Appendix I Standard Operating Procedures and Standard Quality

803 Pages·2011·4.12 MB·English

Appendix I

Standard Operating Procedures and Standard Quality Procedures
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U.S. Department of Energy
Oakland Operations Office, Oakland, California

FINAL STANDARD OPERATING PROCEDURES
for the:
Environmental Restoration/Waste Management
Laboratory for Energy-Related Health Research (LEHR)
University of California at Davis, California
Prepared for:
United States Department of Energy
Oakland Operations Office
1301 Clay Street
Oakland, California 95612-5208
Prepared by:
Weiss Associates
5801 Christie Avenue, Suite 600
Emeryville, CA 94608-1827

DOE Oakland Operations Contract DE-AC03-96SF20686
FINAL STANDARD OPERATING PROCEDURES
for the:
Environmental Restoration/Waste Management
Laboratory for Energy-Related Health Research (LEHR)
University of California at Davis, California
Prepared for:
United States Department of Energy
Oakland Operations Office
1301 Clay Street
Oakland, California 95612-5208
Prepared by:
Weiss Associates
5801 Christie Avenue, Suite 600
Emeryville, CA 94608-1827

DOE Oakland Operations Contract DE-AC03-96SF20686
Issued To: ___________________ Date: ______________
Copy No.: ________ (cid:1) Controlled (cid:2) Uncontrolled
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Approvals Page
FINAL STANDARD OPERATING PROCEDURES
for the:
Environmental Restoration/Waste Management
Laboratory for Energy-Related Health Research (LEHR)
University of California at Davis, California
Prepared for:
United States Department of Energy
Oakland Operations Office
1301 Clay Street
Oakland, California 95612-5208
Prepared by:
Weiss Associates
5801 Christie Avenue, Suite 600
Emeryville, CA 94608-1827
October, 2010

Approved by: Date:
Mary Stallard, R.G.
Project Quality Assurance Manager
Weiss Associates

Approved by: Date:
Robert O. Devany, R.G., C.H.G.
Project Manager
Weiss Associates

Approved by: Date:
Michael D. Dresen, R.G., C.H.G.
Program Manager
Weiss Associates
J:\DOE\4000\D3\SQ&OPS\WASOPS\SOP_TOC1299.DOC WEISS ASSOCIATES Project Number: 128-4000
Standard Operating Procedures and Forms Table of Contents
LEHR Environmental Restoration / Waste Management 12/10/99
DOE Contract No. DE-AC03-96SF20686 Page i of vi

TABLE OF CONTENTS
AND LOG OF REVISIONS

STANDARD OPERATING PROCEDURES

SOP No. Title Revision Date of
No. Revision
SOP 1.1 Chain-of-Custody 1 3/99
SOP 2.1 Sample Handling, Packaging and Shipping 2 12/99
SOP 3.1 Surface and Shallow Subsurface Soil Sampling 1 4/02
SOP 3.2 Subsurface Soil Sampling While Drilling 1 4/02
SOP 4.1 Compaction of Fill Material 0 3/98
SOP 5.1 Water Level Measurements in Monitoring Wells 0 3/98
SOP 5.2 Non-aqueous Phase Liquid Measurement in Monitoring 0 3/98
Wells
SOP 6.1 Sampling Equipment and Well Material Decontamination 0 3/98
SOP 6.2 Drilling, Development and Heavy Equipment 0 3/98
Decontamination
SOP 7.1 Surface and Subsurface Geophysics 0 3/98
SOP 8.1 Monitoring Well Installation 0 3/98
SOP 8.2 Monitoring Well Development 0 3/98
SOP 8.3 Bore Hole and Well Abandonment 0 3/98
SOP 9.1 Low Flow Ground Water Sampling with Dedicated Pumps 1 10/10
SOP 10.1 Soil Organic Vapor Sampling 0 3/98
SOP 10.2 Cone Penetration Testing and Hydropunch Ground Water 0 3/98
Sampling
SOP 10.3 Sample Collection, Handling and Data Documentation for 0 6/98
Field Analysis Using Gamma Spectrometer and Beta
Scintillation Dectector
SOP 10.4 Radium-226 Analysis by Gamma Spectrometer 0 7/01
SOP 10.5 Strontium-90 Analysis by Beta Scintillation Sensor 3 7/01
SOP 11.1 Aquifer Testing 0 3/98
SOP 12.1 Soil Stockpiling 0 3/98
SOP 13.2 Ambient Air Monitoring 1 3/99
SOP 14.1 Hollow Stem Auger Drilling 0 3/98
SOP 14.2 Mud Rotary Drilling 0 3/98
SOP 14.3 Air Rotary Drilling 0 3/98
SOP 14.4 Dual Tube Percussion Drilling 0 3/98
SOP 15.1 Lithologic Logging 0 3/98
SOP 17.1 Sample Labeling 0 3/98
SOP 17.2 Sample Numbering 0 3/98
SOP 18.1 Field QC Sampling 0 3/98
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Standard Operating Procedures and Forms Table of Contents
LEHR Environmental Restoration / Waste Management 12/10/99
DOE Contract No. DE-AC03-96SF20686 Page ii of vi

SOP 19.1 On-Site Sample Storage 0 3/98
SOP 20.1 Sample Containers, Preservation, and Holding Times 0 3/98
SOP 21.1 Data Validation 1 10/10
SOP 21.2 Sample Data Management 0 10/10
SOP 23.1 Land Surveying 0 3/98
SOP 24.1 Radiological Areas and Postings[see RPP] 1 3/99
SOP 25.1 Radiological Surveys and Instrumentation [see RPP] 1 3/99
SOP 25.2 Radiological Survey Forms (Update 1) [see RPP] 0 7/98
SOP 29.1 Drum Crusher Operation and Servicing 0 3/98
SOP 30.1 Taskmaster Heavy Duty Solids Disintegrator (Shredder) 0 3/98
Operation and Servicing
SOP 31.1 Lead Characterization, Packaging and Shipping 0 3/98
SOP 32.1 Contamination Control [see RPP] 1 3/99
SOP 34.1 Waste Processing and Packaging 0 7/98
SOP 34.2 Low-Level Radioactive Waste Storage 0 3/99
SOP 34.3 Waste Shipment 2 6/01
SOP 34.4 Clean Waste Handling 0 3/98
SOP 34.5 Waste Tracking System 0 2/99
SOP 35.1 Waste Certification 0 3/98
SOP 35.2 Waste Characterization for Off-Site Shipment 0 6/01
SOP 37.1 Tennelec Series 5 Low Background Counting System 0 3/99
[see RPP]
SOP 37.2 Liquid Scintillation Counter (LSC) [see RPP] 0 3/99
SOP 38.1 Check-in and Orientation for Radiological Workers, 2 11/99
General Employees and Members of the Public [see RPP]
SOP 38.2 External Dosimetry Issuance [see RPP] 2 11/99
SOP 38.3 Radiation Protection Records [see RPP] 2 11/99
SOP 38.4 Radiological Protection Program Audits [see RPP] 1 3/99
SOP 38.5 Occupational Exposure Reports [see RPP] 1 3/99
SOP 39.1 LEHR Site Inspection [see RPP] 1 3/99
SOP 40.1 Ambient Radiation Monitoring Program 0 4/98
SOP 41.1 LEHR Document Review Procedures 0 3/98
SOP 42.1 Environment, Safety and Health Reporting 0 9/01
SOP 43.1 Security 0 11/01

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Standard Operating Procedures and Forms Table of Contents
LEHR Environmental Restoration / Waste Management 12/10/99
DOE Contract No. DE-AC03-96SF20686 Page iii of vi

FORMS AND FIGURES FOR STANDARD OPERATING PROCEDURES

SOP No. Form No. Form Title Revision Date of
No. Revision
SOP 1.1 Chain-of-Custody Record 1 3/99
Field Activity Daily Log 2 12/99
SOP 2.1 None
SOP 3.1 Sample Collection Log 1 4/02
SOP 3.2 Borehole/Well Construction Log 0 3/98
SOP 4.1 None
SOP 5.1 Water Levels Form 0 3/98
Well Development Data Form 0 3/98
Water Sampling Data Form 0 3/98
SOP 5.2 None
SOP 6.1 None
SOP 6.2 None
SOP 7.1 None
SOP 8.1 Borehole/Well Construction Log 0 3/98
SOP 8.2 Well Development Data Form 0 3/98
SOP 8.3 DWR Form 188, Rev. 7-90 0 3/98
Well Abandonment Log 0 3/98
SOP 9.1 None
SOP 10.1 None
SOP 10.2 None
SOP 10.3 Field Screening Samples and Analysis 0 6/98
Form
SOP 11.1 None
SOP 12.1 None
SOP 13.2 Example Air Monitoring 0 4/98
Chain-of-Custody
Air Sampling Station Meter Log 0 4/98
Radtrack Alpha Track 0 4/98
Chain-of-Custody
SOP 14.1 None
SOP 14.2 None
SOP 14.3 None
SOP 14.4 None
SOP 15.1 Borehole/Well Construction Log 0 3/98
SOP 17.1 Example Sample Label 0 3/98
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Standard Operating Procedures and Forms Table of Contents
LEHR Environmental Restoration / Waste Management 12/10/99
DOE Contract No. DE-AC03-96SF20686 Page iv of vi

SOP 17.2 None
SOP 18.1 None
SOP 19.1 None
SOP 20.1 Equipment Checklist 0 3/98
Table 1. Recommendations for Water 0 3/98
Samples
Table 2. Recommendations for 0 3/98
Sediment/Soil Samples
SOP 21.1 Validation of Organic Data by GC/MS 1 9/10
Analysis
Validation of Organic Data by GC 1 9/10
Analysis
Validation of Radiochemistry Data 0 1/98
Validation of Metals Data 1 9/10
Validation of Data from Wet Chemistry or 0 1/98
other Miscellaneous Analyses
Data Validation Qualifier Definitions 0 1/98
LEHR Data Validation Summary 0 1/98
SOP 21.2 Data Reporting Form 1/98
SOP 23.1 Standards for Third-Order Plane Surveys 0 3/98
SOP 24.1 Surface Confirmation Values 0 6/99
Values for Establishing Sealed Radioactive 1 6/99
Source Accountability with Radioactive
Material Posting and Labeling
Requirements
SOP 25.1 Radiological Survey Log Sheet 1 3/99
SOP 25.2 Radiological Survey Form 0 7/98
Radiological Survey Form Continuation 0 7/98
Sheet
Radiological Survey Log Sheet 1 3/99
Radioactive Airborne Contamination 0 7/98
Survey Report Form
Scaler Setup Sheet 0 7/98
Scaler Daily Source Check Sheet 0 7/98
SOP 29.1 None
SOP 30.1 None
SOP 31.1 None
SOP 32.1 Surface Contamination Values 1 3/99
Guidelines for Contamination Control 1 3/99
Practices
Guidelines for Contamination Control 1 3/99
Practices
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Standard Operating Procedures and Forms Table of Contents
LEHR Environmental Restoration / Waste Management 12/10/99
DOE Contract No. DE-AC03-96SF20686 Page v of vi

Checklist for Reducing Occupational 1 3/99
Radiation Exposure
Physical Access Controls for High and 1 3/99
Very High Radiation Areas
Guidelines for Personnel Contamination 1 3/99
Monitoring with Hand Held Instruments
SOP 34.1 Container Log 0 3/98
SOP 34.2 Waste Management Weekly Inspection
Checklist
SOP 34.3 Waste Shipment Checklist 0 7/98
Transport Vehicle Inspection Checklist 0 7/98
Exclusive Use Instructions 0 7/98
Document Package Distribution 0 7/98
SOP 34.4 Waste/Material Evaluation Process 2 6/01
SOP 34.5 Example of Waste Tracking Sheet (Form 0 2/99
SOP 34.5)
Example of Completed Waste Tracking 0 2/99
Sheet
SOP 35.1 None
SOP 37.1 None
SOP 37.2 None
SOP 38.1 LEHR Visitor Sign-In Log 2 11/99
Visitor Orientation Form 2 11/99
General Employee Radiation Training Log 2 11/99
(GERT)
Personal/Occupational History 2 11/99
Request for Report of Radiation History 2 11/99
Training Certificate List 2 11/99
SOP 38.2 None
SOP 38.3 None
SOP 38.4 RPP Audit Plan Schedule 1 3/99
SOP 38.5 None
SOP 39.1 None
SOP 40.1 Environmental Dosimetry Inspection Form 0 4/98
TLD Locations 0 11/97
SOP 41.1 QA/QC Checklist for Documents 0 3/98
Document Review Tracking Form 0 3/98
SOP 42.1 US DOE Individual Accident/Incident
Report
DOE M 32.1-1
Tabulation of Work Hours and Vehicle
Usage, and Property Valuation
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