ELECTRICAL PULSE ANNEALING IMPROVES SOFT MAGNETIC PROPERTIES OF NANOMETER ...

348 Pages·2014·13.24 MB·English

Ministry of Education and Sience of the Russian Federation
Federal State Educational Establishment of Higer Professional Education
Siberian State Industrial University
Advanced Materials Institute of Tsinghua University
Shanghai Jiao Tong University

External fields processing and treatment technology and
preparation of nanostructure of metals and alloys

Book of the International workshop articles

Russia-China
International workshop
1-7 October, 2014

Novokuznetsk
2014

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UDK 669.419:621.778:539.4

BBK 34.232.4:34.5,3:34.206.22
E 43
Reviewers
Professor, Sc. D. (Engineering) Muraviov V.V.
Professor, Sc. D. (Phys.-math.) Danilov V.I.

External Fields processing and treatment technology and preparation of
nanostructure of metals and alloys: Book of the International seminar articles, 1
– 7 October 2014/ Ed. by V. Gromov; Siberian State Industrial University –
Novokuznetsk: Publishing Center SibSIU, 2014. – 348 p.
ISBN 978-5-7806-0399-3
The repots made at the Russian-Chinese International seminar are brought
in this edition.The problems of the external energy fields action on the structure,
phase composition, defect substructure of different metals and alloys during
deformation are discussed.
The book of articles is intended for the material science and metallurgy
spesialists and can be usefull for the post graduate student of corresponding
specialist.

Dedicated to the 60th anniversary of professor G. Tang

This workshop was supported by Russian Foundation for Basic Research
(project No 13-02-12009 ofi_m), Government state No 2708GS.

ISBN 978-5-7806-0399-3 Siberian State Industrial University, 2014

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Curriculum Vitae

Name: Guoyi TANG Sex: Male
Place of birth: Heilongjiang Province, P. R. China
Citizenship: Chinese Present position: Professor, Executive director
Address: Advanced Materials Institute of Graduate School at Shenzhne,
Tsinghua University.
Building J, 204, Tsinghua Campus, The University Town, Shenzhen, 518055,
China
Tel and Fax: [phone](O), 86-13530478111(Mobile)
E-mail: [email protected]
Education Background:
1986-1990 PhD Candidate: The Central Iron and Steel Research Institute,
Beijing, P.R.China. (Doctoral Degree)
1983-1986 Post-graduate student: Dept. of Materials Science, Northeast Heave-
Machinery Institute, P.R.China. (Master’s Degree)
1978-1982 undergraduate student: Dept. of Materials Science, Northeastern
University, P.R.China. (Bachelor’s Degree)
Experience :
Feb.2003-Present: Professor, Ph.D candidate supervisor, executive director,
Advanced Materials Institute of Graduate School at Shenzhen, Tsinghua
University.
Jan.2009-Mar. 2009, Visiting Professor, Dept. of Aerospace and Mechanical
Engineering, Nanyang Technology University, Singapore.

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Nov.2005-Feb. 2006, Visiting Professor, Dept. of Intelligent and Mechanical
Engineering, Akita University, Japan.
Nov.2001 – Feb.2003: Visiting Professor, Dept. of Materials Science and
Engineering, North Carolina State University, USA.
Major research fields: Nanomaterials, thin film materials, electron materials,
Elelctroplastic processing for metal.
Dec. 2000 – Nov. 2001, Visiting Professor, Mechanical Engineering
Department, University of Alaska Fairbanks, USA.
Graduate course taught: Arctic Materials Engineering.
Major research fields: Arctic materials, Nanomaterials.
Projects Head: Epsco project ($20,000),
Project Title: Study on dynamic damage mechanism for a composite of fiber
reinforcement concrete under arctic environmental service, supported by Alaska
Science Foundation (Approval number: SG01-12), USA.
Oct. 1999 - Dec. 2000: Guest Professor, Institute For Theoretical and Applied
Physics, Stuttgart University, Germany, and Max-Planck Institute for
Metallforschung, Stuttgart, Germany.
Major research field: Nanomaterials.
June 1996 - Oct. 1999: Professor, Ph. D candidate supervisors, Deputy Director
of Advanced Material Research Key Lab of Education Ministry in China, Head
of Nanostructure Research Faculty, Head of Electron Microscope Laboratory of
Materials Science & Engineering School, Tsinghua University, Beijing,
P.R.China.
Undergraduate course taught: Electron Microscopy.
Graduate courses taught: Mechanical Metallurgy, Failure Analysis.
Major research fields: electron microscopy; nanomaterials; advanced metal
materials (super-strength steels, New type petroleum engineering steels, and so
on); surface super hard and wear resistance polymer materials; electroplastic
processing and application in metal materials; composite materials;
electrochemical processing and surface treatment of materials; new

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manufacturing technology of nanomaterials (electrochemical manufacturing
technology of nanomaterials and failure analysis (including mineral equipments,
power station components, Bridges, airplanes, etc.).
Oct.1994 – Apr.1996: Research Scientist, Korea Atomic Energy Research
Institute, Taejon, South Korea.
Research work: materials surface modification and microstructure analysis
(including Zircaloy-4, Polymer, and magnetic film, metal, etc).
June 1992 – Oct. 1994: Associate professor, Dept. of Mechanical Engineering,
Tsinghua University, Beijing, P.R. China.
Research work: failure analysis; dynamic fracture mechanism and its application
in engineering; fracture mechanism of welding structure steel; extension the life
of old steel bridges; microalloyed steel and thermo-mechanical treatment.
June 1990 - June 1992: Postdoctoral research fellow, Dept. of Mechanical
Engineering, Tsinghua University. Beijing, P.R. China. Advisor: Prof. Qigong
Cai and Prof. Jiluan Pan (both are members of the Chinese Academy of
Sciences).
Research works: Dynamic fracture mechanism and its application in
engineering; fracture mechanism of welding structure steel.
Oct. 1986 - June 1990: Ph.D. candidate, The Center Iron and Steel Research
Institute, Beijing, P. R. China. Supervisor Prof. Qigong Cai and Prof. Jing Zhu
(both are members of the Chinese Academy of Sciences). Thesis title: The study
of physical metallurgy and fracture mechanism of V-Ti-N microalloyed steel.
Training skills: microscopic analysis (transmission electron microscope,
scanning electron microscope); experimental and analysis techniques of fracture
mechanics; data acquisition and analysis by computer.
Mar. 1986 -Oct. 1986: Lecturer, Dept. of Materials Science, Northeast Heave-
Machinery Institute, P.R. China.
Aug. 1983 - Mar. 1986: Post-graduate student, Dept. of Materials Science, Dept.
of Materials Science, Northeast Heavy-Machinery Institute, P.R. China.

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Aug. 1982 -Aug. 1983: Assistant lecturer, Dept. of Materials Science, Northeast
Heavy-Machinery Institute, P.R. China.
Sep. 1978 - Aug. 1982: Undergraduate student. Dept. of Materials Science and
Engineering, Northeast University, P.R. China.
Nov. 1970 - Aug. 1978: steel production worker, metallographic and electron
microscopy technician, Qiqihar special steel plant in China. Worked on defect
analysis, quality control and failure analysis. Accumulated practical experiences
for steel production.
Honors:
1. National Award for Technological Invention，second- class prize, China
Government, 2010.
2. Science and Technology Advancement Award of The Education Ministry of
China, 1995.
3. Science and Technology Advancement Award of The Education Ministry in
China, 1996.
4. Science and Technology Advancement Award of The Railway Ministry of
China, 1994.
5. Science and Technology Advancement Award of the Metallurgy Ministry of
China, 1993.
6. Outstanding Young Professor Award. Tsinghua University, 1999.
7. Outstanding Student Award of Northeast University in 1979, 1980, 1981.
Major Research Interests:
1. Advanced materials and new processing technology (advanced metal
materials, film materials, nanomaterials, electrical materials, composite
materials).
2. Techniques of microstructure and microanalysis for materials (interface,
boundary, crystal defects, Precipitate phase etc.).
3. Surface modification and its application (metal, polymer, diamond, nano-
particles, multiplayer film, electrochemical plating, high energy electro-pulse
surface treatment).

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4. Electroplastic processing and its application in the metal materials.
5. Phase change materials and its application in storage energy.
6. Fracture mechanism and application in engineering.
7. Failure analysis (metal, ceramics, electronic devices [MOS], composite
materials, semiconductors, etc).
8. Nano-materials and Function materials.
9. Engineering polymer and Bio-degradable polymer composite.
Recent Research Projects (As responsible Supervisor):
1. ‘Fundamental study on the novel phase change materials (PCMs) and its
applications in textiles and building materials’2008DFA51210, an international
collaborative project of the national Ministry of Science and Technology
(MOST), China, 2009-2011.
2. Bio-degradable polymer composite and its applications, 2010-2012,
industrial funded project.
3. ‘Preparation of nano-sized magnesium hydroxide flame retardant and its
application in thermal shrinkable materials’ (2008131), a Shenzhen Nanshan
Science and Technology Bureau funded project in collaboration with
Changyuan Group Ltd, 2009-2011.
4. Environmental-friendly flame retardant and smoke suppression material: its
preparation and characterization, Shenzhen funded project, 2007-2010.
5. Physical nature of structural-phase transformations at electroblasting
alloying of metals and alloys surface. National Science Foundation from NCSF,
2008-2010. (Approval No.50811120046)
6. Mg alloy electroplastic process and application, National Science
Foundation from NCSF, 2006-2008. (Approval No.50571048)
7. Phase change materials and its application in engineering, National Science
Foundation from NCSF, 2006-2008. (Approval No.50572045)
8. Deformation Mg alloy application research, Shenzhen government
foundation, 2005-2007.

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9. Nano- function material and its application, Shenzhen government
foundation.
10. Study on dynamic damage mechanism for a composite of fiber
reinforcement concrete under Arctic environmental service, Supported by
Alaska Science foundation (Approval number: SG01-12), USA. Completed in
2002 (5/1/2001 - 4/30/2002).
11. Seed Grant to Establish Materials Research for the Arctic Region based on a
Scanning Electron Microscope, Supported by Alaska Science foundation (E01-
04), USA. Completed in 2002 (5/1/2001 - 4/30/2002).
12. Nanomaterials and application in Engineering, Continue research (1999-
2002).
13. Advanced steel materials, The National Key Research Projects of China,
(approval number: 973-15). Completed in 1999 (1998 -1999).
14. Superhard-surface and high wear resistant polymers, supported by The
National Nature Science Foundation of China (approval number: 59673003).
Completed in 1999 (1996 -1999).
15. Study of Mechanism and engineering application of electroplasticity,
supported by The National Nature Science Foundation of China (approval
number: 59475056). Completed in 1997 (1994-1997).
16. Electroplastic effects and fatigue property of metals. Supported by the
Education Ministry of China. Completed in 1998 (1996-1998).
17. The study of ion implantation processing for Zircaloy-4 alloy to be used in
nuclear reactor. Supported by Tsinghua University. Completed in 1996
18. The study of ion implantation processing for amorphous magnetic materials.
Supported by Tsinghua University. Completed in 1996.
Representative Patents:
1. Environmental-friendly flame retarding and smoke suppression form stable
phase change materials and its preparation method, Chinese Patent:
CN200910106596.2.
2. A preparation method for nano-sized magnesium hydroxide, Chinese Patent:

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CN101376511.
3. A surface modification method for nano-sized magnesium hydroxide,
Chinese Patent: CN101368009.
4. A multi-functional ultrasonic reactor, Chinese Patent: 200720196712.
5. A method for preparing micro-encapsulated phase change materials, Chinese
Patent: CN200610157343.4.
6. A method for preparing micro-sphere composite containing phase change
materials, Chinese Patent: CN200710124055.3.
7. A rapid method for preparing microcapsules of phase change materials by
UV initiated polymerization, Chinese Patent: 200910106965.8.
8. A electric plastic rolling method for the deformation of Mg alloy board,
strips and wires and its equipments, Chinese Patent: CN200510080495.4.
9. A fast online treatment method for Mg alloy wires and strips by using high
energy electric pulsing technique, Chinese Patent: CN200610061957.2.
10. A high energy electric pulsing treatment method for steel wires and strips,
Chinese Patent: CN200510101148.5.
Representative Papers：
1. Yanbin Jiang, Guoyi Tang, Chanhung Shek, Yaohua Zhu, Zhuohui Xu On
the thermodynamics and kinetics of electropulsing induced dissolution of b-
Mg17Al12 phase in an aged Mg–9Al–1Zn alloy Acta Materialia 57 (2009)
4797–4808 (SCI and EI index，IF=3.92).
2. Sude Ma, Guolin Song, Wei Li, Pengfei Fan, Guoyi Tang. UV irradiation-
initiated MMA polymerization to prepare microcapsules containing phase
change paraffin. Solar Energy Materials & Solar Cells, 2010. 94 (10): 1643-
1647 (SCI index IF=3.858).
3. Guolin Song, Sude Ma, Guoyi Tang, Zhansong Yin, Xiaowei Wang.
Preparation and characterization of flame retardant form-stable phase change
materials composed by EPDM, paraffin and nano magnesium hydroxide.
Energy, 2010, 35, 2179-2183(SCI Index IF=2.952).
4. Guolin Song, Sude Ma, Guoyi Tang, Xiaowei Wang. Ultrasonic-assisted

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synthesis of hydrophobic magnesium hydroxide nanoparticles. Colloids and
Surfaces A: Physicochemical and Engineering Aspects, 2010. 364 (1-3): 99-
104 (SCI index IF=1.988).
5. Guoyi Tang, Zhuohui Xu, et al, Effect of a pulsed magnetic treatment on the
dislocation substructure of a commercial high strength steel. Materials Science
and Engineering A 398 (2005) 108–112 (2005) (SCI and EI index IF=1.901).

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