APPENDIX G First Quarter 2018 Analytical Laboratory Methods, Method Detection Limits ...

198 Pages·2017·5 MB·English

APPENDIX G
First Quarter 2018 Analytical Laboratory Methods, Method Detection Limits,
Reporting Limits, QA/QC Procedures, and ELAP Certifications
TABLE G
ANNUAL LIST OF ANALYTICAL METHODS BY ANALYTE WITH CORRESPONDING LABORATORY REPORTING LIMITS AND METHOD DETECTION LIMITS
FIRST QUARTER 2018
NPDES PERMIT CA0001309
THE BOEING COMPANY
VENTURA COUNTY, CALIFORNIA
Permit Limits (PL)
Receiving
Monthly Daily Daily Daily Receiving
Water
Average Maximum Maximum Maximum Water
Sediment
Limits Limits Limits Limits Limits
TestAmerica TestAmerica Laboratory Limits
SWRCB
Method Analyte Units Laboratory Laboratory vs
ML
2018 MDL 2018 RL ML(1)
001, 002 003-007,
019, 020 008 Arroyo Simi Arroyo Simi
011, 018 009, 010
EPA 624 - Low-level 1,1,1-Trichloroethane µg/L 0.250 0.500 2 --(b)
EPA 624 - Low-level 1,1,2,2-Tetrachloroethane µg/L 0.250 0.500 1 --(b)
EPA 624 - Low-level 1,1,2-Trichloroethane µg/L 0.250 0.500 2 --(b)
EPA 624 - Low-level 1,1-Dichloroethane µg/L 0.250 0.500 1 --(b)
EPA 624 - Low-level 1,1-Dichloroethene µg/L 0.250 0.500 2 --(a) 3.2 6.0
EPA 624 - Low-level 1,2-Dichlorobenzene µg/L 0.200 0.500 2 --(b)
EPA 624 - Low-level 1,2-Dichloroethane µg/L 0.250 0.500 2 --(a) 0.5
EPA 624 - Low-level 1,2-Dichloropropane µg/L 0.250 0.500 1 --(b)
EPA 624 - Low-level 1,3-Dichlorobenzene µg/L 0.250 0.500 2 --(b)
EPA 624 - Low-level 1,3-Dichloropropene (reported as cis & trans) µg/L 0.250 0.500 2 --(b)
EPA 624 - Low-level 1,4-Dichlorobenzene µg/L 0.250 0.500 2 --(b)
EPA 624 - Low-level Benzene µg/L 0.250 0.500 2 --(b)
EPA 624 - Low-level Bromoform µg/L 0.400 1.00 2 --(b)
EPA 624 - Low-level Bromomethane µg/L 0.250 0.500 2 --(b)
EPA 624 - Low-level Carbon tetrachloride µg/L 0.250 0.500 2 --(b)
EPA 624 - Low-level Chlorobenzene µg/L 0.250 0.500 2 --(b)
EPA 624 - Low-level Chlorodibromomethane µg/L 0.250 0.500 2 --(b)
EPA 624 - Low-level Chloroethane µg/L 0.400 1.00 2 --(b)
EPA 624 - Low-level Chloroform (Trichloromethane) µg/L 0.250 0.500 2 --(b)
EPA 624 - Low-level Chloromethane (Methyl Chloride) µg/L 0.250 0.500 2 --(b)
EPA 624 - Low-level Dibromochloromethane µg/L 0.250 0.500 2 --(b)
EPA 624 - Low-level Ethylbenzene µg/L 0.250 0.500 2 --(b)
EPA 624 - Low-level Methylene chloride µg/L 0.880 2.00 2 --(b)
EPA 624 - Low-level Tetrachloroethene µg/L 0.250 0.500 2 --(b)
EPA 624 - Low-level Toluene µg/L 0.250 0.500 2 --(b)
EPA 624 - Low-level trans-1,2-Dichloroethene µg/L 0.250 0.500 1 --(b)
EPA 624 - Low-level Trichloroethene µg/L 0.250 0.500 2 --(a) 5.0
EPA 624 - Low-level Vinyl chloride µg/L 0.250 0.500 2 --(b)
EPA 624 - Low-level m,p-Xylenes µg/L 0.500 1.00 n/a --(d)
EPA 624 - Low-level Naphthalene µg/L 0.400 1.00 n/a --(d)
EPA 624 - Low-level o-Xylene µg/L 0.250 0.500 n/a --(d)
EPA 624 - Low-level Trichlorofluoromethane µg/L 0.250 0.500 n/a --(d)

VOC - Add-ons (EPA 624) 1,1,2-Trichloro-1,2,2-trifluoroethane µg/L 0.500 2.00 n/a --(d)
VOC - Add-ons (EPA 624) 1,2-Dichloro-1,1,2-trifluoroethane µg/L 1.00 2.00 n/a --(d)
VOC - Add-ons (EPA 624) Cyclohexane µg/L 1.00 2.00 n/a --(d)
Page 1 of 7
TABLE G
ANNUAL LIST OF ANALYTICAL METHODS BY ANALYTE WITH CORRESPONDING LABORATORY REPORTING LIMITS AND METHOD DETECTION LIMITS
FIRST QUARTER 2018
NPDES PERMIT CA0001309
THE BOEING COMPANY
VENTURA COUNTY, CALIFORNIA
Permit Limits (PL)
Receiving
Monthly Daily Daily Daily Receiving
Water
Average Maximum Maximum Maximum Water
Sediment
Limits Limits Limits Limits Limits
TestAmerica TestAmerica Laboratory Limits
SWRCB
Method Analyte Units Laboratory Laboratory vs
ML
2018 MDL 2018 RL ML(1)
001, 002 003-007,
019, 020 008 Arroyo Simi Arroyo Simi
011, 018 009, 010
EPA 624/8260B A-A+2CVE LOW Acrolein µg/L 2.50 5.00 5 --(b)
EPA 624/8260B A-A+2CVE LOW Acrylonitrile µg/L 1.00 2.00 2 --(b)
EPA 624/8260B A-A+2CVE LOW 2-Chloroethyl vinyl ether µg/L 1.00 2.00 1 --(c)

EPA 625+NDMA+Hydrazine -Low-level 1,2,4-Trichlorobenzene µg/L 0.500 1.00 1 --(b)
EPA 625+NDMA+Hydrazine -Low-level 1,2-Dichlorobenzene µg/L 0.200 0.500 2 --(b)
EPA 625+NDMA+Hydrazine -Low-level 1,2-Diphenylhydrazine/Azobenzene µg/L 0.500 1.00 1 --(b)
EPA 625+NDMA+Hydrazine -Low-level 1,3-Dichlorobenzene µg/L 0.200 0.500 1 --(b)
EPA 625+NDMA+Hydrazine -Low-level 1,4-Dichlorobenzene µg/L 0.200 0.500 1 --(b)
EPA 625+NDMA+Hydrazine -Low-level 2,4,6-Trichlorophenol µg/L 0.500 1.00 10 --(a) 6.5 13
EPA 625+NDMA+Hydrazine -Low-level 2,4-Dichlorophenol µg/L 1.00 2.00 5 --(b)
EPA 625+NDMA+Hydrazine -Low-level 2,4-Dimethylphenol µg/L 1.00 2.00 2 --(b)
EPA 625+NDMA+Hydrazine -Low-level 2,4-Dinitrophenol µg/L 2.00 5.00 5 --(b)
EPA 625+NDMA+Hydrazine -Low-level 2,4-Dinitrotoluene µg/L 2.00 5.00 5 --(a) 9.1 18
EPA 625+NDMA+Hydrazine -Low-level 2,6-Dinitrotoluene µg/L 2.00 5.00 5 --(b)
EPA 625+NDMA+Hydrazine -Low-level 2-Chloronaphthalene µg/L 0.200 0.500 10 --(b)
EPA 625+NDMA+Hydrazine -Low-level 2-Chlorophenol µg/L 0.500 1.00 5 --(b)
EPA 625+NDMA+Hydrazine -Low-level 2-Methyl-4,6-Dinitrophenol µg/L 2.00 5.00 5 --(b)
EPA 625+NDMA+Hydrazine -Low-level 2-Nitrophenol µg/L 1.00 2.00 10 --(b)
EPA 625+NDMA+Hydrazine -Low-level 3,3'-Dichlorobenzidine µg/L 2.00 5.00 5 --(b)
EPA 625+NDMA+Hydrazine -Low-level 4-Bromophenyl phenyl ether µg/L 0.500 1.00 5 --(b)
EPA 625+NDMA+Hydrazine -Low-level 4-Chloro-3-methylphenol µg/L 0.200 2.00 1 --(b)
EPA 625+NDMA+Hydrazine -Low-level 4-Chlorophenyl phenyl ether µg/L 0.200 0.500 5 --(b)
EPA 625+NDMA+Hydrazine -Low-level 4-Nitrophenol µg/L 2.00 5.00 10 --(b)
EPA 625+NDMA+Hydrazine -Low-level Acenaphthene µg/L 0.200 0.500 1 --(b)
EPA 625+NDMA+Hydrazine -Low-level Acenaphthylene µg/L 0.200 0.500 10 --(b)
EPA 625+NDMA+Hydrazine -Low-level Anthracene µg/L 0.200 0.500 10 --(b)
EPA 625+NDMA+Hydrazine -Low-level Benzidine µg/L 5.00 10.0 5 --(c)
EPA 625+NDMA+Hydrazine -Low-level Benzo(a)anthracene µg/L 2.00 5.00 5 --(b)
EPA 625+NDMA+Hydrazine -Low-level Benzo(a)pyrene µg/L 0.500 2.00 10 --(b)
EPA 625+NDMA+Hydrazine -Low-level Benzo(b)fluoranthene µg/L 1.00 2.00 10 --(b)
EPA 625+NDMA+Hydrazine -Low-level Benzo(g,h,i)perylene µg/L 2.00 5.00 5 --(b)
EPA 625+NDMA+Hydrazine -Low-level Benzo(k)fluoranthene µg/L 0.250 0.500 10 --(b)
EPA 625+NDMA+Hydrazine -Low-level Bis (2-chloroethoxy) methane µg/L 0.200 0.500 5 --(b)
EPA 625+NDMA+Hydrazine -Low-level Bis (2-chloroethyl) ether µg/L 0.200 0.500 1 --(b)
EPA 625+NDMA+Hydrazine -Low-level Bis (2-chloroisopropyl) ether µg/L 0.200 0.500 2 --(b)
EPA 625+NDMA+Hydrazine -Low-level Bis (2-ethylhexyl) phthalate µg/L 2.00 5.00 5 --(a) 4.0
EPA 625+NDMA+Hydrazine -Low-level Butyl benzylphthalate µg/L 2.00 5.00 10 --(b)
EPA 625+NDMA+Hydrazine -Low-level Chrysene µg/L 0.200 0.500 10 --(b)
Page 2 of 7
TABLE G
ANNUAL LIST OF ANALYTICAL METHODS BY ANALYTE WITH CORRESPONDING LABORATORY REPORTING LIMITS AND METHOD DETECTION LIMITS
FIRST QUARTER 2018
NPDES PERMIT CA0001309
THE BOEING COMPANY
VENTURA COUNTY, CALIFORNIA
Permit Limits (PL)
Receiving
Monthly Daily Daily Daily Receiving
Water
Average Maximum Maximum Maximum Water
Sediment
Limits Limits Limits Limits Limits
TestAmerica TestAmerica Laboratory Limits
SWRCB
Method Analyte Units Laboratory Laboratory vs
ML
2018 MDL 2018 RL ML(1)
001, 002 003-007,
019, 020 008 Arroyo Simi Arroyo Simi
011, 018 009, 010
EPA 625+NDMA+Hydrazine -Low-level Dibenz(a,h)anthracene µg/L 0.250 0.500 10 --(b)
EPA 625+NDMA+Hydrazine -Low-level Diethyl phthalate µg/L 0.500 1.00 2 --(b)
EPA 625+NDMA+Hydrazine -Low-level Dimethyl phthalate µg/L 0.250 0.500 2 --(b)
EPA 625+NDMA+Hydrazine -Low-level Di-n-butyl phthalate µg/L 1.00 2.00 10 --(b)
EPA 625+NDMA+Hydrazine -Low-level Di-n-octyl phthalate µg/L 2.00 5.00 10 --(b)
EPA 625+NDMA+Hydrazine -Low-level Fluoranthene µg/L 0.200 0.500 1 --(b)
EPA 625+NDMA+Hydrazine -Low-level Fluorene µg/L 0.200 0.500 10 --(b)
EPA 625+NDMA+Hydrazine -Low-level Hexachlorobenzene µg/L 0.500 1.00 1 --(b)
EPA 625+NDMA+Hydrazine -Low-level Hexachlorobutadiene µg/L 0.500 2.00 1 --(b)
EPA 625+NDMA+Hydrazine -Low-level Hexachlorocyclopentadiene µg/L 2.00 5.00 5 --(b)
EPA 625+NDMA+Hydrazine -Low-level Hexachloroethane µg/L 0.500 3.00 1 --(b)
EPA 625+NDMA+Hydrazine -Low-level Indeno(1,2,3-cd)pyrene µg/L 1.00 2.00 10 --(b)
EPA 625+NDMA+Hydrazine -Low-level Isophorone µg/L 0.500 1.00 1 --(b)
EPA 625+NDMA+Hydrazine -Low-level Naphthalene µg/L 0.500 1.00 1 --(b)
EPA 625+NDMA+Hydrazine -Low-level Nitrobenzene µg/L 0.500 1.00 1 --(b)
EPA 625+NDMA+Hydrazine -Low-level n-Nitrosodimethylamine µg/L 1.00 2.00 5 --(a) 8.1 16
EPA 625+NDMA+Hydrazine -Low-level n-Nitroso-di-n-propylamine µg/L 1.00 2.00 5 --(b)
EPA 625+NDMA+Hydrazine -Low-level n-Nitrosodiphenylamine µg/L 0.500 1.00 1 --(b)
EPA 625+NDMA+Hydrazine -Low-level Pentachlorophenol µg/L 1.00 2.00 5 --(a) 8.2 16.5
EPA 625+NDMA+Hydrazine -Low-level Phenanthrene µg/L 0.200 0.500 5 --(b)
EPA 625+NDMA+Hydrazine -Low-level Phenol µg/L 0.500 1.00 1 --(b)
EPA 625+NDMA+Hydrazine -Low-level Pyrene µg/L 0.200 0.500 10 --(b)
EPA 625+NDMA+Hydrazine -Low-level
PCB, Low Level (EPA 608) Aroclor 1016 µg/L 0.250 0.500 0.5 --(g) 0.0003
PCB, Low Level (EPA 608) Aroclor 1221 µg/L 0.250 0.500 0.5 --(g) 0.0003
PCB, Low Level (EPA 608) Aroclor 1232 µg/L 0.250 0.500 0.5 --(g) 0.0003
PCB, Low Level (EPA 608) Aroclor 1242 µg/L 0.250 0.500 0.5 --(g) 0.0003
PCB, Low Level (EPA 608) Aroclor 1248 µg/L 0.250 0.500 0.5 --(g) 0.0003
PCB, Low Level (EPA 608) Aroclor 1254 µg/L 0.250 0.500 0.5 --(g) 0.0003
PCB, Low Level (EPA 608) Aroclor 1260 µg/L 0.250 0.500 0.5 --(g) 0.0003
PCB, Low Level (EPA 608) Aroclor 1016 µg/g 0.017 0.049 n/a --(c) 0.12
PCB, Low Level (EPA 608) Aroclor 1221 µg/g 0.017 0.049 n/a --(c) 0.12
PCB, Low Level (EPA 608) Aroclor 1232 µg/g 0.017 0.049 n/a --(c) 0.12
PCB, Low Level (EPA 608) Aroclor 1242 µg/g 0.017 0.049 n/a --(c) 0.12
PCB, Low Level (EPA 608) Aroclor 1248 µg/g 0.017 0.049 n/a --(c) 0.12
PCB, Low Level (EPA 608) Aroclor 1254 µg/g 0.017 0.049 n/a --(c) 0.12
PCB, Low Level (EPA 608) Aroclor 1260 µg/g 0.017 0.049 n/a --(c) 0.12
Page 3 of 7
TABLE G
ANNUAL LIST OF ANALYTICAL METHODS BY ANALYTE WITH CORRESPONDING LABORATORY REPORTING LIMITS AND METHOD DETECTION LIMITS
FIRST QUARTER 2018
NPDES PERMIT CA0001309
THE BOEING COMPANY
VENTURA COUNTY, CALIFORNIA
Permit Limits (PL)
Receiving
Monthly Daily Daily Daily Receiving
Water
Average Maximum Maximum Maximum Water
Sediment
Limits Limits Limits Limits Limits
TestAmerica TestAmerica Laboratory Limits
SWRCB
Method Analyte Units Laboratory Laboratory vs
ML
2018 MDL 2018 RL ML(1)
001, 002 003-007,
019, 020 008 Arroyo Simi Arroyo Simi
011, 018 009, 010
Pesticides, Low Level (EPA 608) Aldrin µg/L 0.0015 0.0050 0.005 --(b)
Pesticides, Low Level (EPA 608) alpha-BHC µg/L 0.0025 0.0050 0.01 --(a) 0.01 0.03
Pesticides, Low Level (EPA 608) alpha-Endosulfan µg/L 0.00300 0.00500 0.02 --(b)
Pesticides, Low Level (EPA 608) beta-BHC µg/L 0.0040 0.0100 0.005 --(b)
Pesticides, Low Level (EPA 608) beta-Endosulfan µg/L 0.00200 0.00500 0.01 --(b)
Pesticides, Low Level (EPA 608) delta-BHC µg/L 0.0035 0.0050 0.005 --(b)
Pesticides, Low Level (EPA 608) gamma-BHC (Lindane) µg/L 0.0030 0.0100 0.02 --(b)
Pesticides, Low Level (EPA 608) Chlordane µg/L 0.0800 0.100 0.1 --(g) 0.001
Pesticides, Low Level (EPA 608) 4,4'-DDD µg/L 0.00400 0.00500 0.05 --(g) 0.0014
Pesticides, Low Level (EPA 608) 4,4'-DDE µg/L 0.00300 0.00500 0.05 --(g) 0.001
Pesticides, Low Level (EPA 608) 4,4'-DDT µg/L 0.00400 0.0100 0.01 --(g) 0.001
Pesticides, Low Level (EPA 608) Dieldrin µg/L 0.00200 0.00500 0.01 --(g) 0.0002
Pesticides, Low Level (EPA 608) Endosulfan sulfate µg/L 0.00300 0.0100 0.05 --(b)
Pesticides, Low Level (EPA 608) Endrin µg/L 0.00200 0.00500 0.01 --(b)
Pesticides, Low Level (EPA 608) Endrin aldehyde µg/L 0.00200 0.0100 0.01 --(b)
Pesticides, Low Level (EPA 608) Heptachlor µg/L 0.00300 0.0100 0.01 --(b)
Pesticides, Low Level (EPA 608) Heptachlor epoxide µg/L 0.00250 0.00500 0.01 --(b)
Pesticides, Low Level (EPA 608) Toxaphene µg/L 0.250 0.500 0.5 --(g) 0.0003
Pesticides, Low Level (EPA 608) Chlordane µg/g 0.0100 0.0500 n/a --(f) 0.0033
Pesticides, Low Level (EPA 608) 4,4'-DDD µg/g 0.00150 0.00500 n/a --(c) 0.002
Pesticides, Low Level (EPA 608) 4,4'-DDE µg/g 0.00150 0.00500 n/a --(f) 0.0014
Pesticides, Low Level (EPA 608) 4,4'-DDT µg/g 0.00150 0.00500 n/a --(f) 0.0003
Pesticides, Low Level (EPA 608) Dieldrin µg/g 0.00150 0.00500 n/a --(f) 0.0002
Pesticides, Low Level (EPA 608) Toxaphene µg/g 0.0500 0.200 n/a --(f) 0.0006
EPA 525.2 Chlorpyrifos µg/L 0.500 1.00 n/a --(f) 0.02
(EPA 525.2) Diazinon µg/L 0.120 0.250 n/a --(c) 0.16
SW8141 Chlorpyrifos µg/L 0.500 1.00 n/a --(f) 0.02
SW8141 Diazinon µg/L 0.120 0.250 n/a --(c) 0.16
ICP/MS 200.8 Antimony µg/L 0.500 2.00 0.5 --(a) 6.0 6.0 6.0
ICP/MS 200.8 Cadmium µg/L 0.250 1.00 0.25 --(a) 2.0 4.0/3.1 4.0 4.0/3.1
ICP/MS 200.8 Copper µg/L 0.500 2.00 0.5 --(a) 5.8 14 13 14
ICP/MS 200.8 Lead µg/L 0.500 1.00 0.5 --(a) 2.6 5.2 5.2 5.2
ICP/MS 200.8 Selenium µg/L 0.500 2.00 2 --(a) 4.1 8.2/5 5
ICP/MS 200.8 Silver µg/L 0.500 1.00 0.25 --(a) 2.0 4.1
ICP/MS 200.8 Thallium µg/L 0.500 1.00 1 --(a) 2.0 2.0 2.0
Page 4 of 7
TABLE G
ANNUAL LIST OF ANALYTICAL METHODS BY ANALYTE WITH CORRESPONDING LABORATORY REPORTING LIMITS AND METHOD DETECTION LIMITS
FIRST QUARTER 2018
NPDES PERMIT CA0001309
THE BOEING COMPANY
VENTURA COUNTY, CALIFORNIA
Permit Limits (PL)
Receiving
Monthly Daily Daily Daily Receiving
Water
Average Maximum Maximum Maximum Water
Sediment
Limits Limits Limits Limits Limits
TestAmerica TestAmerica Laboratory Limits
SWRCB
Method Analyte Units Laboratory Laboratory vs
ML
2018 MDL 2018 RL ML(1)
001, 002 003-007,
019, 020 008 Arroyo Simi Arroyo Simi
011, 018 009, 010
ICP 200.7 Aluminum µg/L 50.0 100 n/a --(d)
ICP 200.7 Arsenic µg/L 8.90 10.0 10 --(a) 10.0
ICP 200.7 Barium µg/L 5.00 10.0 n/a --(c) 1000
ICP 200.7 Beryllium µg/L 1.00 2.00 2 --(a) 4.0
ICP 200.7 Boron mg/L 0.0250 0.0500 n/a --(c) 1.0 1.0
ICP 200.7 Chromium µg/L 2.50 5.00 10 --(a) see Cr VI see Cr VI
ICP 200.7 Cobalt µg/L 5.00 10.0 n/a --(d)
ICP 200.7 Hardness (as CaCO3) mg/L 0.170 0.330 n/a --(d)
ICP 200.7 Iron mg/L 0.0500 0.100 n/a --(c) 0.3
ICP 200.7 Manganese µg/L 10.0 20.0 n/a --(c) 50
ICP 200.7 Nickel µg/L 5.00 10.0 20 --(a) 35 94 86 86
ICP 200.7 Vanadium µg/L 5.00 10.0 n/a --(d)
ICP 200.7 Zinc µg/L 12.0 20.0 20 --(a) 43 119 120 120
Mercury (EPA 245.1) Mercury µg/L 0.100 0.200 0.2 --(f) 0.05 0.10 0.13 0.13

Chromium VI (EPA 218.6) Chromium VI (Hexavalent) µg/L 0.250 1.00 n/a --(c) 8.0 16
Cyanide by EPA (SM4500) Cyanide µg/L 2.50 5.00 5 --(a) 4.3 8.5 9.5 9.5
Asbestos by EPA 600 Asbestos MFL n/a (2) n/a (2) n/a --(d)
EPA 8260B-Mod 1,4-Dioxane µg/L 0.500 2.00 n/a --(d)
EPA 8015-Mod Diesel Range Organics (DRO C13-C28) mg/L 0.100 0.500 n/a --(d)
EPA 8015-Mod Gasoline Range Organics (GRO C4-C12) mg/L 0.0250 0.0500 n/a --(d)
EPA 314.0 Perchlorate µg/L 0.950 4.00 n/a --(c) 6.0 6.0 6.0
EPA 1613 TCDD TEQ µg/L n/a n/a n/a --(e) 1.4E-08 2.8E-08 2.8E-08 2.8E-08
General Chemistry, (Field Test) Chlorine, Total Residual (3) mg/L n/a 0.1 n/a --(c) 0.1
Dissolved Oxygen (3) mg/L n/a 1 n/a --(d)
General Chemistry, EPA 120.1 Conductivity µmhos/cm n/a 1.00 n/a --(d)
General Chemistry, EPA 1664 Oil & Grease mg/L 1.40 5.00 n/a --(c) 10 15 15 15
General Chemistry, EPA 180.1 Turbidity NTU 0.0400 0.100 n/a --(d)
Page 5 of 7
TABLE G
ANNUAL LIST OF ANALYTICAL METHODS BY ANALYTE WITH CORRESPONDING LABORATORY REPORTING LIMITS AND METHOD DETECTION LIMITS
FIRST QUARTER 2018
NPDES PERMIT CA0001309
THE BOEING COMPANY
VENTURA COUNTY, CALIFORNIA
Permit Limits (PL)
Receiving
Monthly Daily Daily Daily Receiving
Water
Average Maximum Maximum Maximum Water
Sediment
Limits Limits Limits Limits Limits
TestAmerica TestAmerica Laboratory Limits
SWRCB
Method Analyte Units Laboratory Laboratory vs
ML
2018 MDL 2018 RL ML(1)
001, 002 003-007,
019, 020 008 Arroyo Simi Arroyo Simi
011, 018 009, 010
General Chemistry, EPA 300 Chloride mg/L 0.250 0.500 n/a --(c) 150 150 150
General Chemistry, EPA 300 Nitrate + Nitrite as Nitrogen (N) mg/L 0.070 0.15 n/a --(c) 8 10 8
General Chemistry, EPA 300 Nitrate - N mg/L 0.0550 0.110 n/a --(c) 8 8
General Chemistry, EPA 300 Nitrite - N mg/L 0.0700 0.150 n/a --(c) 1 1
General Chemistry, EPA 300 Sulfate mg/L 0.250 0.500 n/a --(c) 300 250 300
General Chemistry, SM2540C Total Dissolved Solids mg/L 5.00 10.0 n/a --(c) 950 850 950
General Chemistry, SM2540D Total Suspended Solids mg/L 0.500 1.00 n/a --(c) 15 45
General Chemistry, SM2540F Settleable Solids ml/L n/a 0.100 n/a --(c) 0.1 0.3
General Chemistry, SM4500F-C Fluoride mg/L 0.250 0.500 n/a --(c) 1.6 1.6 1.6
General Chemistry, SM4500-NH3 Ammonia – N mg/L 0.100 0.200 n/a --(c) 1.96 10.1 10.1
General Chemistry, SM5210B Biochemical Oxygen Demand (BOD)(5-Day @ 20 deg. C) mg/L 0.500 2.00 n/a --(c) 20 30
General Chemistry, SM5310B Total Organic Carbon mg/L 0.650 1.00 n/a --(d)
General Chemistry, SM5540 Detergents (as MBAS) mg/L 0.0500 0.100 n/a --(c) 0.5

Radiochemistry Uranium pCi/L n/a 1.00 (4) n/a --(c) 20 20 20
Radiochemistry, EPA 900 Gross Alpha pCi/L n/a 3.00 (4) n/a --(c) 15 15 15
Radiochemistry (Eberline Lab), EPA 900 Gross Beta pCi/L n/a 4.00 (4) n/a --(c) 50 50 50
Radiochemistry, EPA 901.1 Cesium-137 pCi/L n/a 20.0 (4) n/a --(c) 200 200 200
Radiochemistry (Eberline Lab), EPA 901.1 Potassium-40 pCi/L n/a 200 (4) n/a --(d)
Radiochemistry, EPA 903/904 Combined Radium-226 & Radium-228 pCi/L n/a n/a n/a --(e) 5.0 5.0 5.0
Radiochemistry, EPA 905.0 Strontium-90 pCi/L n/a 3.00 (4) n/a --(c) 8.0 8.0 8.0
Radiochemistry, EPA 906.0 Tritium pCi/L n/a 500 (4) n/a --(c) 20000 20000 20000
Page 6 of 7
TABLE G
ANNUAL LIST OF ANALYTICAL METHODS BY ANALYTE WITH CORRESPONDING LABORATORY REPORTING LIMITS AND METHOD DETECTION LIMITS
FIRST QUARTER 2018
NPDES PERMIT CA0001309
THE BOEING COMPANY
VENTURA COUNTY, CALIFORNIA
Permit Limits (PL)
Receiving
Monthly Daily Daily Daily Receiving
Water
Average Maximum Maximum Maximum Water
Sediment
Limits Limits Limits Limits Limits
TestAmerica TestAmerica Laboratory Limits
SWRCB
Method Analyte Units Laboratory Laboratory vs
ML
2018 MDL 2018 RL ML(1)
001, 002 003-007,
019, 020 008 Arroyo Simi Arroyo Simi
011, 018 009, 010
8315M (Truesdail Lab) Monomethyl hydrazine µg/L 0.245 10.0 n/a --(d)
Pass or Pass or % Pass or % Pass or %
Pass or
Toxicity (Aquatic Lab), EPA 1002 Chronic Toxicity Fail, % n/a n/a n/a Effect Effect Effect
Fail
Effect --(e) <50 <50 <50
Biological, SM9221F E. Coli MPN/100ml n/a 1.80 n/a --(c) 235
Notes:
Benchmark limitations: Outfalls 001, 002
Compliance limitations: Outfalls 003-011, 018-020
Columns are used to compare laboratory's reporting limits (RLs) and method detection limits (MDLs) to the SWRCB Minimum Levels (MLs) and the permit limits (PLs).
(1) This column indicates the status of analytical capabilities if the ML is less than the laboratory RL and/or MDL. See explanation for "--" below.
The following designations summarize the comparison of RLs, MDLs, MLs, and permit limits:
-- = Laboratory reporting limit meets ML if applicable and permit limit requirements
--(a) Laboratory reporting limit or method detection limit meets ML and permit limit requirements
--(b) Laboratory reporting limit or method detection limit meets ML. This analyte has no permit limit requirements.
--(c) Laboratory reporting limit or method detection limit meets permit limit. This analyte has no ML.
--(d) This analyte has no ML or permit limit.
--(e) This analyte is a calculation or chronic toxicity and does not have a reporting limit. This calculation or chronic toxicity has no ML.
--(f) This analyte has no ML. Laboratory reporting limit or method detection limit does not meet permit limit.
--(g) Laboratory reporting limit or method detection limit meets ML, but does not meet permit limit requirements
The receiving water sediment limits do not have a ML and are included for reference only.
(2) The RL and MDL for asbestos varies based upon the sample.
(3) Total residual chlorine (TRC) and dissolved oxygen (DO) are measured in the field. The RL is the lowest limit of the instrument. The MDL is not relevant for field parameters.
(4) This value is the minimum detectable activity (MDA) which applies only to radiological constituents.
Acronyms:
MFL = million fibers per liter
mg/L = milligrams per liter
MPN = most probable number per 100 milliliters
pCi/L = picoCuries per liter
SWRCB = State Water Resources Control Board
TIC = tentatively identified compound
µg/L = micrograms per liter
µg/g = micrograms per gram
n/a = not applicable
Page 7 of 7
Document No.: IR-QAM

Revision No.: 5
Effective Date: 03/14/2017
Page 1 of 150

Quality Assurance Manual Cover Page

TestAmerica Irvine

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Document No.: IR-QAM

Revision No.: 5
Effective Date: 03/14/2017
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Title Page:

Quality Assurance Manual

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Linda Scha penb. rg Date
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'J
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Date
Quality Assurance Manager
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