IS 1447-3: Petroleum and its products - Methods of sampling, Part 3: Method of Sampling of Semi-solid and soild petroleum products

12 Pages·1992·1.2 MB·English

by  Bureau of Indian Standards

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timely dissemination of this information in an accurate manner to the public.
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“The Right to Information, The Right to Live” “Step Out From the Old to the New”
IS 1447-3 (1992): Petroleum and its products - Methods of
sampling, Part 3: Method of Sampling of Semi-solid and
soild petroleum products [PCD 1: Methods of Measurement and
Test for Petroleum, Petroleum Products and Lubricants]
“!ान $ एक न’ भारत का +नम-ण”
Satyanarayan Gangaram Pitroda
““IInnvveenntt aa NNeeww IInnddiiaa UUssiinngg KKnnoowwlleeddggee””
“!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता हहहहै””ै”
Bhartṛhari—Nītiśatakam
“Knowledge is such a treasure which cannot be stolen”

,, ~.._._.

Indian Standard
PETROLEUMANDITSPRODUCTS-
METHODSOF SAMPLING
PART 3 METHOD OF SAMPLING OF SEMI-SOLID AND SOLID
PETROLEUM PRODUCTS
First RevWon )
(
UDC 66561.7: 620.113

@ BIS 1992
BUREAU OF INDIAN STANDARDS
MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG
NEW DELHI 110002
July 2991 Price Group 3
sdohteM fo tseT rof ,muelorteP muelorteP stcudorP and stnacirbuL lanoitceS ,eettimmoC PCD 1
FOREWORD
sihT naidnI dradnatS ( traP 3 ) ( tsriF noisiveR ) was detpoda yb eht uaeruB fo naidnI Standards, retfa
eht tfard dezilanif yb eht sdohteM fo, tseT rof ,muelorteP mulorteP stcudorP and stnacirbuL lanoitceS
eettimmoC had neeb devorppa yb eht ,muelorteP laoC and detaleR stcudorP noisiviD .licnuoC
gnilpmaS fo muelortep and its stcudorp era nekat rof eno ro erom fo eht gniwollof :sesoprup
)a roF gniruces evitatneserper seititnauq morf a trap ro morf eht elohw fo a ytitnauq fo lairetam
deriuqer rof lausiv ro yrotarobal noitanimaxe ro rof noitavreserp rof .sdrocer noitanimaxE yam
eb deriuqer ot eb edam rof gninimreted lacisyhp and lacimehc scitsiretcarahc ni redro ot
:erusne
)i ehT egareva ytilauq fo eht elohw ,lairetam and
)ii ehT tnetxe fo noitairav fo seitilauq ni tnereffid snoitrop fo eht elohw .slairetam
)b roF gninimreted eht ytisned and erutarepmet fo eht lairetam rof eht esoprup fo gnitaluclac
eht mass fo a nwonk emulov fo diuqil ro eht emulov fo nwonk mass.
tI deen ton eb dezisahpme that eht tsom luferac krow ni eht yrotarobal ro yna ytitnauq tnemerusaem
yam eb deredner sselesu fi eht samples, nopu hcihw hcus krow is desab era ton ylurt .evitatneserper
nI redro ot tnemelpmi eht deliated snoisivorp nevig ni this sampling dluohs evah eht yrassecen
ecneirepxe and skill. At all semit suolupurcs noitnetta shall eb nevig ot .liated ehT sdohtem derevoc

ni this standard shall eb detnemelppus yb ,tnemegduj skill and .ecneirepxe
nI gnitroper eht stluser fo a tset ro sisylana edam ni ecnadrocca htiw standard, fi eht lanif ,eulav
devresbo ro ,detaluclac is ot eb dednuor ,ffo ti shall eb enod ni ecnadrocca htiw SI 2 : 1960 seluR‘ rof
gnidnuor ffo laciremun seulav ( revised )‘.
IS 1417 ( Part 3 ) : 1992
Indian Standard
PETROLEUMANDITSPRODUCTS-
METHODSOF SAMPLING
PART 3 METHOD OF SAMPLING OF SEMI-SOLID AND SOLID
PETROLEUM PRODUCTS
First Revision
( )
I SCOPE 2.4 Cleaning Procedures
sihT dradnats sebircserp sdohtem rofgniniatbo llA elpmas sreniatnoc llahs eb yletulosbanaelc
evitatneserper selpmas fo dilos-imes dna dilos and free of water, dirt, lint, washing
muelortep dna sti stcudorp rof esoprup fotset ,sdnuopmoc ahthpan ro rehto stnevlos tsur ro
ro.noitanimaxe oil. Before using the container, rinse it with
petroleum hydrocarbon solvent or naphtha of
2 REFERENCES similar volatility. Dry either by passing a
tnuoma fo naelc mraw ria hguorht ehtreniatnoc
The Indian Standard 1s 436 ( Part 2 ) : 1965 ro yb gnicalp ti ni a toh eerf-tsud tenibac ta
sdohteM‘ fo gnilpmas fo laoc dna ekoc traP 2 : C°04 ro .rehgih nehW ,yrd reppots ro paceht
gnilpmaS fo ’ekoc smrof eht yrassecentcnujda reniatnoc .yletaidemmi
ot siht.dradnats
3.4 Sampling Apparatus
3 TERMINOLOGY Sampling apparatus is described in detail in
hcae fo eht cificeps gnilpmas .erudecorp-lpmaS
roF eht esoprup fo siht ,dradnats ehtgniwollof
gni sutarappa llahs eb ,naelc yrd dna eerf folla
snoitinifed llahs.ylppa
secnatsbus that thgim contaminate the
1.3 Boring Sample materials.
A elpmas deniatbo yb gnitcelloc eht spihcedam 5 SNOITUACERP DNASNOITCURTSNI
,yb gnirob seloh htiw a pihs regua morf potot
mottob fo eht lairetam deniatnoc ni a ,lerrab 5.1 It is not possible to give directions for
,esac gab ro.ekac sampling, explicit enough to cover all cases.
yehT llahs eb detnemelppus yb ,tnemegdujlliks
2.3 braGelpmaS
dna gnilpmas ecneirepxe ylralucitrap ni drager

ot eht epyt fo selpmas ot eb .nekat emertxEerac
A elpmas deniatbo yb gnitcelloc esool sdilosni

and good judgement are necessary to erusne
lauqe seititnauq morf hcae trap ro egakcapro
a shipment and in sufficient amount to be selpmas hcihw tneserper lareneg retcarahcdna
egareva noitidnoc fo eht.lairetam
citsiretcarahc fo lla sezis dna.stnenopmoc
5.2 In addition to these general precuations,
3.3 esaerG elpmaS
there are special precautions which shall be
A elpmas deniatbo yb gnipoocs ro gnippid a devresbo ni gnilpmas rof niatrec .stset emoSfo
ytitnauq fo tfos ro diuqil-imes ,lairetam hcussa these are covered in this standard, while the
esaerg morf a egakcap ni hcus a rennamtaht srehto era nevig ni eht tnaveler sdohtem fo.tset
the material on the scoop or dipper is
evitatneserper fo eht lairetam ni eht.egakcap 3.5 A elpmas llahs ton edulcni lairetamrehto
than that to be sampled and shall not be
4 APPARATUS ,deretla rof ,elpmaxe yb noitaropave foelitalov
stneutitsnoc ro yb noitadixo ni eht ssecorp fo
4.1 Sample Containers ,gnilpmas gnirots ro .noitaropsnart
Sample containers shall be of glass, plastic
5.4 Samples shall be taken by, or under the
bottles or metal covered bottles or cans
etaidem mnioisivrepus fo a nosrep fo,tnemegduj
gnidneped no eht lairetam ot eb.deldnah The
lliks dna ecneirepxe ni.gnilpmas
reniatnoc llahs eb ediw dehtuom htiw wolskcen
rof ysae gnillif dna .gnitnaced ehT ezis fohcus 5.5 The sampling apparatus and sample
sreniatnoc lliw yrav gnidneped no ehtesoprup containers shall be dry and free from any
rof hcihw gnilpmas si gnieb.enod gnitanimatnoc .ecnatsbus
1
IS 1447 ( Part 3 ) : 1992
5.6 gniruD sampling ,snoitarepo eht lairetam eht yrotarobal esiwrehto enibmoc eht eerht sets
gnieb delpmas shall eb detcetorp as raf as fo sgnirob otni eno .elpmas fI noisivid-bus fo
elbissop morf eht stceffe fo wind and rehtaew eht sgnirob is ,derised llihc ezirevlup ( fi
and eht elpmas sreniatnoc shall eb desolc yrassecen ,) ,xim and retrauq eht sgnirob litnu
yletaidemmi retfa eht elpmas has neeb .nekat decuder ot derised .tnuoma
5.7 ehT rotarepo degagne ni sampling shall evah
6.2
naelc hands, eerf morf yna lairetam ( unless ti Garb Sampling
eb eht lairetam gnieb delpmas .) naelC sevolg
yam eb ,nrow tub ylno nehw laitnesse ot tcetorp 6.2.1 Application
eht rotarepo morf htlaeh ro rehto .sdrazah ehT brag sampling erudecorp is elbacilppa rof
sampling all ypmul sdilos ni bins, ,sreknub
5.8
Labelling Sample Container
thgierf ,srac ,slerrab bags, sexob and .sroyevnoc
lebaL eht reniatnoc yletaidemmi retfa a elpmas tI is ylralucitrap elbacilppa rof eht noitcelloc fo
is .deniatbo edulcnI eht gniwollof :noitamrofni neerg muelortep ekoc samples morf daorliar
srac and rof eht noitaraperp fo hcus samples
)a etaD and ;emit
rof yrotarobal .sisylana
)b emaN fo eht ;elpmas
)c emaN ro rebmun and renwo fo eht lessev 6.2.2 Place of Sampling
ro ;reniatnoc
muelorteP ekoc yam eb delpmas elihw gnieb
)d dnarB and edarg fo ;lairetam and
dedaol otni daorlia.t srac morf selip ro retfa
)e ecnerefeR ro noitacifitnedi rebmun and gnieb dedaol otni daorliar srac morf gnikoc
rehto noitamrofni yrassecen ot eb .nevig drums.
6
SAMPLING PROCEDURE 6.2.3
Apparatus
~6.1 Boring Sampling
enelyhteylop pail fo
6.2.3.1 Sample container, a
6.1.1 Application yletamixorppa 9.5 1 .yticapac
ehT gnirob sampling erudecorp is elbacilppa rof
6.2.3.2 stainless leets ro .muinimula
sampling sexaw and tfos sdilos ni ,slerrab ,sesac SCOC~J,
bags ro sekac nehw yeht tonnac eb detlem and
6.2.4
delpmas as liquids. Procedure
6.1.2 Apparatus 6.2.4.1 Sanzpling
6.1.2.1 Ship auger ypmuL sdilos cra yllausu suonegoreteh and
ship regua 19 mm ni retemaid ralimis ot erofereht era tluciffid ot elpmas .yletarucca tI is
Use a
that nwohs ni .giF 1 and fo tneiciffus htgnei ot elbareferp ot ekat samples gnirud eht gnidaolnu
pass hguorht eht lairetam ot eb .delpmas fo skcurt ro gnirud transit fo eht lairetam yb

.sroyevnoc morF lairetam ni transit, niatbo
6.1.2.2 Sample container rebmun f;c snoitrop at tneuqerf and raluger
,naelc ediw htuom latem ,sreniatnoc glass slavretni a:ld enibmoc .meht
Use
jars htiw .srevoc
6.2.4.2 nehW sampling morf ,snogaw esu eno fo
6.1.3
Procedure eht gniwollof :serudecorp
evomeR eht sdaeh ro srevoc fo slerrab and
.sesac nepO bags and wrappings fo .sekac )a Being loaded from a pile - ekaT 3 lluf
evomeR yna ,trid ,skcits gnirts ro rehto ngierof cpoocs fo elpmas at hcae fo eht evif
secnatsbus morf eht secafrus fo eht .lairetam sampling stniop nwohs ni .giF 2 and
eroB eerht tset seloh hguorht eht ydob fo tisoped ni eht enelyhteylop pail. revoC
eht lairetam - eno at eht ,ertnec eht rehto owt eht elpmas and reviled ot eht .yrotarobal
yaw-flah neewteb eht ertnec and egde fo hcaE sampling tniop shall eb detacol
egakcap no thgir and tfel sides .ylevitcepser fI tnatsidiuqe morf eht sides fo eht :daorliar
yna ngierof rettam is devomer morf eht roiretni .rac
fo, eht lairetam gnirud gnirob noitarepo edulcni
ti as trap fo eht .sgnirob tuP eht eerht sets fo )b Wagons ofrer ti’lxc’t loading from coki/!g
sgnirob ni laudividni elpmas ,sreniatnoc lebal drums - At yna evif fo eht sampling
and reviled meht ot eht .yrotarobal stniop nwohs ni .giF 3 ekat a lluf poocs fo
ekoc morf tuoba 0.3 m woleb eht ecafrus
6.1.4
Laboratory Inspection and tisoped ti ni eht enelyhteylop pail.
fI ereht era yna elbisiv secnereffid ni eht revoC eht elpmas and reviled ot eht
samples, enimaxe and tset hcae tes fo gnirob at .yrotsrobal
IS 1447( Part 3 ) : 1992
FIG. 1 SHIP AUGER
.GIF 2 NOITACOL FO GNILPMAS STNIOP TA TNEREFFID LEVELSO F CAR
k-- L = LENGTH OF CAR d
,w
i-q.._.__. 10 x+) (= L > c 6 ._
I 0 l 0 t L
w
6
.GIF 3 DESOPXE ECAFRUS FO
LOCATION OF SAMPLING POINTS FROM CAR
nehW sampling morf ,sroyevnoc ekat eht gniretrauq .noitarepo nI this ,rennam eht
~6.2.4.3
eno poocs rof hcae 8 ot 10 snot fo ekoc elpmas lliw yllanif eb decuder ot a ,evntatneserper
.detropsnart esehT samples yam eb deidnah elbatius ezis rof yrotarobal .sesoprup lebaL and
,yletarapes ro detisopmoc retfa all samples reviled eht elpmas ot eht yrotarobal ni elbatius

gnitneserper eht tol evah neeb .nekat .reniatnoc
6.2.4.4 nehW sampling morf bags, ,slerrab ro 6.3
Grease Sampling
,sexob niatbo snoitrop morf a rebmun fo
segakcap detceles at modnar as nwohs ni 6.3.1 Application
elbaT 1 ro ni ecnadrocca htiw eht tnemeerga
sihT dohtem srevoc secitcarp rof gniniatbo
uccwteb eht resahcrup and eht .reilppus
samples evitatneserper fo noitcudorp stol ro
6.2.4.5 stnempihs fo gnitacirbul ,sesaerg ro fo tfos
Quartering
sexaw ro tfos snemutib ralimis ot esaerg ni
ylluferaC xim eht elpmas and ecuder ti ni ezis
.ycnetsisnoc ehT erudecorp is ylirassecen etiuq
ot a tneinevnoc yrotarobal elpmas yb eht
lareneg ot revoc eht ediw yteirav fo snoitidnoc
gniretrauq erudeccrp as nevig ni SI 436
deretnuocne and yam eriuqer noitacifidom ot
( traP 2 ) : 1965. mrofreP eht gniretrauq -arepo
teem laudividni .noitacificeps
noit ho a ,drah naelc ,ecafrus eerf morf ,skcarc
and detcetorp morf ,niar ,wons wind and sun.
6.3.2
Inspection
diovA noitanimatnoc htiw ,srednic sand, spihc
morf eht ,roolf ro yna rehto .lairetam tcetorP fI eht lairetam is a gnitacirbul esaerg and
eht elpmas morf ssol ro gain fo erutsiom ro noitcepsni is edam at eht gnirutcafunam plant,
dust. xiM and daerps eht elpmas ni a ralucric ekat samples morf eht dehsinif shipping
,reyal and edivid ti otni quadrants ot mrof a sreniatnoc fo hcae noitcudorp hctab ro .tol
evitatneserper decuder .elpmas fI this elpmas is reveN ekat esaerg samples yltcerid morf esaerg
llits rof yrotarobal ,sesoprup taeper ,elttek gnilooc pans, tanks, ro gnissecorp
too large
3
BS 1447 ( Part 3 ) : 1992
.tnempiuqe oD ton elpmas eht esaerg litnu ti 6.3.3 Sample Size
has delooc ot erutarepmet ton erom than C”3*8
evoba that fo eht ria gnidnuorrus eht sreniatnoc Select sreniatnoc at modnar morf hcae tol ro
and litnu ti has neeb ni eht dehsin6 sreniatnoc tnempihs ot evig eht derised ytitnauq deificeps
rof at tsael 12 h. nehW eht sreniatnoc rof a ni elbaT 2.
noitcudorp hctab fo esaerg era fo tnereffid ,sezis
taert eht esaerg ni hcae ezis fo reniatnoc as a 6.3.4
Procedure
etarapes .tol nehW noitcepsni is edam at eht
ecalp fo ,yreviled niatbo a elpmas morf hcae
tnempihs fi a tnempihs stsisnoc fo sreniatnoc 6.3.4.1 Inspection
morf erom than eno noitcudorp hctab ( tol
enimaxE eht denepo sreniatnoc ot enimreted
srebmun ,) elpmas hcae hcus hctab .yletarapes
rehtehw eht esaerg tseraen eht retuo secafrus fo
eht reniatnoc htiw that ni eht ,ertnec at tsael
Table 1 Minimum Number of Packages to be 152 mm woleb eht pot ,ecafrus rof erutxet and
Selected for Sampling .ycnetsisnoc nehW erom than eno reniatnoc fo
( Clause 6.2.4.4 ) a tol ro tnempihs is ,denepo osla erapmoc eht
esaerg ni eht evitcepser .sreniatnoc
Num!;aoLoqackages Number of Packages
to be Sampled 6.3.4.2 Sampling
, ~ )2(
(1)
fI on dekram ecnereffid ni eht esaerg is ,dnuof
all
1to 3 ekat eno noitrop morf eht yletamixorppa ertnec
4 to 64 4 and at tneiciffus ytitnauq ot edivorp a
etisopmoc elpmas fo eht derised ytitnauq ( .ees
65 to 125 5 elbaT 2 .) Withdraw snoitrop htiw a naelc
126 to 216 6 ,poocs egral noops ro spatula and ecalp meht ni
a naelc .reniatnoc yreV ,tfos diulf-imes sesaerg
217 to 343 7 yam eb delpmas yb gnippid htiw a 0.4 kg nac
344 to 512 8 ro elbatius .reppid fI yna dekram ecnereffid ni
eht ,esaerg owt etarepes samples fo tuoba
513 to 729 9
54-O kg hcae eno morf eht pot ecafrus tnecajda
730 to 1 000 10 ot eht wall, and eht rehto morf eht ertnec fo
1001 to 1 331 11 dekram noitairav era deton neewteb tnereffid
sreniatnoc fo a tol ro ,tnempihs ekat etarapes
1 332 to 1 728 12 samples fo tuoba 0.45 kg morf hcae .reniatnoc
nehW erom than eno elpmas fo ?t‘ hctab ro
1 729 to 2 197 13
tnempihs is nekat esuaceb fo kcal fo ,ytimrofinu
2 198 to 2 744 14 dnes meht ot eht yrotarobal as etrapes samples.
2 745 to 3 375 15

3 376 to 4 096 16 6.3.4.3 Handling Samples

4 097 to 4.913 17 fI erom than eno noitrop is deriuqer ot tneserper
4 914 to 5 832 18 a tol ro tnempihs fo esaerg retfos than 175
,noitartenep eraperp a etisopmoc elpmas yb
5 833 to 6 859 19
gnixim lauqe snoitrop .ylhguoroht esU a egral
6 860 to over 20 noops ro spatula ni a naelc .reniatnoc diovA
suorogiv gnixim ro gnikrow fo ria otni eht
6.3.2.1 fI eht lairetam gnieb detcepsni is fo .esaerg As esaerg samples emoceb yllaitrap
ekil-esaerg ,ycnetsisnoc tub is ton yllautca a ’dekrow‘ ni gnieb devomer morf ,sreniatnoc eht
gnitacirbul ,esaerg tub emos erutxim fo yvaeh erudecorp is ton elbatius rof gniniatbo samples
snobracordyh hcus as enillatsyrc-orcim sexaw ro fo esaerg retfos than 175 noitartenep no hcihw
tfos ,snemutib ti lliw eb elbissimrep ot ekat ’dekrownu‘ noitartenep is ot eb .denimreted roF
samples morf pans, tanks, ro rehto gnissecorp esaerg gnivah a noitartenep less than 175, tuc
,tnempiuqe as llew as morf sreniatnoc fo eht samples morf eht reniatnoc htiw a efink ni eht
dehsinif .tcudorp ehT esaerg sampling dohtem mrof fo skcolb tuoba 152 x 152 x 51 .mm fI
shall eb elbacilppa ot ,hcus skcots ylno fi rof ,deriuqer ekam dekrownu noitartenep stset no
emos nosaer ti is ton elbissop ot ylppa taeh and skcolb as ,derucorp and rehto noitcepsni stset
trevnoc eht lairetam otni a eurt .diuqil no esaerg tuc morf eht .skcolb
IS 1447 ( Part 3 ) : 1992
Table 2 Size of Grease Samples
( Clause 6.3.3 )
Container Lot or Shipment Minimum Sample
(1) (2) (31
sebuT ro ,segakcap ssel naht 1 kg llA hguonE stinu rof a 1 kg elpmas
1 kg snac llA eerhT snac
5 ro 10 kg snac llA enO nac
regraL naht 10 kg sseL naht 10 000 kg 1 ot 2 kg morf one ro erom
sreniatnoc
regraL naht 10 kg 10 000 ot 50 000 kg 1 ot 3 kg morf owt ro erom
sreniatnoc
regraL naht 10 kg eroM naht 50 000 kg 1 ot 3 kg morf eerht ro erom
sreniatnoc

5