Reference Materials in Measurement and Technology: Proceedings of the Third International Scientific Conference PDF
Preview Reference Materials in Measurement and Technology: Proceedings of the Third International Scientific Conference
Ural Scientific Research Institute for Metrology Reference Materials in Measurement and Technology Proceedings of the Third International Scientific Conference Reference Materials in Measurement and Technology Sergei V. Medvedevskikh Olga N. Kremleva (cid:129) (cid:129) ’ Irina E. Vasil eva Egor P. Sobina (cid:129) Editors Reference Materials in Measurement and Technology Proceedings of the Third International fi Scienti c Conference 123 Editors SergeiV.Medvedevskikh OlgaN.Kremleva UralScientificResearch UralScientificResearch Institute for Metrology Institute for Metrology Ekaterinburg, Russia Ekaterinburg, Russia Irina E. Vasil’eva EgorP. Sobina A.P. Vinogradov Institute of Geochemistry UralScientificResearch Siberian Branch,Russian Academy Institute for Metrology of Sciences Ekaterinburg, Russia Irkutsk,Russia ISBN978-3-030-32533-6 ISBN978-3-030-32534-3 (eBook) https://doi.org/10.1007/978-3-030-32534-3 ©SpringerNatureSwitzerlandAG2020 Thisworkissubjecttocopyright.AllrightsarereservedbythePublisher,whetherthewholeorpart of the material is concerned, specifically the rights of translation, reprinting, reuse of illustrations, recitation, broadcasting, reproduction on microfilms or in any other physical way, and transmission orinformationstorageandretrieval,electronicadaptation,computersoftware,orbysimilarordissimilar methodologynowknownorhereafterdeveloped. The use of general descriptive names, registered names, trademarks, service marks, etc. in this publicationdoesnotimply,evenintheabsenceofaspecificstatement,thatsuchnamesareexemptfrom therelevantprotectivelawsandregulationsandthereforefreeforgeneraluse. The publisher, the authors and the editors are safe to assume that the advice and information in this book are believed to be true and accurate at the date of publication. Neither the publisher nor the authors or the editors give a warranty, expressed or implied, with respect to the material contained hereinorforanyerrorsoromissionsthatmayhavebeenmade.Thepublisherremainsneutralwithregard tojurisdictionalclaimsinpublishedmapsandinstitutionalaffiliations. ThisSpringerimprintispublishedbytheregisteredcompanySpringerNatureSwitzerlandAG Theregisteredcompanyaddressis:Gewerbestrasse11,6330Cham,Switzerland Preface This Springer collection features selected fundamental and appliedresearch papers devoted to various issues involved with the development and application of refer- encematerialsandmethods.ThesepaperswerepresentedattheThirdInternational ScientificConferenceReferenceMaterialsinMeasurementandTechnology,which was held on 11–14 September 2018 in Ekaterinburg (Russia) under the auspices of the Federal Agency for Technical Regulation and Metrology (Rosstandart) and the Ural Scientific Research Institute for Metrology (UNIIM), a scientific method- ological centre of the State service of reference materials for the composition and properties ofsubstances andmaterials. The conference was aimed at facilitating the exchange of scientific information between its participants about fundamental and applied research in the field of reference materials, as well as at attracting attention to reference materials as an importanttechnicalandregulatorybasisforensuringtheuniformityandaccuracyof measurements. In the context of knowledge economy, when digitisation comes to embrace not only industrial and social sectors, but also the entire quality control infrastructure, the maintenance of international uniformity of measurements becomes essential. In turn, the system aimed at providing uniformity of measure- ments also undergoes massive transformations concerned with increased informa- tisation and digitisation. Under these circumstances, metrological activity is acquiring an infrastructural character by bolstering the national economy in all areas of activity, including health care, labour safety, pharmaceutical production, environmental protection, development and maintenance of diagnostic equipment. There is a clear trend towards theuseofmeasuringinstrumentswithdistributed andvirtual components, as well as cloud computing services and databases. Intelligentsystemsareintendedtosimplifyandoptimiseproductionandsupport the development of new technologies and substances. Already, new technologies permit more accurate data on measurementobjectsto be obtained, while advanced dataprocessingmethodsofferimprovedapproachestoanalysingsuchmeasurement data. Experimental work devoted to the development of new reference materials is also becoming more accurate and efficient. As a result, the problem of both v vi Preface expanding the range and increasing the quality of modern reference materials is movingtotheforefront.Anotherurgenttaskistheoptimisationofmechanismsfor forecasting the needs of states and society in terms of metrological measurement support, which can be achieved by increasing the competitiveness of domestic reference materials in international markets. Therefore, in the context of global digitalisation, key objectives of metrological support include not only monitoring but also a prompt response to the growing demands of national economies. Leading experts in the field of measurements and reference materials from dif- ferent countries are working on solving the aforementioned issues. The Third International Scientific Conference Reference Materials in Measurement and Technology brought together scientists, lecturers, postgraduate researchers and practitionersfromvariousuniversities,researchinstitutesandindustrialcompanies. The conference was also attended by the representatives of ISO/REMCO, CITAC, COOMET, COMAR Central Secretariat and experts in the area of reference materials from Belarus, Germany, Israel, Kazakhstan, the Netherlands, Poland, Russia, South Africa, Switzerland and the USA. Theconferencehostedmeetingsof11themedsections.Duringplenary,themed and poster conference sections, participants made over 80 presentations. This collection contains 21 conference papers, which were selected during a rigorousdouble-blindpeer-reviewprocessorganisedbytheeditorsofthisevent.The papers presented in this collection were published in Russian in the peer-reviewed scientific and technical journal Reference Materials. Ekaterinburg, Russia Sergei V. Medvedevskikh Ekaterinburg, Russia Olga N. Kremleva Irkutsk, Russia Irina E. Vasil’eva Ekaterinburg, Russia Egor P. Sobina Acknowledgements OnbehalfoftheOrganisingCommitteeoftheThirdInternationalScientific Conference Reference Materials in Measurement and Technology,we express our sincere grati- tude to all invited speakers, section chairpersons and conference participants for their valuable contribution to this event. We are also thankful to Anna Kveglis and Dr. Natalia Popova, Head oftheForeignLanguagesDepartmentoftheInstituteofPhilosophyandLaw,UralBranchofthe RussianAcademyofSciences(Ekaterinburg)fortheirassistanceintranslatingandpreparingthis bookforpublication. We especially appreciate the work done by the members of the Conference Organising CommitteeI.E.Vasil’eva,A.I.Krylov,M.V.Okrepilov,N.P.Muravskaya,E.V.Kulyabina, whogreatlyhelpedinreviewingandeditingtheseconferenceproceedings. Contents Development and Creation of Reference Materials Development of Interlaboratory Comparison Test Samples and Reference Materials for the Quality Assurance of Air Composition Measurements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 Anna M. Bogacheva, Olga B. Ponomareva and Yuliya V. Kanaeva Metrological Assurance of Dioxin Measurements. A Certified Reference Material for Measuring the Dioxin Mass Fraction in Animal Fat. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11 Alexandra G. Budko, Alena Y. Mikheeva and Anatoliy I. Krylov Development of Certified Reference Materials for Physicochemical Analysis. Certified Reference Solutions for the Composition of Aqueous Aluminium, Indium, Magnesium, Nickel and Titanium. . . . . . 27 Ianina I. Ermakova, Alexander V. Ivanov, Irina N. Zyablikova and Anna N. Shobina Multiparametric Reference Materials for Metrological Support in the Area of Coating Parameter Control. . . . . . . . . . . . . . . . . . . . . . . 39 Vyacheslav V. Kazantsev and Alexander S. Vasilyev Reference Materials Used for Specific Safety Evaluation of Human Immunoglobulin and Human Albumin Products: Features of Development, Certification and Application. . . . . . . . . . . . . . . . . . . . 47 Olga G. Kornilova, Maxim A. Krivykh, Rauza A. Volkova and Igor V. Borisevich Reference Materials for Ensuring the Metrological Traceability of Enzyme Catalytic Activity Measurement (KATAL) . . . . . . . . . . . . . . 57 Elena V. Kulyabina, Olga N. Melkova, Ekaterina A. Guskova and Tatiana V. Grebennikova vii viii Contents Manufacturing and Certification of Reference Materials for the Mass Fraction of Boron in Silumin. . . . . . . . . . . . . . . . . . . . . . . 67 Dmitry G. Lisienko, Margarita A. Dombrovskaya and Eugeniya D. Kubrina PreparationandCertificationofaReferenceMaterialforthePhysical Properties of Clay Soils (Loam) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 77 Ilona N. Matveeva and Vladimir V. Tolmachev Development of Reference Materials for Thermodynamic Properties: Metrological Support of Measurements in the Field of Thermal Analysis and Calorimetry in Russia . . . . . . . . . . . . . . . . . . . . . . . . . . . . 83 Andrey M. Nepomiluev, Vyacheslav V. Kazantsev and Artyom P. Shipitsyn Development of Alumina-Based Porosity Reference Materials for the Mercury Porosimetry Method . . . . . . . . . . . . . . . . . . . . . . . . . . 91 Egor P. Sobina Development of a Reference Material for the Composition of 0.1M Potassium Dichromate Solution. Certified Reference Material GSO 10992-2017 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 107 Alexander Yu. Shimolin and Alena V. Sobina Development and Testing of a Certified Reference Material of the Lead Mass Fraction in Solutions for Measurements Using Inductively Coupled Plasma Methods. . . . . . . . . . . . . . . . . . . . . . 123 Alexey A. Stakheev and Tatiana P. Stolboushkina Radiation-Sensitive Film Compositions for Measuring Absorbed Doses Within the 100–1000 Gy Range . . . . . . . . . . . . . . . . . . . . . . . . . . 131 Vladimir P. Tenishev and Ivan A. Emelyanenko Developing a Reference Material Set for the Magnetic Properties of NdFeB Alloy-Based Hard Magnetic Materials . . . . . . . . . . . . . . . . . . 141 Ekaterina A. Volegova, Tatiana I. Maslova, Vladimir O. Vaskovskiy and Aleksey S. Volegov Mathematical and Statistical Support of Reference Material Characterisation Estimation of Consensus Value of Interlaboratory Measurement Results Accompanied by a Minimum Increase in Associated Uncertainty. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 151 Peter M. Aronov Contents ix Quality Assessment of the Preparation of Reference Materials of Moist Solid Substances. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 157 Sergej V. Medvedevskikh, Maria Yu. Medvedevskikh and Maria P. Krasheninina A Method for Estimating the Certified Value Uncertainty of a Multicomponent Reference Material . . . . . . . . . . . . . . . . . . . . . . . . 175 Pavel V. Migal, Sergei V. Medvedevskikh and Valery A. Firsanov Use of Reference Materials Bismuth-Containing Glassy Reference Materials for Establishing the Content of Transition Elements Using Luminescent-Based Methods . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 189 Valentina V. Borisova, Valentin A. Kutvitsky, Elena V. Mironova, Inna A. Romanova and Olga I. Ostanina Participation of the All-Russian Research Institute of Physical-Technical and Radio-Technical Measurements (VNIIFTRI) in International Comparisons in the Field of Physicochemical Measurements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 201 Vladimir I. Dobrovolskiy, Narine G. Oganyan, Sergey V. Prokunin and Alexey A. Stakheev Quality Improvement of Commercially Available Certified Reference Gas Mixtures . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 209 Leonid A. Konopelko, Anna V. Kolobova and Olga V. Fatina Application of Raman Spectroscopy in the Quality Control of Injectable Medicines. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 219 Maria P. Krasheninina, Maria Yu. Medvedevskikh, Ekaterina V. Galeeva and Roman R. Galeev Reference Materials for Isotopic Composition Used in Implementing Isotope Dilution Mass Spectrometry. . . . . . . . . . . . . . . . . . . . . . . . . . . . 237 Olga N. Kremleva and Tatiana N. Tabatchikova Combined Measurement Uncertainty for pH-Values Using Certified Reference Materials in Potentiometric Measurements with Glass Electrodes. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 251 Samuel Wunderli Development and Creation of Reference Materials
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