedstock-process-structure-property-performance relation- ships, specifically where these components and structures are being used in safety criticalapplications.Therefore,theFourthASTMInternationalSymposiumonthe StructuralIntegrity ofAdditive Manufactured Materials and Parts tookplace from October 7–10, 2019, in the Washington, DC, area in coordination with partners from government,industry, and academia, toprovide aforum for theexchange of ideas regarding the structural integrity of parts fabricated using additive manufacturingwithafocusonthelackofindustrystandards,designprinciples,as wellasqualificationandcertificationchallenges. The first event of this kind was sponsored by ASTM International Committee E08 asaworkshop inSanAntonioin May2016. The second event was sponsored by Committees E08 and F42 as a symposium in Atlanta in November 2017. The third event was held in Washington, DC and sponsored by Committees F42, E08, andE07inNovember2018. AfterthecreationofASTMInternationalAdditiveManufacturingCenterofEx- cellence(AMCoE)inearly2018andthegrowthoftheAMindustry,theefforthas beencentralizedandisnowbeingledandsponsoredbytheAMCoE,involvingsev- eral co-sponsoring ASTM technical committees, including: B09 on Metal Powders and Metal Powder Products; D20 onPlastics; D30 on Composite Materials; E07 on Nondestructive Testing; E08 on Fatigue and Fracture; F04 on Medical and Surgical Materials and Devices; and F42 on Additive Manufacturing Technologies. In addi- tion,thefourtheventwassupportedbytheNationalAeronauticsandSpaceAdmin- istration(NASA),NationalInstituteofStandardsandTechnology(NIST),European StructuralIntegritySociety(ESIS)TC15,andtheFoodandDrugAdministration. This event continues to receive interest from the international community and has been growing drastically, becoming the main gathering around standardization, qualification, and certification for additively manufactured materials and parts. This yearwearepleasedtoreportthatwehave133talks,including44invitedspeakers,10 posters, 25 student competition talks, 3 panel discussions, and over 300 attendees, representingindustry,academia,andgovernmentfrommorethan30countries. Thereare24selectedtechnicalpapers(STPs)inthiscollectionthatwillprovide anopportunitytodelvemoredeeplyintothewidevarietyoftopicscoveredduring the symposium. While individual papers often touch on multiple topics, the . ix

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