Conference Proceedings of the Society for Experimental Mechanics Series Alex Arzoumanidis · Meredith Silberstein Alireza Amirkhizi Editors Challenges in Mechanics of Time Dependent Materials, Volume 2 Proceedings of the 2017 Annual Conference on Experimental and Applied Mechanics Conference Proceedings of the Society for Experimental Mechanics Series Series Editor Kristin B. Zimmerman Ph.D. Society for Experimental Mechanics, Inc. Bethel, CT, USA More information about this series at http://www.springer.com/series/8922 Alex Arzoumanidis (cid:129) Meredith Silberstein (cid:129) Alireza Amirkhizi Editors Challenges in Mechanics of Time Dependent Materials, Volume 2 Proceedings of the 2017 Annual Conference on Experimental and Applied Mechanics Editors AlexArzoumanidis MeredithSilberstein Psylotech,Inc DepartmentofMechanicalandAerospaceEngineering Evanston,IL,USA CornellUniversity Ithaca,NY,USA AlirezaAmirkhizi UMassLowellNorthCampus,Perry332 UniversityofMassachusetts Lowell,MA,USA ISSN2191-5644 ISSN2191-5652 (electronic) ConferenceProceedingsoftheSocietyforExperimentalMechanicsSeries ISBN978-3-319-63392-3 ISBN978-3-319-63393-0 (eBook) DOI10.1007/978-3-319-63393-0 LibraryofCongressControlNumber:2015952466 #TheSocietyforExperimentalMechanics,Inc.2018 Thisworkissubjecttocopyright.AllrightsarereservedbythePublisher,whetherthewholeorpartofthematerialisconcerned,specificallytherightsof translation, reprinting, reuse of illustrations, recitation, broadcasting, reproduction on microfilms or in any other physical way, and transmission orinformationstorageandretrieval,electronicadaptation,computersoftware,orbysimilarordissimilarmethodologynowknownorhereafterdeveloped. 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Printedonacid-freepaper ThisSpringerimprintispublishedbySpringerNature TheregisteredcompanyisSpringerInternationalPublishingAG Theregisteredcompanyaddressis:Gewerbestrasse11,6330Cham,Switzerland Preface ChallengesinMechanicsofTime-DependentMaterialsrepresentsoneofninevolumesoftechnicalpaperspresentedatthe SEM 2017 Annual Conference and Exposition on Experimental and Applied Mechanics organized by the Society for Experimental Mechanics and held in Indianapolis, IN, in June 12–15, 2017. The complete proceedings also includes the following volumes: Dynamic Behavior of Materials; Advancement of Optical Methods in Experimental Mechanics; Mechanics of Biological Systems, Materials and other topics in Experimental and Applied Mechanics; Micro- and Nanomechanics;MechanicsofComposite,HybridandMultifunctionalMaterials;Fracture,Fatigue,FailureandDamage Evolution;ResidualStress,Thermomechanics&InfraredImaging,HybridTechniquesandInverseProblems;andMechan- icsofAdditiveandAdvancedManufacturing. Eachcollectionpresentsearlyfindingsfromexperimentalandcomputationalinvestigationsonanimportantareawithin experimentalmechanics,themechanicsoftime-dependentmaterialsbeingoneoftheseareas. Thistrackwasorganizedtoaddressconstitutive,time(orrate)-dependentconstitutive,andfracture/failurebehaviorofa broad range of materials systems, including prominent research in both experimental and applied mechanics. Papers concentratingonbothmodelingandexperimentalaspectsoftime-dependentmaterialsareincluded. Thetrackorganizersthankthepresenters,authors,andsessionchairsfortheirparticipationandcontributiontothistrack. ThesupportandassistancefromtheSEMstaffisalsogreatlyappreciated. Evanston,IL,USA AlexArzoumanidis Ithaca,NY,USA MeredithSilberstein Lowell,MA,USA AlirezaAmirkhizi v Contents 1 ExperimentalCharacterisationoftheMechanicalPropertiesoftheClay-Rock/Concrete InterfacesandTheirEvolutioninTime. . . . . .. . . . . . . .. . . . . . . .. . . . . . . .. . . . . . . .. . . . . . . .. . . . 1 EleniStavropoulou,MatthieuBriffaut,Fre´de´ricDufour,andGuillaumeCamps 2 CoupledAnisothermalChemomechanicalDegradationSolutionsinOneDimension. . . . . . . . . . . . . . . 5 M.Anguiano,H.Gajendran,R.B.Hall,andA.Masud 3 Time-TemperatureAnalysis,DMAandCompressioninPBXs. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11 DarlaGraffThompson,JamieStull,RacciDeluca,andGeoffBrown 4 StatisticalLifeTimePredictionUnderTensionLoadingforUnidirectionalCFRP withThermoplasticsasMatrices. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19 MasayukiNakada,YokoMorisawa,andYasushiMiyano 5 TimeandTemperatureDependenceonTensileStrengthofUnidirectionalCFRP withVariousCarbonFibers. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25 YasushiMiyano,YoshikiKobayashi,andMasayukiNakada 6 TimeTemperatureSuperpositionandPronySeriesCoefficientsofAsphaltRoof ShingleMaterialfromViscoelasticCreepTesting. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 33 SreehariRajan,MichaelA.Sutton,RyanFuerte,andIgorEmri 7 AMixtureTheorywithInteractiveBodyForcesforCompositeInterphases.. . . . . . . . . . . . . . .. . . . . . 39 R.B.Hall 8 MaterialCreepBehaviorwithPredictionofTertiaryCreepFailure byaSphericalMicro-indentationMethod. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 43 DumbiC.OtunyoandBruceS.Kang 9 MechanicalandBiodegradableBehaviorofAZ31MagnesiumAlloy ImmersedinSimulatedBodyFluid. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49 WenxueLin,NingZou,andQizhenZ.Li 10 FailureofLaserWeldedStructuresSubjectedtoMultiaxialLoading: ExperimentalDevelopment. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 57 BonnieR.AntounandKevinConnelly 11 CharacterizationandModelingofPEEKinHistorieswithReverseLoading. . . . . . . . . . . . . . . . . . . . . 65 WenlongLi,GeorgeGazonas,EricN.Brown,PhilipJ.Rae,andMehrdadNegahban 12 ABiomimeticCompositeforSpaceVehicle/HabitatDesign. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 71 AshokKumarGhosh,RamonMartinez,andCarlM.Cady vii viii Contents 13 MolecularDynamicsMotivatedMaxwellElementSpringNonlinearity. . . . . . . . . . . . . . . . . . . . . . . . . 79 G.A.Arzoumanidis,T.J.L.Mustard,M.D.Halls,andStephenChristensen 14 CharacterizationandSimulationofTime-DependentResponseofStructural MaterialsforAeroStructuresandTurbineEngines. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 83 StephanM.Russ,RejiJohn,andCraigP.Przybyla Chapter 1 Experimental Characterisation of the Mechanical Properties of the Clay-Rock/Concrete Interfaces and Their Evolution in Time EleniStavropoulou,MatthieuBriffaut,Fre´de´ricDufour,andGuillaumeCamps Abstract Thedelayedmechanicalbehaviouroftheclay-rock/concreteinterfaceundershearstresshasbeenexperimentally investigated. After a first characterisation of the short-term response of the interface with direct shear tests, long duration sheartestsunderconstantnormalloadhavebeenperformedwithanewexperimentalapparatuswhichwasdevelopedforthis study.Theresponseoftheinterfaceintimeisdiscussed. Keywords Interface•Creep•Sheartest•Clay-rock•Concrete 1.1 Introduction In the context of the underground nuclear waste disposal projects in deep argillaceous geological formations in several countries, Underground Research Laboratories (URL’s) have been developed in order to demonstrate the underground isolation. The French National Radioactive Waste Management Agency (ANDRA) is studying the behaviour of a deep geological radioactive repository in Callovo Oxfordian clay-rock (known as COx) in Bure, France. Such projects require predictionofirreversibledeformationsoveralargetimescale,inordertoassesthedurabilityoftheconfinement. Thesealingoftheundergroundrepositorytunnel,ispartlyensuredbyamechanicalbarriermadeofconcrete,directlyin contactwiththerock.Thus,thedelayedmechanicalbehaviouroftheclay-rock/concreteinterfaceisofalargeinterest.The amplitudeofdelayedstrainsdependsonthematerialandtestconditions.Thestateofstressdeterminesthemodeoffailureof thesampleandthebrittle-ductiletransition[2].Gonze[3]showedthatforhigherdeviatoricstresses,thestrainrateincreases. ZhangandRothfuchs[8]showedthatclay-rockcreepsalreadyunderverylowstressof2MPa,indicatingthatalowercreep limitseemsnottoexistforthisclay-rock.Concerningthedelayedbehaviourofconcrete,manystudieshaveshownthatthe obtainedcreepdeformationdoesn’tincreaseproportionallywiththeincreaseoftheappliedloadinglevels[6,7].Ponsand Torrenti[5]showedthatforappliedchargelowerthan50%ofthecompressivestrengthofconcrete,thedelayedstrainrate decreaseswithtime. Althoughthephysicalpropertiesofmostofthematerialsinvolved(rock,concreteandbentonitemixtures)areextendedly studied,therehavebeenfewstudiesonthebehaviourofthecontactinterfacesbetweenthesematerials.Thescientificgoalof thisworkinvolvestheunderstandingofthecreepmechanismoftheinterfaceoftwomaterialsandmorespecificallywhether the interface itself highlights its own creep mechanism, independently of the creep of both materials in contact. An experimental campaign on the mechanical characterisation of the interface of the underground concrete gallery with the hostrockintimehasbeendevelopedandwillbepresented. E.Stavropoulou(*) UniversityofGrenobleAlpes,CNRS,GrenobleINP(InstituteofEngineeringUniversityofGrenobleAlpes,Grenoble,France), 3SR,F-38000,Grenoble,France AgenceNationalepourlagestiondesDe´chetsRadioactifs(ANDRA),92290Chaˆtenay-Malabry,France e-mail:[email protected] M.Briffaut(*)•F.Dufour UniversityofGrenobleAlpes,CNRS,GrenobleINP(InstituteofEngineeringUniversityofGrenobleAlpes,Grenoble,France), 3SR,F-38000,Grenoble,France G.Camps AgenceNationalepourlagestiondesDe´chetsRadioactifs(ANDRA),92290Chaˆtenay-Malabry,France #TheSocietyforExperimentalMechanics,Inc.2018 1 A.Arzoumanidisetal.(eds.),ChallengesinMechanicsofTimeDependentMaterials,Volume2, ConferenceProceedingsoftheSocietyforExperimentalMechanicsSeries,DOI10.1007/978-3-319-63393-0_1 2 E.Stavropoulouetal. 1.2 Experimental Campaign Theinvestigationofthemechanicalbehaviouroftheclay-rock/concreteinterfaceintime,requiredastudyoftheshort-term response, performing shear tests with the BCR3D apparatus (a 3D shear box for rocks, [4]). This device allows shearing underconstantnormalstressorconstantnormalvolumewiththeapplicationofsymmetricalandoppositedisplacementon thejoint’sactivepart.SamplesofCOx(78mmØ)havebeenmouldedinshearboxeswiththestudiedconcrete,asshownin Fig. 1.1. Short-term shear tests under constant normal volume (with applied normal stress up to 12 MPa) have been performed,inordertocharacterisetheelastoplasticbehaviourofthejoints.TheresultshavebeenanalysedusingtheMohr- Coulombfailurecriterion,allowingtheevaluationoftheresistanceoftheinterfaceinshearing. The characterisation of the mechanical behaviour of the interface in time, required the design of a new experimental device. For the purpose of this work, SInC Box (Shear-Interfaces-Creep Box) has been developed, a sophisticated device whichallowsthestudyofaninterfaceinshearingunderlongdurationload.SInCBoxisbasedontheexistingcreepdevices intractionforintactsamples[1]andintroducesasecondloadingaxis,orthogonaltotheexistingone.Itisdesignedinaway, so that the normal force is centered in the mean plane of the interface and the applied shear force passes the axis of the interface(Fig.1.1(1and2)).Theapplicationofanormalandashearload,isfollowedbythemeasurementoftherelative shearing displacement (Fig. 1.1c), as well as dilatancy/contraction, allowing the demonstration of the failure mode of the interface. 1.3 Test Results Severaltestshavetakenplaceonsamplesofclay-rock/concreteinterface,intemperaturecontrolledenvironment(20(cid:1)C)and underdifferentconstantnormalstress.Theresultsofthreetestsarepresented.Theapplicationofthenormalloadisfollowed bytheapplicationofashearload.Test1wasperformedundernormalstressσn¼6MPaandshearstressτ¼2.7MPawhich wemaintainedconstantthroughouttheentiretest.InTest2,underσn¼8MPa,aninitialshearstressofτ¼1.3MPawas followed by an increase to 2.5 MPa. Finally, Test 3 was performed under normals stress σn ¼ 10 MPa and shear stress τ¼3.8MPa. Fortheanalysisoftheresultsofalong-durationtest,theinstantaneouselastoplasticresponseoftheinterfaceistakeninto account.Figure1.2ashowstheratioτ/τmaxforeachtest,whereτmaxisthecalculatedinstantaneousshearresistanceforthe Fig.1.1 Left:Sampleillustration;(a)3Dconceptofthetwohalfshearboxes,(b)Verticalcutillustrationtheinterfaceofthetwogeomaterials,(c) Illustrationoftheappliedforces(Fnnormalforce,Ftshearforce,tothemeanplaneoftheinterface)andtherelativesheardisplacement(dut)ofthe twohalfshearboxes.Right:SInCBoxzoomedin,illustratingthepositionofthesampleandtheapplicationofthetwoorthogonalloads;(1)normal forcetransducer,(2)shearforcetransducer,(3)samplemouldedinthetwohalf-shearboxes(rotatedby90(cid:1)) 1 ExperimentalCharacterisationoftheMechanicalPropertiesoftheClay-Rock/ConcreteInterfacesandTheir... 3 (*103 ) 1.2 12 10 83% 1 a) P M 8 0.8 m/ m/ µ 6 0.6 e ( 74% c 83% an 4 σ pli σ 0.4 σ m σ σ co 2 54% σ 29% 0.2 0 0 100 200 300 400 500 600 700 800 0 100 200 300 400 500 600 700 800 time (h) time (h) Fig.1.2 (a)Evolutionoftheratioofappliedshearstressovershearstrength,(b)complianceoftheshearresponse givennormalstress.TheevolutionofthemeasuredcomplianceinshearingispresentedinFig.1.2b,wherethecomplianceis calculatedasthedelayedshearstrainovertheappliedshearstress(εxy/τ). Observing the initial evolution of the compliance between the three tests (t ¼ 0 ! t ¼ 100 h), one can notice that the measured compliance increases faster for higher shear strength levels. Although this observation is not obvious for Tests 1 and 3, given the similar levels of applied shear stress (83% and 74%), it is more clear for Test 2. Indeed for a low τ/ τmax¼29%,thecomplianceisverylowandgetsquicklystabilised.Anincreasefrom29%to54%leadstoanincreaseof the rate of compliance, being though lower than the rates of Tests 1 and 3. In all three tests the measured product εxy/τ increasesnonlinearlyintime,withadecreasingrate.Thisresponseindicatestheexistenceofdelayeddeformationswithin theprimaryphase. 1.4 Conclusions/Perspectives ThedelayedbehaviourinshearingoftheCOx/concreteinterfaceshasbeenexperimentallyinvestigated.Thedevelopmentof anewapparatus(SInCBox)allowedmeasurementofthedeformationoftheinterfaceintime,inbothnormalandtangential direction.Fortheappliedstresspathsandthegivendurationofthetests,onlyprimarycreepwasobserved. Thestudyofcreepininterfacesiscomplex,asitinvolvestheevolutionintimeoftwodifferentmaterials.Theobtained delayed response can be the result of the delayed response of each material or of the interface itself independently. The resultsoflongerdurationtestsaregoingtobediscussed. References 1.Fabre,G.,Pellet,F.:Creepandtime-dependentdamageinargillaceousrocks.Int.J.RockMech.Min.Sci.43(6),950–960(2006) 2.Gatelier,N.:ETUDEEXPERIMENTALEETTHEORIQUEDEL’ENDOMMAGEMENTDESROCHESANISOTROPES.Diss.(2001) 3.Gonze,P.:Techniquesdecalculutilise´esenconge´lationdesterrains.Lathermomecaniquedesroches.16,(1988) 4.Hans,J.,Boulon,M.:Anewdeviceforinvestigatingthehydro-mechanicalpropertiesofrockjoints.Int.J.Numer.Anal.MethodsGeomech.27 (6),513–548(2003) 5.Pons, G., J. M. Torrenti. “Retrait et fluage.” La durabilite´ des be´tons: bases scientifiques pour la formulation de be´tons durables dansleur environnement,OllivierJP,VichotA.,Pressesdel’E´coleNationaledesPontsetChausse´es.167–216(2008) 6.Roll,F.:Long-timecreep-recoveryofhighlystressedconcretecylinders.Spec.Publ.9,95–114(1964) 7.Sellier,A.,Buffo-Lacarriere,L.:Towardsasimpleandunifiedmodellingofbasiccreep,shrinkageanddryingcreepofconcrete.Eur.J.Environ. CivilEng.13(10),1161–1182(2009) 8.Zhang,C.,Rothfuchs,T.:Experimentalstudyofthehydro-mechanicalbehaviouroftheCallovo-Oxfordianargillite.Appl.ClaySci.26(1), 325–336(2004)