Validated data for SDGs 87, 90, and 92 of the Camp Edwards impact area groundwater study: Massachusetts Military Reservation, Cape Cod, Massachusetts PDF
Preview Validated data for SDGs 87, 90, and 92 of the Camp Edwards impact area groundwater study: Massachusetts Military Reservation, Cape Cod, Massachusetts
Validated Data for SDG s 87, 90, • and 92 of the Camp Edwards Impact Area Groundwater Study Massachusetts Military Reservation Cape Cod Massachusetts , Ogden Environmental and Energy Services September 1998 VALIDATED DATA FOR SDGs 87, 90, AND 92 OF THE CAMP EDWARDS IMPACT AREA GROUNDWATER STUDY MASSACHUSETTS MILITARY RESERVATION CAPE COD, MASSACHUSETTS Prepared for NATIONAL GUARD BUREAU ARLINGTON, VIRGINIA Prepared by OGDEN ENVIRONMENTAL AND ENERGY SERVICES 239 Littleton Road, Suite IB Westford, Massachusetts 01886 September 1998 QUALIFICATION CODE REFERENCE TABLE Qualifier Organics Inorganics H Holding times wereexceeded. Holding times were exceeded. • S Surrogate recoverywasoutside QC limits. The sequenceornumberofstandardsusedfor the calibration was incorrect. c Calibration %RSD or%D were noncompliant. Correlation coefficientis <0.995. R Calibration RRF was O.05. %Rforcalibration isnotwithin control limits. B Presumedcontamination frompreparation Presumedcontaminationfrompreparation (method) blank. (method) orcalibrationblank. %R L Not applicable. Laboratory Control Sample werenotwithin control limits. MS/MSD recover/was poororRPD high. MS recover/waspoor. E Not applicable. Duplicates showed poor agreement. I Internal standard performance was unsatisfactory. ICP ICS results were unsatisfactory. A Not applicable. ICP Serial Dilution%D were notwithincontrol limits. M Tuning (BFB orDFTPP) was noncompliant. Not applicable. T Presumedcontamination fromtrip blank. Not applicable. + False positive - reportedcompoundwasnot Not applicable. present. - Falsenegative - compoundwas presentbutnot Notapplicable. reported. F Presumedcontamination from FB orER. Presumedcontamination from FB orER. $ Reportedresultorotherinformationwas Reportedresultorother informationwas incorrect. incorrect. ? TIC identityorreportedretentiontimehasbeen Notapplicable. changed. D The analysis with this flagshouldnotbeused The analysis withthisflagshouldnotbeused because anothermoretechnically sound analysis because anothermoretechnicallysound analysis is available. is available. P Instrumentperformanceforpesticideswaspoor. PostDigestion Spikerecoverywasnotwithin control limits. *# Unusual problems foundwith thedatathathave Unusual problems foundwiththe datathathave beendescribedin Section 1, "Data Validation beendescribed inSection 1, "Data Validation Findings." Thenumberfollowingthe asterisk(*) Findings." Thenumberfollowingthe asterisk(*) will indicate the subsectionwhere adescriptionof will indicatethe subsection where adescriptionof the problem canbefound. the problemcanbefound. DATA QUALIFIERREFERENCETABLE Qualifier Organics Inorganics U The analytewas analyzedfor,butwasnotdetected Thematerial was analyzedfor,butwas not abovethereportedsample quantitationlimit. detected above the level ofthe associated value. The associatedvalue is eitherthe sample quantitation limitorthe sample detectionlimit J The analytewaspositivelyidentified; the The associatedvalue is anestimated quantity. associatednumerical value isthe approximate concentrationofthe analyte inthe sample. N The analysis indicatesthepresenceofan analyte Notapplicable. forwhichthere ispresumptiveevidence tomakea "tentative identification." NJ The analysis indicatesthepresenceofan analyte Notapplicable. thathasbeen "tentatively identified" andthe associatednumerical valuerepresents its approximateconcentration. UJ The analytewas notdeemedabove thereported The matenal was analyzedfor, butwasnot sample quantitation limit. However, thereported detected. The associatedvalue is anestimate quantitation limit is approximate andmayormay andmaybe inaccurate orimprecise. notrepresentthe actual limitofquantitation necessary to accuratelyandpreciselymeasurethe analyte inthe sample. R The sampleresults are rejecteddueto serious Thedata are unusable. (Note: Analyte mayor deficiencies in the abilityto analyzethe sample and maynotbepresent). tomeetqualitycontrol criteria. 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