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Solid State Physics - Volume 65 PDF

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AcademicPressisanimprintofElsevier 525BStreet,Suite1800,SanDiego,California92101-4495,USA 225WymanStreet,Waltham,MA02451,USA TheBoulevard,LangfordLane,Kidlington,Oxford,OX51GB,UK 32JamestownRoad,London,NW17BY,UK Radarweg29,POBox211,1000AEAmsterdam,TheNetherlands Firstedition2014 Copyright©2014,ElsevierInc.Allrightsreserved. Nopartofthispublicationmaybereproduced,storedinaretrievalsystem,ortransmittedin anyformorbyanymeanselectronic,mechanical,photocopying,recordingorotherwise, withoutthepriorwrittenpermissionofthepublisher. PermissionsmaybesoughtdirectlyfromElsevier’sScienceandTechnologyRights DepartmentinOxford,UK:phone:(+44)(0)1865843830;fax:(+44)(0)1865853333; e-mail:permissions@elsevier.com.Alternativelyyoucansubmityourrequestonlineby visitingtheElsevierwebsiteathttp://elsevier.com/locate/permissions,andselecting ObtainingpermissiontouseElseviermaterial. Notice Noresponsibilityisassumedbythepublisherforanyinjuryand/ordamagetopersonsor propertyasamatterofproductsliability,negligenceorotherwise,orfromanyuseor operationofanymethods,products,instructionsorideascontainedinthematerialherein. Becauseofrapidadvancesinthemedicalsciences,inparticular,independentverificationof diagnosesanddrugdosagesshouldbemade. ISBN:978-0-12-800175-2 ISSN:0081-1947 ForinformationonallAcademicPresspublications visitourwebsiteatstore.elsevier.com PrintedandboundinUSA 14 15 16 17 10 9 8 7 6 5 4 3 2 1 CONTRIBUTORS Numbersinparenthesisindicatethepagesonwhichtheauthors’contributionsbegin AnjanBarman(1) ThematicUnitofExcellenceonNanodeviceTechnologyandDepartmentofCondensed MatterPhysicsandMaterialSciences,S.N.BoseNationalCentreforBasicSciences,Kolkata, India GustavBihlmayer(353) PeterGru¨nbergInstitut(PGI-7),andInstituteofAdvancedSimulation(IAS-1), ForschungszentrumJu¨lich,Ju¨lich,Germany ZoeBudrikis(109) ISIFoundation,Turin,Italy ArabindaHaldar(1) ThematicUnitofExcellenceonNanodeviceTechnologyandDepartmentofCondensed MatterPhysicsandMaterialSciences,S.N.BoseNationalCentreforBasicSciences,Kolkata, India ThomasSaerbeck(237) DepartmentofPhysics,andCenterforAdvancedNanoscience,UniversityofCalifornia SanDiego,LaJolla,California,USA WolfgangSpeier(353) JARA-Fundamentalsof FutureInformationTechnology,ForschungszentrumJu¨lich, Ju¨lich,Germany KrzysztofSzot(353) PeterGru¨nbergInstitut(PGI-7),ForschungszentrumJu¨lich,Ju¨lich,Germany,and A.ChelkowskiInstituteofPhysics,UniversityofSilesia,Katowice,Poland vii PREFACE Itisourgreatpleasuretopresentthe65theditionofSolid-StatePhysics.The vision statement for this series has not changed since its inception in 1955, and Solid-State Physics continues to provide a “mechanism ... whereby investigators and students can readily obtain a balanced view of the whole field.” What has changed is the field and its extent. As noted in 1955, the knowledge in areas associated with solid-state physics has grown enor- mously, and in 2014, its clear boundaries have gone well beyond what wasonce,traditionally,understoodassolidstate.Indeed,researchontopics in materials physics, applied and basic, now requires expertise across a remarkably wide range of subjects and specialties. It is for this reason that there exists an important need for up-to-date, compact reviews of topical areas. The intention of these reviews is to provide a history context for a topic that has matured sufficiently to warrant a guiding overview. Thetopicsreviewedinthisvolumeillustratethegreatbreadthanddiver- sityofmodernresearchintomaterialsandcomplexsystems,whileproviding thereaderwithacontextcommontomostphysiciststrainedorworkingin condensed matter. We have a wide range of research represented in this volume. This includes work on magnetization dynamics in thin films and nanostructures,thepropertiesofartificialspinicesystems,neutronscattering as a probe for magnetic exchange, and a review of the recently discovered resistiveswitchingphenomenawherevariousoxidescanbereversiblychan- ged from a high-resistance state to a low-resistance state. Both editors and publishershopethatreaderswillfindtheintroductionsandoverviewsuseful andof benefit bothas summariesfor workersin these fieldsandastutorials and explanations for those just entering. ROBERT E. CAMLEY Department of Physics, University of Colorado Colorado Springs, Colorado, USA ROBERT L. STAMPS School of Physics and Astronomy University of Glasgow, Glasgow, UK ix CHAPTER ONE Time-Domain Study of Magnetization Dynamics in Magnetic Thin Films and Micro- and Nanostructures Anjan Barman, Arabinda Haldar ThematicUnitofExcellenceonNanodeviceTechnologyandDepartmentofCondensedMatterPhysics andMaterialSciences,S.N.BoseNationalCentreforBasicSciences,Kolkata,India Contents 1. GeneralIntroduction 2 2. TheoreticalBackground 7 2.1 TimeScalesofMagnetizationDynamics 7 2.2 Laser-InducedUltrafastMagnetizationDynamics 8 2.3 LLGEquation 10 2.4 FerromagneticResonance 11 2.5 Spinwaves 15 2.6 Magneto-opticalKerrEffect 19 3. BackgroundofTRMOKE 25 3.1 BackgroundofTRMOKEExperiments 25 3.2 Laser-InducedUltrafastSpinDynamics 29 3.3 ImagingofPropagatingSpinWaves 32 3.4 Time-ResolvedKerrEffectMeasurementonSamplesDeposited onOpaqueSubstrate 33 3.5 All-OpticalTRMOKEMicroscope 35 3.6 BenchtopTRMOKEMagnetometer 36 4. Time-ResolvedImagingofMagnetizationDynamicsinMicroscopicMagnetic Elements 37 4.1 ImagingNonuniformPrecessionalDynamicsinSingleFerromagnetic Microstructures 38 4.2 ImagingofNoisebyTime-ResolvedKerrMicroscopy 41 4.3 ImagingofSpin-WaveModesinFerromagneticMicrowires 42 4.4 ConfigurationalAnisotropyinPrecessionFrequencyandDamping 43 4.5 ExcitationandImagingIndividualResonantModesbyTime-Resolved KerrMicroscopy 46 4.6 ImagingLargeAngleReorientationof2(cid:1)2mm2CoFe/NiFeElement 47 4.7 ImagingMagnetizationDynamicsofHardDiskWriters 47 SolidStatePhysics,Volume65 #2014ElsevierInc. 1 ISSN0081-1947 Allrightsreserved. http://dx.doi.org/10.1016/B978-0-12-800175-2.00001-7 2 AnjanBarmanandArabindaHaldar 4.8 ConversionofFreeSpaceMicrowavetoMagnonicArchitecture: TRSKMImaging 48 5. Time-ResolvedMagnetizationDynamicsofMagneticMultilayers 48 5.1 Time-ResolvedMagnetizationDynamicsofSpinValvesand Exchange-CoupledBilayers 49 5.2 UltrafastMagnetizationDynamicsofMagneticMultilayerswithPMA 50 6. PrecessionalDynamicsofMagneticNanodotArrays 54 6.1 Size-DependentCrossovertoNonuniformPrecession 55 6.2 DynamicalConfigurationalAnisotropy 57 6.3 CouplingBetweenMagneticandElasticModes 57 6.4 CollectiveSpin-WaveDynamicsinArraysofNanomagnets 58 7. MagnetizationDynamicsinSingleNanomagnets 64 7.1 Cavity-EnhancedMagneto-OpticalMeasurementsofPicosecond DynamicsofSingleNanomagnets 64 7.2 UltrafastThermalSwitching,Relaxation,andPrecessionofIndividual FerromagneticDisks 67 7.3 EffectsofMagneticGroundStatesonMagnetizationDynamics inSingleNanodisk 68 7.4 LargeAmplitudeMagnetizationDynamicsinaSingleNanomagnet 69 7.5 DetectingSingleNanomagnetDynamicsinVaryingMagnetostatic Environment 70 8. MagneticVortexandDomainWallDynamics 71 9. Time-DomainCoherentControlofPrecessionalDynamics 79 9.1 CoherentSuppressionofPrecessioninMagneticThinFilms 80 9.2 CoherentSuppressionofPrecessioninMicroscaleThin-FilmElement 83 9.3 CoherentSuppressioninMagneticMicrostrips 85 10. Time-DomainPrecessionalSwitching 86 11. SummaryandFutureDirections 92 Acknowledgments 94 References 94 1. GENERAL INTRODUCTION Magnetismisanoldsubjectwhoseorigingoesbacktoabout600BC [1]. Since its early discovery, magnetism has been used to the benefit of humansocietystartingfromitsuseinsurgerytotheuseofcompassfornav- igation.Overtheyears,magnetismhasseendiscoveryofmanyfundamental phenomenaandcontributedmanymodern-daytechnologiesinelectromag- neticsindustry,healthscience,andmorerecentlyinminiaturizedsolid-state devicesincludingmagneticdatastorageandmemorydevices.Themodern Time-DomainStudyofMagnetizationDynamics 3 magnetismhasitsorigininthebeginningofnineteenthcentury,whichbegan withtheseminalworksbyOersted,Ampere,Gauss,Biot-Savart,Faraday,and Lorentz, which formed the basis of magnetostatics and magnetodynamics. Based upon these works, Maxwell [2] in 1861–1862 formulated the well- knownMaxwell’sequationsunifyingelectricity,magnetism,andoptics. Magnetic domain theory was developed in 1906 by Weiss [3], who suggestedthatalargenumberofatomicmagneticmomentsarealignedpar- allelineachdomain.Weissexplainedthespontaneousalignmentofatomic momentwithinaferromagnetic materialby Weiss’smeanfield theory.Ifa system is in a single-domain state in equilibrium and the spins rotate uni- formly during reversal, then it can be described by a macrospin model. Quasisingle-domain systems may reverse by inhomogeneous modes, such ascurling,fanning,buckling,andbytheformationof“C,”“S,”andvortex states [4,5]. The simplest classical model describing single-domain systems with coherent rotation was developed by Stoner and Wohlfarth [6] and is commonly referred to as Stoner–Wohlfarth model. The aim of this model istoanalyticallycalculatetheequilibriumdirectionsofthemagnetizationfor a given anisotropy and a given applied field and its history. Further, for a magnetic field applied along a given direction, one can calculate the field value at which the magnetization reverses. As spatial variation of magneti- zationisignoredinthismodel,theexchangeenergydoesnotplayaroleand the magnetic switching is governed by the interplay between the Zeeman energy and the effective anisotropy. In 1935, Landau and Lifshitz [7] gave a theory of the dispersion of magnetic permeability in ferromagnetic body andpredictedanequationofmotiondescribingprecessionofmagnetization. TheLandau–LifshitzequationwaslatermodifiedbyGilbert[8],wherethe original damping term was replaced by a dimensionless Gilbert damping term. In 1946, Griffith [9] experimentally observed the ferromagnetic res- onance(FMR)forthefirsttime.In1948,Kittel[10]derivedtheformulafor theFMRfrequencyintermsofexternalmagneticfieldandtheinternalmag- netic parameters famously known as Kittel formula. Today,withtheinventionofvariousnewmagneticmaterials,synthetic structures, micro- and nanostructures, and metamaterials, magnetism has comealongwayandfoundapplicationsinarangeofmultidisciplinaryfields inmodernandfuturenanotechnologieslikenonvolatilemagneticmemory [11,12],magneticstoragemedia[13],magneticrecordingheads[14],mag- netic resonance imaging [15], and biomedicine and health science [16,17]. Morerecently,emergingtechnologiesareproposedinthefieldsofspinlogic [18,19], spin-torque nano-oscillators (STNOs) [20], and magnonic 4 AnjanBarmanandArabindaHaldar crystals [21]. The new technologies demand the invention of new material properties,whichmaynotalwaysbepossibletoachieveinasinglematerial inthebulkorthin-filmform.Instead,structuringofknownmaterialsinone andtwodimensionsatvariouslengthscalesandexploitingdynamicalmag- netic properties over various time scales may potentially offer the desirable material properties. An existing example is the patterned magnetic media, which uses ordered arrays of lithographically patterned two-dimensional arraysofbits,andthemagneticswitchingbehaviorsofsuchsystemsinclud- ing switching field distribution have been thoroughly studied. An essential criterion has been to eliminate magnetostatic interaction (crosstalks) betweentheindividualbitsfortheapplicationinpatternedmagneticmedia. Thesamesystemmaybeusedtotransmitmagneticexcitationsintheformof collective long wavelength spin waves as information carrier in magnonic crystals,whentheindividualmagneticelementsarestronglymagnetostatically coupled.Forvariousapplications,explorationofavarietyofnewphenomena isrequiredandthisrangesfromslowerprocessessuchasdomainwalldynamics andmagneticvortexdynamicstofasterprocessessuchasspin-wavepropaga- tion and localization and ultrafast demagnetization and relaxation. This also introduces magnetic structures at various length scale such as nanodots, microdisks, andfinally magnetic nanowires andnanostripes. Thekeychallengestoinvestigateandtoapplythephysicalphenomenon mentioned above are the synthesis or fabrication of high quality magnetic materialsandtheircharacterization.Technologydemandsfabricationofmag- neticultrathinfilmsandmultilayers(MLs)withhighsurfaceandinterfacequal- ities.Applicationsinvariousmagnetoelectronicandmagnonicdevicesrequires the fabrication of nanomagnets with narrow size dispersion arranged in an orderedarrayoveramacroscopiclengthscale.Theseledtothedevelopment ofanumberof“top-down”and“bottom-up”approachesinnanofabrication methodsandmorerecentlyacombinationofthetwo.Whilethebottom-up approachmainlyreliesuponsolutionphasecolloidalchemistry[22]andelec- trochemistry using different templates such as track-etched polymer [23], anodicalumina[24],anddiblockcopolymermembranes[25],thetop-down approachreliesprimarilyonphysicalprocesses.Thisincludesdifferentkindsof lithographictechniquessuchasphotolithography[26],electronbeamlithog- raphy (EBL) [27], deep ultraviolet lithography (DUV) [28], X-ray lithogra- phy [29], interference or holographic lithography (IL) [30], nanoimprint lithography(NIL)[31],andionbeamlithography(IBL)[32].Scanningprobe lithography[33],stepgrowthmethods[34],shadowmasks[35],andlaseror ionirradiation[36]arealsoverypromisingtechniques. Time-DomainStudyofMagnetizationDynamics 5 The quasistatic and ultrafast magnetization dynamics of magnetic thin films,multilayers,andnanostructuresaredifferentfromtheirbulkcounter- parts.Magnetizationdynamicsofthesesystemsstronglydependsupontheir staticmagnetizationstates,whichdependnotonlyontheirintrinsicmaterial parameterssuchasexchangestiffnessconstant,saturationmagnetization,and magnetocrystallineanisotropy,butalsoontheirphysicalstructuresaswellas theexternalparameterssuchasthestrengthanddirectionofthebiasmagnetic field. To study the quasistatic and ultrafast dynamic properties of nanomagnets, different kinds of sensitive characterization techniques have been developed in last few decades [37]. Magnetic force microscopy (MFM) [38] and Lorentz force microscopy [39] are two such examples, which are now extensively used to map the gradient of the stray magnetic fieldandthesamplemagnetization,respectively,withaspatialresolutionbet- terthan10nm.ForMFM,thecontrastoftheimagescomesfrommagnetic forcebetweenthescanningmagnetictipandthegradientofthestraymag- neticfromthesample.Ontheotherhand,thedeflectionoftheaccelerated electrons by Lorentz force after transmitting through thin magnetic speci- menscreatesthemagneticcontrastincaseofLorentzmicroscopy.However, it is not straightforward to extract quantitative information directly from either of these imaging techniques. Electron holography [40] is another imagingtechniquebasedupontheelectroninterference,bywhichtheampli- tude and phase information of the spin configurations and stray magnetic fields can be mapped with a very high spatial resolution down to 2nm. Magneto-optical Kerr effect (MOKE) microscopy [41] is an old technique and is widely used to map the sample magnetization with a sub-mm spatial resolution.Thephotoemissionelectronmicroscopy(PEEM)[42]isaform ofX-raymicroscopyandhasafarbetterspatialresolutionthanvisiblelight imaging. Spin-polarized low-energy electron microscopy (SPLEEM) [43], scanning electron microscopy with polarization analysis (SEMPA)[44], spin-polarizedscanningtunnelingmicroscopy(SP-STM)[45],andballistic electronmagneticmicroscopy(BEMM)[46]areotherimagingtechniques, whichgiveexcellentspatialresolutionof10nmorbetter.Thesetechniques usethespin-dependenttransmission,scatteringortunnelingofelectronsfor imagecontrast.However,despitehavingverygoodspatialresolution,allthe abovetechniquessuffer frompoorormoderatetemporalresolution. Subsequently,differentkindsofexperimentaltechniqueshaveemerged to investigate fast magnetization dynamics of magnetic thin films and nanostructures. The conventional FMR [47] and vector network analyzer-based broadband ferromagnetic resonance (VNA-FMR) [48] 6 AnjanBarmanandArabindaHaldar techniquesareveryefficienttomeasurethehigh-frequencymagneticreso- nance,permeability,andlossfromMHztotensofGHzregimelimitedonly by the instrumental bandwidth with a very good spectral resolution. Later, Tamaruetal.[49]developedthespatiallyresolvedFMRtoimageresonant modeprofilesofconfinedmagnetic elements.Pulsedinductivemicrowave magnetometry (PIMM) [50] is an oscilloscope-based time-domain tech- niquetomeasurethemagnetizationdynamicswithtensofpicosecondtem- poral resolution. Brillouin light scattering (BLS) is based upon the inelastic lightscatteringfromspinwavesandotherquasiparticlesandisconvention- allyused to studythespinwavesin thewavevectordomain[51].Thefre- quencydispersionofthespinwaveswiththeirwavevectorcanbemeasured directlybyvaryingtheangleofincidenceoflightwithrespecttothesample planeusingthistechnique.Recentlyspace-resolvedandtime-resolvedBLS techniqueshavebeendevelopedtoobtainsub-mmspatialresolutionandfew ns temporal resolution [52]. The best spatiotemporal resolution is obtained from time-resolved magneto-optical Kerr effect (TRMOKE) micro- scope [53]. They are used to probe the ultrafast magnetization dynamics in time domain and can achieve tens of femtosecond temporal resolution limited only by the pulse width of the laser. The magnetoresistive methods[54]andX-raymicroscopy[55]alsohavethepotentialtoachieve very good spatiotemporal resolution similar to TRMOKE. Time-resolved scanning Kerr microscopy (TRSKM) is a variant of TRMOKE, which is used to image the time evolution of magnetization excited by a time- dependent magnetic field. Here,wewillreviewthetime-domainstudyofmagnetizationdynamics inmagneticthinfilmsandnanostructures.Theremainingpartofthereview will be divided into 11 subsections. In Section 2, we will describe the backgroundtheoryofmagnetizationdynamics.InSection3,wewillrevisit the development of TRMOKE experiments from early 1990s to cater the need of various measurement systems and properties starting from funda- mental science to industrial needs. We will discuss some milestone instru- mental development and investigation of new phenomena using this technique.InSections4–9,wewilldescribethetime-domainmeasurements of precessional dynamics in some specific and important magnetic systems. This includes microscopic elements (Section 4), magnetic multilayers (Section 5), magnetic nanodot arrays (Section 6), single nanomagnet (Section 7), and magnetic vortex and domain wall dynamics (Section 8). InSection9wereviewthecoherentsuppressionofmagnetizationdynamics usingmagneticfieldpulseshaping,andinSection10wereviewtheprogress Time-DomainStudyofMagnetizationDynamics 7 inprecessionalswitching.Finally,weconcludeanddiscussthefuturedirec- tions in the study of time-domain magnetization dynamics (Section 11). 2. THEORETICAL BACKGROUND 2.1. Time Scales of Magnetization Dynamics Magnetization dynamics can occur over a wide range of time scale. Figure 1.1 shows various kinds of magnetization dynamics with their characteristictimescales[56].Thetimescales(t)aredeterminedbytheinter- actionenergies(E)viaHeisenbergrelationt¼h/E.Thefastestprocessisthe fundamental exchange interaction, which occurs within 10fs. The spin– orbit coupling and spin-transfer torque occur in the time scale of 10fs– 1ps. Laser-induced ultrafast demagnetization occurs within few hundreds offs.Thefastremagnetizationtimefollowingtheultrafastdemagnetization covers the time scale of 1–10ps. The magnetic writing which is done via reversalofspinhasatimescaleoffewpstofewhundredsofps,whereasvor- texcoreswitchingoccursfromfewtensofpstonstimescale.Theprecession of magnetization occurs within few ps to few hundreds of ps whereas the dampingassociatedwithmagnetizationprecessionoccursfromsub-nstotens Figure1.1 Characteristictimesscalesofvariouskindsofmagnetizationdynamics.

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