Particles on Surfaces 9: Detection, Adhesion and Removal TThhiiss ppaaggee iinntteennttiioonnaallllyy lleefftt bbllaannkk PARTICLES ON 9: SURFACES DETECTION, ADHESION AND REMOVAL Editor: K.L. Mittal //IVS Pill LEIDEN • BOSTON 2006 CRC Press Taylor & Francis Group 6000 Broken Sound Parkway NW, Suite 300 Boca Raton, FL 33487-2742 © 2006 by Taylor & Francis Group, LLC CRC Press is an imprint of Taylor & Francis Group, an Informa business No claim to original U.S. Government works Version Date: 20120727 International Standard Book Number-13: 978-9-04-741822-1 (eBook - PDF) This book contains information obtained from authentic and highly regarded sources. Reasonable efforts have been made to publish reliable data and information, but the author and publisher cannot assume responsibility for the validity of all materials or the consequences of their use. The authors and publishers have attempted to trace the copyright holders of all material reproduced in this publication and apologize to copyright holders if permission to publish in this form has not been obtained. If any copyright material has not been acknowledged please write and let us know so we may rectify in any future reprint. Except as permitted under U.S. Copyright Law, no part of this book may be reprinted, reproduced, transmitted, or utilized in any form by any electronic, mechanical, or other means, now known or hereafter invented, including photocopying, microfilming, and recording, or in any information stor- age or retrieval system, without written permission from the publishers. For permission to photocopy or use material electronically from this work, please access www.copy- right.com (http://www.copyright.com/) or contact the Copyright Clearance Center, Inc. (CCC), 222 Rosewood Drive, Danvers, MA 01923, 978-750-8400. CCC is a not-for-profit organization that pro- vides licenses and registration for a variety of users. For organizations that have been granted a pho- tocopy license by the CCC, a separate system of payment has been arranged. Trademark Notice: Product or corporate names may be trademarks or registered trademarks, and are used only for identification and explanation without intent to infringe. Visit the Taylor & Francis Web site at http://www.taylorandfrancis.com and the CRC Press Web site at http://www.crcpress.com Contents Preface Vll Part 1: Particle Detection/A nalysis/Characterization and General Cleaning-Related Topics Recent developments in imaging and analysis of micro- and nanosize particles and surface features R. Kohli 3 Photodigital imaging as a means of monitoring particulate contamination on surfaces R. Kaiser, J Grilly and A. Kulczyk 63 Determination of residual particles on surfaces. An updated method for particle extraction using ultrasonics S. B. Awad 75 Laser inactivation of surfaces and detection of bacteria I. A. Watson, D. E. S. Stewart-Tull, R. Parton,!. Peden, A. Yeo, B. K. Tan and G. Ward 83 Laser-assisted nanofabrication on surfaces using micro- and nanoparticles Y. F. Lu, L. P. Li, K. K. Mendu, J. Shi, D. W Doerr and D. R. Alexander 95 Clean-then-assemble versus assemble-then-clean: Several comparisons R. W Welker I 07 Development of a non-contact post-CMP cleaning process for copper D. A. Koos, J Svirchevski, D. J. Vitkavage, D. G. Hansen, K. A. Reinhardt, F. Huang, M Mitchel and G. Zhang 127 Using ozonated DI water for pre-gate cleaning L. Liu, I. Kashkoush, A. Walter and R. Novak 145 VI Contents Decontamination of surrogate Pu-238 legacy wastes R. Kaiser, J Desrosiers and A. Kulczyk 153 Solar panel obscuration by dust and dust mitigation in the Martian atmosphere M K. Mazumder, A. S. Biris, C. E. Johnson, C. U. Yurteri, R. A. Sims, R. Sharma, K. Pruessner, S. Trigwell and J S. Clements 16 7 Part 2: Particle Adhesion and Removal Adhesion and friction of single micrometer-sized particles M Kappl, L. Heim, S. Ecke, M Farshchi and H. J Butt 199 The effect of laser-induced micro-roughness of textile fibers on adhesion and capture of micrometer-sized particles T. Bahners, K. Opwis, T. Textor, W Labuda and E. Schollmeyer 211 Advances in wafer cleaning and particle removal technology K. A. Reinhardt 225 Particle removal challenges and solutions in semiconductor fabrication CMP processes M T. Andreas 243 Laser cleaning of model sub-micrometer particulate contaminants from Si surfaces S. I. Kudryashov, S. D. Shukla and S. D. Allen 255 Removal of particles using the combined effect oflaser-induced shock wave and explosive vaporization of liquid D. Jang and D. Kim 267 Particle removal by attenuated total internal reflection of laser light G. Dube, A. J Braundmeier, Jr. and J. D. Kelley 277 Removal of sub-1 00-nm particles from structured substrates with C0 snow 2 J C. J van der Danek, R. Schmits, R. E. van Vliet and Ton (A.) G. T M Bastein 291 Particle removal by dense-phase fluids using ultrasonics W T. McDermott, G. Parris, D. V Roth and C. J Mammarella 303 Prediction of particle removal using surfactants M L. Free 317 Removal of micrometer-size particles from solid surfaces by an impinging air jet K. Gotoh 329 Particles on Swfaces 9: Detection, Adhesion and Removal, pp. vii-viii Ed. K.L. Mittal ((;! VSP 2006 Preface This volume chronicles the proceedings of the 9th International Symposium on Par ticles on Surfaces: Detection, Adhesion and Removal held under the aegis of MST Conferences in Philadelphia, PA, June 17-18, 2004. This event represented a con tinuation of the series of symposia initiated on this topic in 1986 under the auspices of the Fine Particle Society. Since 1986 this topic has been covered on a regular bi ennial basis (except that no symposium was held in 1994) and the proceedings of these earlier symposia have been properly documented in seven hard-bound books [ 1-7]. Apropos, because of the interest in and tremendous importance of this topic, the next (lOth) event in this series is scheduled to be held in Toronto, Canada dur ing June 19-21, 2006. This symposium was organized with the following objectives in mind: to provide an update on this topic since the last symposium, to provide a forum for cross pollination of ideas, and to identify areas which needed intensified R&D efforts. As mentioned in the Prefaces to the previous books in this series, the study of particles on surfaces is crucially important in a legion of diverse technological areas, ranging from microelectronics to biomedical to space. With the burgeoning interest in nanotechnologies, the need to detect, characterize, analyze and remove particles on a nanoscale becomes quite patent. Moreover, it is quite obvious that the need to re move sub-nanometer particles will become more and more intense in the future. The technical program for this symposium was comprised of 31 papers covering many different aspects of particles on surfaces. The presentations ranged from criti cal reviews of particular subtopics to original research contributions, and the pre senters hailed from academia, industry and other research organizations. There were spontaneous, lively and illuminating (not exothermic) discussions throughout the symposmm. Now coming to this volume, it contains a total of 21 papers covering many rami fications of particles on surfaces, ranging from detection to removal. Apropos, this volume also contains a paper which was not listed in the program but is quite rele vant and an important addition to this book. It must be recorded that all manuscripts were rigorously peer-reviewed and revised (some twice or thrice) and properly ed ited before inclusion in this book. Concomitantly, this volume represents an archi val publication of the highest standard. It should not be considered a proceedings volume in the usual and ordinary sense, as many proceedings volumes are neither peer-reviewed nor adequately edited. This volume is divided into two parts: Part 1: Particle Detection/A nal ysis/Characterization and General Cleaning-Related Topics; and Part 2: Particle Vlll Preface Adhesion and Removal. The topics covered include: imaging and analysis of micro and nanosize particles and surface features; determination of particles on surfaces; laser inactivation of surfaces; laser-assisted nanofabrication on surfaces; post-CMP cleaning process; pre-gate cleaning; solar panel obscuration in the Martian atmos phere; adhesion and friction of microsized particles; microroughness of textile fi bers and capture of particles; factors affecting particle adhesion and removal; vari ous techniques for cleaning or removal of particles from different substrates including laser, combination of laser-induced shock wave and explosive vaporiza tion of liquid, attenuated total internal reflection of laser light, C0 snow, use of 2 dense-phase fluids, use of surfactants, and impinging air jet; and removal of sub- 10 0-nm particles. This volume and its predecessors [ 1-7] containing bountiful information on vari ous ramifications of particles on surfaces provide a unified and comprehensive ref~ erence source, and yours truly hopes that anyone interested or involved (centrally or peripherally) in any aspect of particles on surfaces will find these volumes of great interest and value. Acknowledgements Now comes the pleasant task of thanking those who helped in many and different ways. First, I am thankful to Dr. Robert H. Lacombe, a dear friend and colleague, for taking care of many details entailed in organizing this symposium. The unsung heroes (reviewers) must be thanked profusely for their time and efforts in providing valuable comments which are a sine qua non for maintaining high standard of any publication. Special thanks are extended to the authors for their interest, cooperation and for providing written accounts of their presentations without which this book could not be materialized. Finally, my sincere appreciation goes to the staff of Brill Academic Publishers for giving this book a body form. K. L. Mittal P.O. Box 1280 Hopewell Jet., NY 12533 I. K. L. Mittal (Ed.), Particles on Surfaces 1: Detection. Adhesion and Removal, Plenum Press, New York (1988). 2. K. L. Mittal (Ed.). Particles on Swfaces 2: Detection, Adhesion and Removal, Plenum Press. New York (1989). 3. K. L. Mittal (Ed.), Particles on Surfaces 3: Detection, Adhesion and Removal, Plenum Press, New York (1991). 4. K. L. Mittal (Ed.), Particles on Surfaces: Detection, Adhesion and Removal. Marcel Dekker, New York ( 1995). (Proceedings of the 4th Symposium.) 5. K. L. Mittal (Ed.), Particles on Surfaces 5&6: Detection, Adhesion and Removal, VSP, Utrecht (1999). (Proceedings of the 5th & 6th Symposia.) 6. K. L. Mittal (Ed.), Particles on Swfaces 7: Detection, Adhesion and Removal, VSP. Utrecht (2002). 7. K. L. Mittal (Ed.), Particles on Smfaces 8: Detection, Adhesion and Removal, VSP, Utrecht (2003). Part 1 Particle Detection/A nalysis/ Characterization and General Cleaning-Related Topics
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