Advanced Micro-Device Engineering Edited by Osamu Hanaizumi Masafumi Unno Advanced Micro-Device Engineering Selected, peer reviewed papers from the 5th International Symposium on Silicon Science and the 1st International Conference on Advanced Micro-Device Engineering (ISSS & AMDE 2009), was held by the International Education and Research Center for Silicon Science and the Advanced Technology Research Center (ATEC), Gunma University on 10 and 11 December 2009 in Kiryu, Japan Edited by Osamu Hanaizumi and Masafumi Unno TRANS TECH PUBLICATIONS LTD Switzerland • UK • USA Copyright 2011 Trans Tech Publications Ltd, Switzerland All rights reserved. No part of the contents of this publication may be reproduced or transmitted in any form or by any means without the written permission of the publisher. Trans Tech Publications Ltd Laubisrutistr. 24 CH-8712 Stafa-Zurich Switzerland http://www.ttp.net Volume 459 of Key Engineering Materials ISSN 1013-9826 Full text available online at http://www.scientific.net Distributed worldwide by and in the Americas by Trans Tech Publications Ltd. Trans Tech Publications Inc. Laubisrutistr. 24 PO Box 699, May Street CH-8712 Stafa-Zurich Enfield, NH 03748 Switzerland USA Phone: +1 (603) 632-7377 Fax: +41 (44) 922 10 33 Fax: +1 (603) 632-5611 e-mail: [email protected] e-mail: [email protected] Preface A joint symposium of the 5th International Symposium on Silicon Science (ISSS 2009) and the 1st International Conference on Advanced Micro-Device Engineering (AMDE 2009) was held by the International Education and Research Center for Silicon Science and the Advanced Technology Research Center (ATEC), Gunma University on 10 and 11 December 2009 in Kiryu, Japan. The symposium was attended by 124 researchers, and the number of presentations was 80, including 23 oral presentations (7 invited and 16 regular) and 57 poster presentations. Gunma University was established more than fifty years ago from an amalgamation of several educational institutions, including Maebashi Medical College, Kiryu Technical College, Gunma Normal School, and Gunma Youth Normal School. From these institutions, the Faculty of Medicine, the Faculty of Engineering, and the Faculty of Education were formed. Since its inception, the university has striven to foster distinguished physicians, engineers and teachers. Focusing on science and technology, the university has contributed significantly to the development of postwar Japan. The postwar industrial and economic growth of Japan has been steadily declining while neighboring countries appear ready to overtake Japan’s lead position. The effects of these changes can be seen in various social phenomena. The university must take its position at the head of our society in order to lead the way toward the construction of a new era. It is imperative that the university accomplishes its mission to stimulate new energy for a new era. In order to achieve this goal, we need the participation of students who will bear the burdens of a new age. Research in silicon science also has a long history comparable to that of the university. Many professors devoted their energies to study silicon science to develop functional materials. A research team led by Professors Matsumoto and Hiratsuka proposed an advanced research project for the establishment of silicon science, leading to the birth of G-ASiST, the Gunma association of silicon science and technology, in March 2005. This project has been adopted as Co-operative projects, called Renkei-Yuugou Jigyou, and in March 2008, we established the International Education and Research Center for Silicon Science (Silicon Center). The Advanced Technology Research Center (ATEC) was established in 1996 as the Satellite Venture Business Laboratory (SVBL). After the Japanese National Universities were incorporated in 2006, SVBL was renamed ATEC. ATEC seeks to create fundamental technologies to foster future advanced industries and to develop human resources having professional skills and venturesome minds. The main research projects at ATEC are “Applied Materials,” “Nanotechnologies,” “Applied Optics,” and “Analog Circuit Technologies”. Such projects have been advanced through close collaboration with the Silicon Center. AMDE was first organized in 2009 to promote the activity of ATEC, as a joint symposium with ISSS. This special issue collects the contributions, submitted and accepted by at least two independent referees for this issue of Key Engineering Materials. We are greatly thankful to all participants of ISSS & AMDE 2009. We also acknowledge the authors and referees for their contribution to the present proceedings. Chairs of ISSS & AMDE 2009 Osamu Hanaizumi Masafumi Unno Gunma University, Japan Organized by International Education and Research Center for Silicon Science, Gunma University Advanced Technology Research Center, Gunma University Organizing Committee ISSS AMDE Chairs: M. Unno O. Hanaizumi Vice-chairs: H. Matsumoto M. Hanaya Secretaries: K. Miura N. Sakaguchi (Gunma University) Supported by Gunma University Kiryu City New Gunma Analog College, MEXT Foundation for Science and Technology, Gunma University Chisso Corporation Shin-Etsu Chemical Co.,Ltd. Momentive Performance Materials Inc. Colcoat Co.,Ltd. Ajinomoto Fine-Techno Co.,Inc. The Institute of Electronics, Information and Communication Engineers The Illuminating Engineering Institute of Japan Editorial Committee Editor-in-Chief: O. Hanaizumi (Gunma University, Japan) Vice Editor-in-Chief: M. Unno (Gunma University, Japan) Editor: M. Ito (Gunma University, Japan) Editor: H. Sakurai (Gunma University, Japan) Editor: S. Adachi (Gunma University, Japan) Editor: S. Hosaka (Gunma University, Japan) Editor: Y. Yamakoshi (Gunma University, Japan) Editor: Y. Fujii (Gunma University, Japan) Editor: N. Takai (Gunma University, Japan) Assistant Editor: K. Miura (Gunma University, Japan) Table of Contents Preface Organizers I. Material Science Spin and Orbital Magnetic Moment of Pd Co Evaluated by X-Ray Magnetic Diffraction 3 Experiment M. Ito, Y. Oba, A. Sato, K. Suzuki, T. Tadenuma, R. Nagayasu, H. Sakurai and H. Adachi 3 Spin Density Distribution of YTiO Observed by X-Ray Magnetic Diffraction 3 K. Suzuki, M. Ito, N. Tsuji, H. Adachi, H. Nakao, Y. Murakami, Y. Taguchi, Y. Tokura, E. Nishibori and M. Sakata 7 Magnetic Compton Profile Measurement of Thin Films H. Nishino, R. Yamaki, M. Itou, Y. Sakurai, H. Sakurai and M. Ito 11 Ferromagnetic Resonance Frequency of Single-Layer Magnetic Metal Films with Lattice Distortion N. Shigeno, S. Negishi, K. Hoshi, T. Fukunaga, S. Furusawa and H. Sakurai 15 Effect of Annealing on Sub-Gap Absorption in Amorphous InGaZnO Films 4 T. Gotoh, K. Kawarai, H. Wakabayashi and K. Kaneda 19 Improvement of Crystallization Rate in Post-Annealed Ge Sb Te Films 2 2 5 K. Kawarai and T. Gotoh 23 Ionic Conductivity of Polycrystalline Li Ge Si O (x = 0.0~1.0) 2 x 1-x 3 S. Furusawa and S. Enokida 27 Structural Analysis of Rf Sputtered Er Doped Ta O Films 2 5 J.P. Bange, M.K. Singh, K. Kano, K. Miura and O. Hanaizumi 32 Preparation of CaTiO :Pr Phosphor by Using CaB O as a Flux 3 2 4 T. Kyômen, K. Hirozumi and M. Hanaya 38 II. Chemical Science and Technology Solvent-Free Synthesis of Siloxanes and their Usage as Potential Cross-Coupling Reagents M. Unno, R. Tanaka, D. Obinata, M. Endo, T. Sakurai, S. Ojima, T. Katayama and K. Fugami 43 Preparation of Anisotropic Chitosan Hydrogel with Birefringence and Analysis of Gel Formation Process N. Tomita, Y. Maki, T. Yamamoto and T. Dobashi 48 Thermosensitive Micelles Composed of Poly(lactide)-g-Poly(NIPAM-co-HEMA) Graft Copolymers T.M. Quynh, M. Yoneyama, Y. Maki, N. Nagasawa and T. Dobashi 51 Nano-Platelet Structure of Clay Materials Observed by Atomic Force Microscope M. Kakiage, R. Takamatsu, H. Uehara, T. Yamanobe and K. Suzuki 57 Synthesis and Properties of Fluorescent Biological Molecules Labeled with Novel Silylated Perylene Derivative Y. Sato, A. Ozaki, M. Hosaka, T. Moriguchi and K. Shinozuka 63 Effect of Organometallic Compounds on the Formation of Carbon Nanostructures by Pulsed Electric Discharge of Fluorine-Containing Organic Liquid between Metal Electrodes K. Hosoi and S. Kuroda 67 Control of Methanol Crossover Using a Perforated Metal Sheet for DMFC Application T. Tsujiguchi, N. Masumi, A. Kawakubo and N. Nakagawa 71 A Key Factor for the Actual Application of a Vapor Feed Passive DMFC Operated with High Concentration of Methanol M.A. Abdelkareem and N. Nakagawa 78 Relationship between Dielectric Characteristic by DEP Levitation and Differentiation Activity for Stem Cells Y. Hirota and M. Hakoda 84 b Silicon Science and Advanced Micro-Device Engineering I Application of Micro-Metal Textile for Flexible Dye-Sensitized Solar Cell K. Kakiage, E. Fujimura, M. Abe, H. Shinoda, T. Kyômen and M. Hanaya 92 The Hydrophobicity of Micro Water Pool and the Interfacial Fluidity of PC-Based W/O Microemulsion Droplet Involved with Reactivity of Phospholipase A 2 K. Yamazaki and M. Imai 100 III. Nano-Science and Technology Simple Nanoimprint Lithography with 50 nm Resolution Using Vacuum Packing K. Itoh, H. Hirai, T. Ando, K. Takagi and K. Noguchi 111 Fabrication of Nanometer Sized Si Dot Arrays Using Ar Ion Milling with Calixarene Resist Dot Arrays T. Tamura, Y. Tanaka, T. Akahane, Y. Yin and S. Hosaka 116 Self-Assembled Nanodot Fabrication by Using Diblock Copolymer M. Huda, Y. Yin and S. Hosaka 120 Guide Pattern for Long-Range-Order Nanofabrication of Self-Assembled Block Copolymers T. Akahane, M. Huda, Y. Yin and S. Hosaka 124 Prototype of Illumination-Collection Mode Scanning Near-Field Optical Microscopy and Raman Spectroscopy with Gold Inner-Coated Aperture-Less Pyramidal Probe S. Hosaka, H. Koyabu, Y. Aramomi, H. Sone, Y. Yin, E. Sato and K. Tochigi 129 Prototype of Frame-Type Cantilever for Biosensor and Femtogram Detection H. Sone, S. Ichikawa, Y. Matsubara, M. Suzuki, H. Okano, T. Izumi and S. Hosaka 134 Large Resistance Ratio for High Reliability of Multi-Level Storage in Phase-Change Memory Y. Yin, T. Noguchi, H. Ohno and S. Hosaka 140 Proposed Phase-Change Memory with a Step-Like Channel for High-Performance Multi- State Storage Y. Yin and S. Hosaka 145 IV. Photonics Device and Technology Mach-Zehnder Type Thermo-Optic Switch with Antenna-Coupled Y-Junction Fabricated by Selective Photobleaching of Polysilane Films O. Hanaizumi, K. Miura, Y. Hiratani, Y. Machida and M. Uehara 153 Polarization Control of SOA-Fiber Ring Laser Y. Takahashi and R. Niida 157 Theoretical Analysis of Photonic Band Gaps and Defect Modes of Novel Photonic Crystal Waveguides Consisting of Si-Ion Implanted SiO Using the Finite-Difference Time-Domain 2 Method A.V. Umenyi, S. Kawashiri, K. Miura and O. Hanaizumi 162 Design and Fabrication of Novel Photonic Crystal Waveguide Consisting of Si-Ion Implanted SiO Layers 2 A.V. Umenyi, M. Honmi, S. Kawashiri, T. Shinagawa, K. Miura, O. Hanaizumi, S. Yamamoto, A. Inouye and M. Yoshikawa 168 Demonstration of Light-Emitting Two-Dimensional Photonic Crystals Composed of Silicon- Rich Silicon-Dioxide Thin Films K. Miura and O. Hanaizumi 173 V. Novel Measurement and System Technology Tilt Mechanism for Precision Control of Down-Slope Component of Gravitational Force for Micro Force Generation K. Maru, W. Khunnam, L. Hu, R.S. Lu, P.P. Yupapin and Y. Fujii 179 Microforce Material Tester Using Small Pendulum J. Ozawa, K. Maru, K. Kobayashi and Y. Fujii 183 Key Engineering Materials Vol. 459 c Interdigital Ring Coupler Sensor for Parameter Estimation of Moving Objects T. Miwa and Y. Yamakoshi 190 A Design Method for Two-Degree-of-Freedom Multi-Period Repetitive Control Systems K. Yamada, N. Nakazawa, I. Murakami, Y. Ando, T. Hagiwara, S. Yamamoto, N.L.T. Nguyen and T. Sakanushi 194 A Design Method for Modified PID Control Systems to Attenuate Unknown Disturbances T. Hagiwara, K. Yamada, I. Murakami, Y. Ando and S. Matsuura 211 A Design Method for Stabilizing Modified Smith Predictors for Multiple-Input/Multiple- Output Time-Delay Plants K. Yamada, N.T. Mai, Y. Ando, T. Hagiwara, I. Murakami and T. Hoshikawa 221 A Novel Thermoelectric System with Conductive Metal Rods and its Effective Seebeck Coefficients T. Sasaki, Y. Kondoh, O. Hanaizumi and M. Goto 235 VI. Information and Communication Engineering Architecture of Wideband High-Efficiency Envelope Tracking Power Amplifier for Base Station M. Kaneta, A. Kanbe, H. Hirata, T. Shimura, K. Yamagishi and H. Kobayashi 241 High-Speed Data Transmission Techniques Using Raised Cosine Signaling Y. Yuminaka 252 High-Speed Multiple-Valued Data Transmission Based on Time-Domain Pre-Emphasis Techniques Y. Yuminaka and K. Henmi 260 Dynamics Simulation of Microbubbles in Ultrasonic Wave Field Considering the Secondary Bjerknes Force T. Miwa and Y. Yamakoshi 271