Journal of Analytical and Applied Pyrolysis 1993: Vol 25 Table of Contents

3 Pages·1993·0.77 MB·English

JOURNAL OF ANALYTICAL AND APPLIED PYROLYSIS JUNE 1993
Special Issue
Proceedings of the 10th International Conference on Fundamental Aspects, Processes and Applications of
Pyrolysis, Hamburg, Germany, September 28-—October 2, 1992
Preface
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Editorial: A change in scope
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Analytical and Instrumental Analysis
Pyrolysis—gas chromatography for end group analysis of polystyrene macromonomers using
stepwise pyrolysis combined with on-line methylation
H. Ohtani, S. Ueda, Y. Tsukahara (Nagoya, Japan), C. Watanabe (Koriyama, Japan) and S.
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Polymer degradation modified by blending with polymers chosen on the basis of their
@-factors
P. Gardner, R. Lehrie and D. Turner (Birmingham, UK) ...............0.00.0. e0e0u e e 11
Polyaromatization in common synthetic polymers at elevated temperatures
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Electrothermal vaporization and pyrolysis of materials for environmental analysis
A. Golloch, M. Haveresch-Kock (Duisburg, Germany) and W.G. Fischer (Bonn, Germany) 37
Assessment of Scotch whisky quality by pyrolysis—mass spectrometry and the subsequent
correlation of quality with the oak wood cask
K.J.G. Reid, J.S. Swan (Edinburgh, UK) and C.S. Gutteridge (Reading, UK)............. 49
Experimental polysaccharide chars and their ‘‘fingerprints’’ in charred archaeological food
residues
|. Pastorova, T.F.M. Oudemans and J.J. Boon (Amsterdam, The Netherlands) .......... 63
Application of pyrolysis—gas chromatography and pyrolysis—gas chromatography/mass spec-
trometry to the unmasking of amber forgeries
A.M. Shedrinsky (Brooklyn, NY, USA), D.A. Grimaldi (New York, NY, USA), J.J. Boon
(Amsterdam, The Netherlands) and N.S. Baer (New York, NY, USA) ................... 77
Pyrolysis in Geochemistry, Biological Science, Tobacco Research
Analytical pyrolysis of humic substances and soils: geochemical, agricultural and ecological
consequences
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Dynamics of soil organic matter studied by pyrolysis—field ionization mass spectrometry
P. Leinweber (Vechta, Germany) and H.-R. Schulten (Wiesbaden, Germany)............ 123
The effect of various chemical treatments on the pyrolytic pattern of peat humic acid
G. Almendros (Madrid, Spain), F. Martin, F.J. Gonzalez-Vila and J.C. del Rio (Seville,
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Structural characterization of lignin polymers by temperature-resolved in-source pyrolysis—
mass spectrometry and Curie-point pyrolysis—gas chromatography/mass spectrometry
E.R.E. van der Hage, M.M. Mulder and J.J. Boon (Amsterdam, The Netherlands)....... 149
The effect of cations on the thermal decomposition of lignins
E. Jakab (Budapest, Hungary), O. Faix (Hamburg, Germany), F. Till and T. Székely
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Nitrobenzene oxidation vs. pyrolysis—gas chromatography/mass spectrometry as a means to
determine lignin composition
J.B. Reeves Ill (Beltsville, MD, USA) and G.C. Galletti (Gallina, Italy).................. 195
Quantification of lignin and carbohydrates in kraft pulps using analytical pyrolysis and
multivariate data analysis
M. Kleen, G. Lindblad and S. Backa (Stockholm, Sweden).....................200005. 209
Flash pyrolysis of coal sub-structures. A mechanistic and kinetic evaluation
J.V. Christiansen, A. Feldthus, H. Egsgaard, P. Bo and L. Carlsen (Roskilde, Denmark) . 229
Studies of the yield of sulphur from a coal sample by pyrolysis—gas chromatography
P. Almén, |. Ericsson and P. Selsbo (Lund, Sweden)..........0.c. c.c e.ce. e.e.e 0ee e 243
Cell wall development in maize somatic embryos studied by pyrolysis—mass spectrometry
M.M. Mulder (Amsterdam, The Netherlands) and A.M.C. Emons (Wageningen, The Nether-
CREE ERE CS ee a ee ee eee ee eee ee ere 255
The application of pyrolysis—mass spectrometry to microbial ecology: rapid characterisation
of bacteria isolated from an estuarine environment
R.J. Heyler, S.J. Bale and R.C.W. Berkeley (Bristol, UK).............. 0.6.00... cece eee 265
Degradation kinetics of tobacco — survey by fast thermogravimetry analysis
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Technical Pyrolysis
Pyrolysis of ‘‘Fusen”’
O. Kock, W. Kaminsky and H. Sinn (Hamburg, Germany)................0..00c0 e0eu 5e e 285
Fluid bed pyroiysis of anhydride-hardened epoxy resins and polyether—polyurethane by the
Hamburg process
N. Grittner, W. Kaminsky and G. Obst (Hamburg, Germany) .................0.00ee0u 293
The VEBA OEL Technologie pyrolysis
HP. Wenning (GelsenKITGNeN, GOTMAMY).... 2. ccc ccc ccc ccccccccvcecesesccvssesecece 301
Preparation of cyanuric and isocyanic acids in a fluidized bed reactor
V.V. Dragalov, S.V. Karachinsky, O.Y. Peshkova and V.P. Kirpichev (Moscow, Russian
el oe a ee ek eee eed CCADEAAS DEAS E5000 065 KOO E8 06-6 311
Temperature-programmed pyrolysis—mass spectrometry (TPP-—MS) and pyrolysis—gas
chromatography/mass spectrometry (Py—GC/MS) — practical applications to industrial
problems
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Polycyclic aromatic hydrocarbons in polystyrene derived pyrolysis oil
P.T. Williams, P.A. Horne and D.T. Taylor (Leeds, UK) ........0..0. ..ee.e0 .ee e 325
Pyrolysis for Biomass Conversion
Analytical pyrolysis and semicontinuous catalytic hydropyrolysis of Organocell lignin
D. Meier, J. Berns, C. Grunwald and O. Faix (Hamburg, Germany).................... 335
Characterisation of rosin-based commercial resins by pyrolysis— and simultaneous pyrolysis
methylation—gas chromatography/mass spectrometry techniques
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Mechanisms and Kinetics of Pyrolysis Reactions
Mechanistic aspects of ionic reactions in flames
H. Egsgaard and L. Carlsen (Roskilde, Denmark)......0.... .ce.ce .ce.ce. e.e e.ee .ee s 361
Pyrolysis mechanisms of O-(2-hydroxyethyl)celluloses
P.W. Arisz and J.J. Boon (Amsterdam, The Netherlands) ................0.c.c0c 0uu0e e 371
A three-dimensional model for determination of kinetic data from the pyrolysis of beech wood
F. Bonnefoy, P. Gilot and G. Prado (Mulhouse, France) ..............00.0 c.e.e u.u0ee s 387
Modelling of the decomposition of methane at 1273 K in a plug flow reactor at low conversion
O. Olsvik (Trondheim, Norway) and F. Billaud (Nancy, France)........................
Effect of cross-linking on the pyrolysis of diphenylalkanes
P.F. Britt, A.C. Buchanan Ill, E.A. Malcolm and C.A. Biggs (Oak Ridge, TN, USA)
Information for Authors
Author Index
Subject Index