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NASA Technical Reports Server (NTRS) 20150003433: Method and Apparatus for Non-Destructive Evaluation of Materials PDF

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(cid:9)(cid:9)(cid:9) 1111111111111111111inuuu1111111111u ~ (12) United States Patent (lo) Patent No.: (cid:9) US 8,928,316 B2 Goldfine et al. (45) Date of Patent: (cid:9) Jan. 6, 2015 (54) METHOD AND APPARATUS FOR 324/519, 658, 661, 686, 718, 754.28; NON-DESTRUCTIVE EVALUATION OF 702/35, 38, 47, 52, 57-59, 127, 182, MATERIALS 702/183, 185; 73/760, 763, 774, 780, 73/862.626, 335.04 (75) Inventors: Neil J. Goldfine, Newton, MA (US); See application file for complete search history. Andrew P. Washabaugh, Chula Vista, CA (US); Robert Lyons, Pelham, MA (56) References Cited (US); Zachary Thomas, Cambridge, U.S. PATENT DOCUMENTS MA (US); David A. Jablonski, Whitman, MA (US); Christopher 4,348,635 A * 9/1982 (cid:9) Wright et al . (cid:9) ................. (cid:9) 324/559 Martin, Concord, MA (US) 4,814,690 A 3/1989 (cid:9) Melcher et al. 5,015,951 A (cid:9) * 5/1991 (cid:9) Melcher (cid:9) ........................ (cid:9) 324/232 (73) Assignee: JENTEK Sensors, Inc., Waltham, MA (Continued) (US) OTHER PUBLICATIONS (*) Notice: (cid:9) Subject to any disclaimer, the term of this ASTM WK8211 "Standard Guide for Nondestructive Testing of patent is extended or adjusted under 35 Polymer Matrix Composites Used in Aerospace Applications," Des- U.S.C. 154(b) by 411 days. ignation: E2533-09, (Jul. 2009). (21) Appl. No.: 13/297,933 (Continued) (22) Filed: (cid:9) Nov. 16, 2011 Primary Examiner Hoai-An D Nguyen (74) Attorney, Agent, or Firm Hamilton, Brook, Smith & (65) (cid:9) Prior Publication Data Reynolds, P.C. US 2012/0126803 Al (cid:9) May 24, 2012 (57) ABSTRACT Methods and apparatus for characterizing composite materi- Related U.S. Application Data als for manufacturing quality assurance (QA), periodic (60) Provisional application No. 61/414,008, filed on Nov. inspection during the useful life, or for forensic analysis/ 16, 2010, provisional application No. 61/524,520, material testing. System are provided that relate eddy-current filed on Aug. 17, 2011. sensor responses to the fiber layup of a composite structure, the presence of impact damage on a composite structure with (51) Int. Cl. or without a metal liner, volumetric stress within the compos- GOIR 33112 (cid:9) (2006.01) ite, fiber tow density, and other NDE inspection requirements. GOIN27182 (cid:9) (2006.01) Also provided are systems that determine electromagnetic GOIR 33110 (cid:9) (2006.01) material properties and material dimensions of composite GOIR 33100 (cid:9) (2006.01) materials from capacitive sensor inspection measurements. (52) U.S. Cl. These properties are related to the presence of buried defects CPC ............ GOIR 33110 (2013.01); GOIR 3310064 in non-conductive composite materials, moisture ingress, (2013.01); GOIR 3310094 (2013.01) aging of the material due to service or environmental/thermal USPC ............ 324/242; 324/238; 324/239; 324/243 exposure, or changes in manufacturing quality. (58) Field of Classification Search USPC ......... 324/216, 228, 237-240, 456, 500, 512, 8 Claims, 12 Drawing Sheets 100 ~ 11G Ensvum,;nt ttt- (cid:9) 113 (cid:9) 116 (cid:9) 119 ~prnc¢a5pr ~ ..Enterface (cid:9) triemorY (cid:9) Interface ~ it& 1G9 it7 hd R (cid:9) "wgnal Hardware (cid:9) Generator Motion 11R ecorder F, ue 14G 143 Motion (cid:9) Sensor Encoder (cid:9) 120 nneters rest anaea at (cid:9) tN US 8,928,316 B2 Page 2 (56) (cid:9) References Cited Goldfine, "Uncalibrated, Absolute Property Estimation and Mea- surement Optimization for Conducting and Magnetic Media Using U.S. PATENT DOCUMENTS Imposed w-k Magnetometry," Doctoral Thesis, Massachusetts Insti- tute of Technology, Cambridge, MA, pp. 1-139, (Sep. 1990). 5,345,514 A * 9/1994 Mandavieh et al. (cid:9) .......... 382/152 Goldfine, et al., "Eddy Current Sensor Networks for Aircraft Fatigue 5,453,689 A 9/1995 Goldfine et al. Monitoring," ASNT Materials Evaluation, Aerospace Health Moni- 5,747,999 A * 5/1998 Yamaoka (cid:9) ...................... 324/501 5,895,439 A * 4/1999 Fisher et al . (cid:9) .................... 702/36 toring, 61(7):1-13, (Jul. 2003). 6,188,218 B1 * 2/2001 Goldfine et al . (cid:9) .............. 324/243 Goldfine, et al., "Rapid Nonlinear `System' Identification for NDT, 6,380,747 B1 4/2002 Goldfine et al. Using Sensor Response Databases," Mat. Eval., 66(7):1-12, (Jul. 6,784,662 B2 * 8/2004 Schlicker et al . (cid:9) ............. 324/242 2008). 6,992,482 B2 1/2006 Shay et al. Hashin, "Analysis of Properties of Fiber Composites with 7,161,350 B2 * 1/2007 Goldfine et al . (cid:9) .............. 324/238 Anisotropic Constituents," J. App. Mech., 46(3):543-550, (Sep. 7,839,282 B1 * 11/2010 Mathur et al . (cid:9) ................ 340/562 1979). 8,264,243 B2 * 9/2012 Tarui et al . (cid:9) .................... 324/663 2003/0071615 Al* 4/2003 Schlicker et al . (cid:9) ............. 324/242 Melcher, "Continuum Electromechanics," The MIT Press, Cam- 2003/0164700 Al* 9/2003 Goldfine et al . (cid:9) .............. 324/235 bridge, MA (1981). 2004/0004475 Al* 1/2004 Goldfine et al . (cid:9) .............. 324/242 Park, J.B., et al., "Electromechanical Modeling of Unidirectional 2004/0056654 Al* 3/2004 Goldfine et al . (cid:9) .............. 324/239 CFRP Composites under Tensile Loading Condition," Composites: 2004/0066188 Al* 4/2004 Goldfine et al . (cid:9) .............. 324/228 Part A, 33:267-275, (2002). 2004/0225474 Al* 11/2004 Goldfine et al . (cid:9) .............. 702/183 Russell, John D., "Composites Affordability Initiative: Transitioning 2004/0232911 Al* 11/2004 Schlicker et al . (cid:9) ............. 324/242 Advanced Aerospace Technologies through Cost and Risk Reduc- 2007/0120561 Al* 5/2007 Goldfine et al . (cid:9) .............. 324/238 2010/0045277 Al* 2/2010 Goldfine et al . (cid:9) .............. 324/209 tion," The AMMTIAC Quarterly, 1(3):3-6, (2006). 2012/0123699 Al* 5/2012 Kawata et al . (cid:9) .................. 702/35 Wang, X., et al., "Electromechanical Behavior of Carbon Fiber," OTHER PUBLICATIONS Carbon, 35(5): 452-453, (1997). Wang, X., et al., "Electromechanical Study of Carbon Fiber Com- Goldfine, "Magnetometers for Improved Materials Characterization posites," J. Mater. Res., 13 (11):3081-3092, (Nov. 1998). in Aerospace Applications," Materials Evaluation, pp. 396-405, (Mar. 1993). * cited by examiner (cid:9) U.S. Patent ,Tan. 6, 2015 (cid:9) Sheet 1 of 12 (cid:9) US 8,928,316 B2 110 Instrument Motion Recorder L,, 121 123 (cid:9) Fixture 140 143 Motion (cid:9) Sensor Encoder (cid:9) 120 Motors "t Object 141 (cid:9) 130 Fig. 1 (cid:9) U.S. Patent (cid:9) Jan. 6, 2015 (cid:9) Sheet 2 of 12 US 8,928,316 B2 200 i Fig. 2A 210 220 V (cid:9) . Fig. 26(cid:9) Fig. 2C (cid:9) U.S. Patent (cid:9) Jan. 6 2015 (cid:9) Sheet 3 of 12 US 8,928,316 B2 , I Grw Fig. 3 (cid:9) 400 420 I Fig. 4A Fig. 4B ~ 420 Fig. 4C (cid:9) Fig. 4D (cid:9) U.R. Patent Jan 6 2013 (cid:9) Sheet 4 of 12 (cid:9) US 8,928, 16 G2 }\\ ~ \%\ \\ƒ ~ \\ ~ ~ \ ca LO , , ? ) LL LL ~ ~ N (cid:9) U.S. Patent Jan. 6, 2015 (cid:9) Sheet 5 of 12 (cid:9) US 8,928,316 B2 600 10.0 MHz - Wgnftdo v (cid:9) i 0movin g 605 601 (cid:9) 1 §: airTM L (cid:9) Thal Variation During tational Scan il,V (cid:9) X4 W, k-o", mss: 610 10,00 MHz - Phase VS, X axis 410-flow MARV average) (cid:9) (cid:9) 603 605 ,.4 fi bers X,v f, 601 (cid:9) 4S, "Op fibers $s N .4h lop 1~`. qF £nk (cid:9) U.S. Patent (cid:9) Jan. 6, 2015 (cid:9) Sheet 6 of 12 US 8,928,316 B2 705 Process impedance response Identify fiber wraps from response 711 709 NO Within specfficabon? Reject test object 1 YES 713 (cid:9) NO More for-ations? End 715 YES Position sensor at net location Fig. 7 U.S. Patent (cid:9) Jan. 6, 2015 (cid:9) Sheet 7 of 12 (cid:9) US 8,928,316 B2 800 Start 801 803 Processing the impedances to obtain a current property image 805 Registering the current property image with a baseline property image 807 Differencing the registered images 809 Determining an amount of damage based on the property change End Fig. 8 U.S. Patent (cid:9) Jan. 6, 2015 (cid:9) Sheet 8 of 12 (cid:9) US 8,928,316 B2 900 to Ft 901 905 (cid:9) ............ Processing the first impedances to obtain a first property image characterizing the composite overwr 907 " Processing the second impedances to obtain a second property image characterizing the liner 909 Analyzing the first and second property images to identify damage. End Fig. 9

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