Advanced electron microscopy and nanomaterials : selected, peer reviewed papers from the First Joint Advanced Electron Microscopy School for Nanomaterials and the Workshop on Nanomaterials (AEM-NANOMAT '09), Saltillo (Coahuila) México, September 29th-Oct PDF
Preview Advanced electron microscopy and nanomaterials : selected, peer reviewed papers from the First Joint Advanced Electron Microscopy School for Nanomaterials and the Workshop on Nanomaterials (AEM-NANOMAT '09), Saltillo (Coahuila) México, September 29th-Oct
Advanced Electron Microscopy and Nanomaterials Advanced Electron Microscopy and Nanomaterials Selected, peer reviewed papers from the First Joint Advanced Electron Microscopy School for Nanomaterials and the Workshop on Nanomaterials (AEM-NANOMAT’09), Saltillo (Coahuila) México, September 29th-October 2nd, 2009 Edited by: Arturo Ponce and Darío Bueno TRANS TECH PUBLICATIONS LTD Switzerland • UK • USA Copyright © 2010 Trans Tech Publications Ltd, Switzerland All rights reserved. No part of the contents of this publication may be reproduced or transmitted in any form or by any means without the written permission of the publisher. Trans Tech Publications Ltd Laubisrutistr. 24 CH-8712 Stafa-Zurich Switzerland http://www.ttp.net Volume 644 of Materials Science Forum ISSN 0255-5476 Full text available online at http://www.scientific.net Distributed worldwide by and in the Americas by Trans Tech Publications Ltd Trans Tech Publications Inc. Laubisrutistr. 24 PO Box 699, May Street CH-8712 Stafa-Zurich Enfield, NH 03748 Switzerland USA Phone: +1 (603) 632-7377 Fax: +41 (44) 922 10 33 Fax: +1 (603) 632-5611 e-mail: [email protected] e-mail: [email protected] Saltillo (Coahuila) Mexico th nd September 29 – October 2 , 2009 Organizers Local Committee: Chairman Arturo Ponce Pedraza [email protected] Co-Chairman Darío Bueno Baqués [email protected] Program Coordinator: Leticia Rodríguez González [email protected] Gerardo Martínez and Esmeralda [email protected] School Secretariat: Saucedo [email protected] Support Committee: Oliverio Rodríguez Fernández [email protected] Exhibition contact: Jesús Olivo Padilla [email protected] Student Support Luis Ernesto Elizalde Herrera [email protected] Coordinator: Treasurer: Josefina del Refugio Pérez Huerta [email protected] National Committee: Institute of Physics National University of Jesús Arenas Alatorre [email protected] Mexico Juan Méndez-Nonell Research Center for Applied Chemistry (CIQA) [email protected] Vicente Garibay Febles Mexican Petroleum Institute (Mexico) [email protected] Leopoldo Enriquez Jeol de México SA de CV [email protected] Fernando Mendoza FEI Company [email protected] Kaheri Arellano Carl Zeiss de México, SA de CV [email protected] Invited speakers Dual/Beam (SEM/FIB) applications Dr. Tomas Vystavel FEI Specialist Title 1: TEM Sample Preparation with DualBeam DUAL-BEAM (SEM/FIB) – Netherlands Title 2: Advanced DualBeam Applications in NanoPrototyping and 3-D Characterization High resolution transmission electron microscopy (HRTEM) and scanning transmission electron Dr. Dong Tang microscopy (STEM) FEI Specialist HRTEM and STEM - Netherlands Title 1: Atomic scale high-resolution transmission electron microscopy Title 2: STEM applications in nano-sciences In-lens and LAB detectors in FEG-STEM M.C. Martin Palacios Title 1: The high resolution at low kV in a FEG scanning Jeol Specialist - Mexico electron microscope Title 2: Study of nonconductive samples using the r-Filter Dr. Antonio Casares Advanced EELS and Omega filter for TEM Carl Zeiss NTS GmbH Specialist applications EELS and Omega filter – Germany Title: Advanced EELS and Omega filter for TEM applications Dr. Marco Antonio Ramirez Cross Beam (AURIGA) Carl Zeiss Cross Beam (AURIGA) – México Title: SEM/FIB preparation samples Dr. Alfredo Gomez HRTEM and electron diffraction simulation Institute of Physics UNAM Mexico Title: HRTEM and electron diffraction simulation kinematical and dynamical diffraction and HRTEM Dr. Laurence D. Marks Northwestern University – USA Title: kinematical and dynamical diffraction and HRTEM: quantitative analysis Dr. Stavros Nicolopoulos Precession Electron diffraction in TEM NanoMEGAS SPRL – Belgium Title: Precession interface Spinning Star Dr. José Reyes-Gasga Electron diffraction Institute of Physics UNAM Mexico Title: Dynamical electron diffraction in crystals Dr. Jean-Paul Morniroli LACBED. Applications in Materials Science Laboratoire de Metallurgie Physique CNRS – France Title: LACBED. Applications in Materials Science Dr. Miguel Ávalos Borja EELS CNyN-UNAM - Mexico Title: EELS theory and applications International Advisory Committee Juan Méndez-Nonell CIQA - (Mexico) Fernando Ponce Arizona State University (USA) Miguel José Yacamán University of Texas at San Antonio (USA) János L Lábár Institute for Technical Physics (Hungary) Sven Hovmöller Stockholm University (Sweden) David Ríos IPICYT (Mexico) Robert Sinclair University of Stanford (USA) Karla Balzuweit Universidade Federal de Minas Gerais (Brazil) Rafael Garía Roja University of Cadiz (Spain) José Reyes-Gasga National University of Mexico (Mexico) Alejandro Zúñiga University of Chile (Chile) Gustavo Martínez National University of Colombia (Colombia) Walter Jose Botta Federal University of São Carlos (Brazil) Jean-Paul Morniroli University of Lille (France) Sergio Lozano-Perez University of Oxford (UK) Topics •Multifunctional nanocomposites •Smart materials •Nanoparticles: synthesis and applications •Structure phenomena and modeling •Growth of thin films •Semiconductors and optoelectronic materials •Other nanomaterials and interdisciplinary topics Table of Contents Organizers Invited Speakers International Advisory Committee Picture Topic 1: Multifunctional Nanocomposites Precession Electron Diffraction Assisted Orientation Mapping in the Transmission Electron Microscope J. Portillo, E.F. Rauch, S. Nicolopoulos, M. Gemmi and D. Bultreys 1 TEM Characterization on the Nanocomposite Al 7075 and Silver Nanoparticles Synthesized by Powder Metallurgy R. Flores-Campos, R. Deaquino-Lara, J.M. Herrera-Ramírez, A. Ponce, I. Estrada-Guel, M. Miki- Yoshida and R. Martínez-Sánchez 9 Synthesis of Plasticizer-Based Ferrofluid and its Use in the Preparation of Magnetic PVC Nanocomposite E. Servín-Hernández, O.S. Rodríguez-Fernández and L.A. García-Cerda 13 Effect of Type and Concentration of Ionomer Compatibilizer on the Hdpe/ Ionomer/ Clay Nanocomposites Morphology S. López-García, S. Sánchez-Valdés and L.F. Ramos de Valle 17 Elemental Analysis of a Heterogeneous Polymeric System by EDS: Detection of the Compatibilizer Agent Containing Si Atoms and Silver Nano-Particles (AgNP´s) in High Impact Polystyrene F. Soriano, C. de Anda, G. Morales and A. Ponce 21 Dielectric Properties of PMMA-SiO Hybrid Films 2 M.D. Morales-Acosta, M.A. Quevedo-López, H.N. Alshareef, B.E. Gnade and R. Ramírez-Bon 25 Synthesis and Characterization of Magnetic Polyurethane Nanocomposite Foams A. Cámara-Hinojosa, D. Bueno-Baqués, O.S. Rodríguez-Fernández and R.F. Ziolo 29 Topic 2: Smart Materials Preparation of Electrospun Barium Titanate – Polyvinylidene Fluoride Piezoelectric Membranes V. Corral-Flores, J.J. Pérez-Herrera, E. Torres-Moye, J. Romero-García, D. Bueno-Baqués and R.F. Ziolo 33 Topic 3: Nanoparticles: Synthesis and Applications Preparation and Properties of CoFe O Synthesized by the Modified Citrate-Gel Method 2 4 E.M. Múzquiz-Ramos, D.A. Cortés-Hernández, O.A. Herrera-Romero and J.C. Escobedo- Bocardo 39 Alumina-Copper Composites with High Fracture Toughness and Low Electrical Resistance E. Rocha-Rangel and J.G. Miranda-Hernández 43 Obtaining NiHCF Nanoparticles Using a Reverse Micellar System A. Gutiérrez Becerra, T. Vega Venegas, M. Bárcena Soto, N. Casillas and J.I. Escalante 47 Iron Oxide Nanoparticles Obtained from a Fe(II) - Chitosan Polymer Film J.F. Luna Martínez, E. Reyes-Melo, V. González-González, A. Torres-Castro, C. Guerrero- Salazar and S. Sepúlveda-Guzmán 51 Synthesis and Characterization of Branched Gold Nanoparticles A. Mayoral, A. Vazquez-Duran, S.G. Heinze and M.J. Yacaman 57 Surface Modification of ZnO Nanoparticles R. Betancourt-Galindo, M.L. Berlanga Duarte, B.A. Puente Urbina, O.S. Rodríguez-Fernández and S. Sánchez-Valdés 61 Topographical Characterization of Electrodeposited Nickel Nanoparticles on an Indium Tin Oxide on Glass Thin Film G.T. Martinez, G. Zavala and M. Videa 65
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