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Sn Organotin Compounds: Part 18 Organotin-Nitrogen Compounds R3Sn-Nitrogen Compounds with R = Methyl, Ethyl, Propyl, and Butyl PDF

311 Pages·1990·6.665 MB·English
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Preview Sn Organotin Compounds: Part 18 Organotin-Nitrogen Compounds R3Sn-Nitrogen Compounds with R = Methyl, Ethyl, Propyl, and Butyl

2 He I 10 Ne I 18 Ar I 36 Kr I 54 Xe I 86 Rn I H.'31 ~ I 2 5 6 7 8 a I H 9 F 17 CI 35 Br 53 I 85 At8 3 9 10 II 12 71 8 o 16 S 34 Se 52 Te 84 Po 71 Lu 103 Lr 7 N 4 IS P 16 33 As 17 51 Sb 18 83 Bi 19 70 Yb 102 No 71 6 C 14 14 Si 15 32 45 Ge 50 Sn 46 82 Pb 47 69 Tm 101 Md 71 bers 5 B 13 13 AI 35 31 Ga 36 49 In 37 81 TI 38 68 Er 100 Fm 71 ~- m m Nu 30 Zn 32 48 Cd 33 80 H34 g 67 Ho 99 Es 71 yste 60 61 62 71 n S 29 Cu 47 Ag 79 Au 66 Dy 98 Cf meli 57 65 68 71 e G 28 Ni 46 Pd 78 Pt 65 Tb 97 Bk with th 27 Co 58 45 Rh 64 77 Ir 67 64 Gd 96 71 Cm nts 59 63 66 7! me 26 Fe 44 Ru 76 Os 63 Eu 95 Am e the El 25 Mn 56 43 Tc 69 75 Re 70 62 Sm 94 Pu 7! Table of I I 24 Cr 52 42 M53 0 74 W 54 61 Pm 93 Np 71 dic 48 49 50 71 55 erio 23 V 41 Nb 73 Ta 105 60 Nd 92 U P 22 Ti 41 40 Zr 42 72 Hf 43 104 71 59 Pr 91 Pa 51 21 Sc 39 39 Y 39 57** La 39 89*** 40 Ac 58 Ce 90 Th 44 1 H 2 3 4 li 20 26 Be II 12 Mg27 21 Na 19 * 20 K 22 Ca 28 37 38 Sr 29 24 Rb 56 55 Ba 30 Cs 25 87 88 Ra 31 25a Fr *Lanthan ides 39 ** Actin ides * * ):> .. '"' .. ~ Q :::r CI) c;) ;; ~ 'OJ" r '" ;; 00" .r Ie CI) " .. c " :::r CI) ~ is.: CI) ... "" ,.. <> n c ~ Gmelin Handbook of Inorganic and Organometallic Chemistry 8th Edition Gmelin Handbook of Inorganic and Organometallic Chemistry 8th Edition Gmelin Handbuch der Anorganischen Chemie Achte, v6llig neu bearbeitete Auflage PREPARED Gmelin-Institut fUr Anorganische Chemie AND ISSUED BY der Max-Planck-Gesellschaft zur Forderung der Wissenschaften Director: Ekkehard Fluck FOUNDED BY Leopold Gmelin 8TH EDITION 8th Edition begun under the auspices of the Deutsche Chemische Gesellschaft by R. J. Meyer CONTINUED BY E. H. E. Pietsch and A. Kotowski, and by Margot Becke-Goehring i Springer-Verlag Berlin Heidelberg GmbH 1990 Gmelin-Institut fUr Anorganische Chemie der Max-Planck-Gesellschaft zur F6rderung der Wissenschaften ADVISORY BOARD Dr. G. Breil, Chairman (Ruhrchemie AG, Oberhausen-Holten), Prof. Dr. K. Dehnicke (Philipps Universitiit, Marburg), Prof. Dr. N. N. Greenwood (University of Leeds), Prof. Dr. H. Grunewald (Bayer AG, Leverkusen), Prof. Dr. H. Harnisch (Hoechst AG, FrankfurtiMain-H6chst), Prof. Dr. H. N6th (Universitiit Munchen), Prof. Dr. H. Offermanns (Degussa AG, FrankfurtiMain), Prof. Dr. G. zu Putlitz (Universitiit Heidelberg), Prof. Dr. A. Rabenau (Max-Planck-Institut fUr Fest k6rperforschung, Stuttgart), Prof. Dr. A. Simon (Max-Planck-Institut fur Festk6rperforschung, Stuttgart), Prof. Dr. Dr. h. c. mult. G. Wilke (Max-Planck-Institut fUr Kohlenforschung, MUlheim/ Ruhr), Prof. Dr. H. Zacher (Priisident der Max-Planck-Gesellschaft, Munchen) DIRECTOR DEPUTY DIRECTOR Prof. Dr. Dr. h. c. Ekkehard Fluck Dr. W. Lippert CORRESPONDENT MEMBERS OF THE SCIENTIFIC STAFF Dr. P. L. Bayless, Dr. A. W. Frank, Dr. V. Haase, Dipl.-Ing. G. Kirschstein, Dr. U. Kruerke, Dr. G. P. Richter, Dr. K. Rumpf EMERITUS MEMBER OF THE INSTITUTE Prof. Dr. Dr. E. h. Margot Becke CORRESPONDENT MEMBERS OF THE INSTITUTE Prof. Dr. Hans Bock Prof. Dr. Dr. Alois Haas, Sc. D. (Cantab.) GMELIN HANDBOOK CHIEF EDITORS Dr. K.-C. Buschbeck - Dr. H. Bergmann, J. FusseL, H. Hartwig, Dr. H. Katscher, Dr. R. Keirn, Dr. E. Koch, DipL.-Phys. D. KoscheL, Dr. A. Kubny, Dr. P. MerLet, Dr. E. SchLeitzer-Rust, Dr. F. A. Schroder, Dr. A. SLawisch, Dr. W. Topper STAFF Dr. G. Bar, D. BartheL, Dr. N. Baumann, Dr. K. Behrends, Dr. W. Behrendt, D. Benzaid, Dr. L. Berg, G. Borgerding, Dr. R. Bohrer, K. D. Bonn, P. Born-Heck, Dr. U. Busch, DipL.-lng. V. A. Chavizon, E. Cloos, DipL.-Phys. G. Czack, DipL.-Chem. H. Demmer, DipL.-GeoL. R. Ditz, R. Dowi de it, DipL.-Chem. M. DroBmar, U. Duggen, DipL.-Chem. E. Duve, Dr. H.-J. Fachmann, Dr. J. Faust, B. Fischer, G. Funk, DipL.-Ing. N. Gagel, Dr. U. W. Gerwarth, DipL.-Phys. D. Gras, DipL. BibL. W. Grieser, Dr. I. Haas, R. Hanz, Dr. R. Haubold, DipL.-Min. H. Hein, A. Heise, H.-P. Hente, H. W. Herold, U. Hettwer, G. Hoell, Dr. G. Hones, Dr. W. Hoffmann, G. Horndasch, Dr. W. Huisl, B. Jaeger, Dr. R. Jotter, Dr. J. von Jouanne, DipL.-Chem. P. Kampf, Dr. B. Kalbskopf, DipL. Chern. W. Karl, H.-G. Karrenberg, DipL.-Phys. H. KeLler-Rudek, B. Kirchner, DipL.-Chem. C. Koeppel, R. Kolb, Dr. M. Kotowski, E. Kranz, DipL.-Chem. I. Kreuzbichler. Dr. W. Kurtz, M. Langer, Dr. B. Leduc, Dr. A. Leonard, H. Mathis, E. Meinhard, M. MeBer, C. Metz, K. Meyer, Dr. M. Mirbach, DipL.-Chem. B. Mohsin, Dr. U. Neu-Becker, K. Noring, DipL.-Min. U. Nohl, Dr. U. Ohms-Bredemann, Prof. Dr. W. Petz, I. Rangnow, DipL.-Phys. H.-J. Richter-Ditten, E. Ru dolph, G. Rudolph, DipL.-Chem. S. Ruprecht, Dr. B. Sarbas, Dr. H. Schafer, Dr. R. Schemm, Dr. D. Schioberg, P. Schleimer, V. Schlicht, DipL.-Chem. D. Schneider, DipL.-Min. P. Schubert, A. Schwarzel, Dr. B. Schwager, DipL.-Ing. H. M. Somer, Dr. C. Strametz, G. Strauss, Dr. G. Swoboda, M. Teichmann, Dr. D. Tille, DipL.-Ing. U. Vetter, H.-M. Wagner, DipL.-Phys. J. Wagner, R. Wagner, Dr. E. Warkentin, Dr. C. Weber, K. Weil, Dr. A. Wietelmann, Dr. M. Winter, Dr. B. Wobke, K. Wolff GMELIN ONLINE EXECUTIVE MANAGER HEAD OF DEPARTMENT Dr. R. Deplanque Dr. P. Kuhn, Dr. G. Olbrich STAFF Dr. R. Baier, Dr. B. Becker, DipL.-Chem. E. Best, Dr. H.-U. Bohmer, DipL.-Phys. R. Bost, Dr. A. Brandl, Dr. R. Braun, DipL.-Chem. R. Durban, Dr. A. Kirchhoff, DipL.-Chem. H. Kottelwesch, W. Korba, Dr. M. Kunz, Dr. A. Nebel, DipL.-Chem. R. Nohl, Dr. B. Rempfer, U. Tolle, DipL.-Ing. H. Vanecek Organometallic Compounds in the Gmelin Handbook The following listing indicates in which volumes these compounds are discussed or are referred to: Ag Silber B 5 (1975) Au Organogold Compounds (1980) Be Organoberyllium Compounds 1 (1987) Bi Bismut-Organische Verbindungen (1977) Co Kobalt-Organische Verbindungen 1 (1973). 2 (1973). Kobalt Erg.-Bd. A (1961). B 1 (1963). B 2 (1964) Cr Chrom-Organische Verbindungen (1971) Cu Organocopper Compounds 1 (1985). 2 (1983). 3 (1986). 4 (1987). Index (1987) Fe Eisen-Organische Verbindungen A 1 (1974). A 2 (1977). A 3 (1978). A 4 (1980). A 5 (1981). A 6 (1977). A 7 (1980). Organoiron Compounds A 8 (1985). A 9 (1989). Eisen Organische Verbindungen B 1 (partly in English; 1976). Organoiron Compounds B 2 (1978). Eisen-Organische Verbindungen B 3 (partly in English; 1979). B 4 (1978). B 5 (1978). Organoiron Compounds B 6 (1981). B 7 (1981). B 8 to B 10 (1985). B 11 (1985). B 12 (1984). B 13 (1988). B 14 (1989). B 15 (1989). B 17 (1990). Eisen-Organi sche Verbindungen C 1 (1979). C 2 (1979). Organoiron Compounds C 3 (1980). C 4 (1981). C 5 (1981). C 7 (1985). and Eisen B (1929-1932) Ga Organogallium Compounds 1 (1986) Ge Organogermanium Compounds 1 (1988). 2 (1989). 3 (1990) Hf Organohafnium Compounds (1973) Mo Organomolybdenum Compounds 6 (1990) Nb Niob B 4 (1973) Ni Nickel-Organische Verbindungen 1 (1975). 2 (1974). Register (1975). Nickel B 3 (1966). and C 1 (1968). C 2 (1969) Np.Pu Transurane C (partly in English; 1972) Pb Organolead Compounds 1 (1987). 2 (1990) Po Main Volume (1941) Pt Platin C (1939) and D (1957) Re Organorhenium 1 (1989). 2 (1989) Ru Ruthenium Erg.-Bd. (1970) Sb Organoantimony Compounds 1 (1981).2 (1981). 3 (1982). 4 (1986).5 (1990) Sc. Y. D 6 (1983) La to Lu Sn Zinn-Organische Verbindungen 1 (1975). 2 (1975). 3 (1976). 4 (1976). 5 (1978). 6 (1979). Organotin Compounds 7 (1980). 8 (1981). 9 (1982). 10 (1983). 11 (1984). 12 (1985).13 (1986). 14 (1987).15 (1988).16 (1988).17 (1989).18 (1990) present volume Ta Tantal B 2 (1971) Ti Titan-Organische Verbindungen 1 (1977). 2 (1980). Organotitanium Compounds 3 (1984).4 and Register (1984). 5 (1990) U Uranium Suppl. Vol. E 2 (1980) V Vanadium-Organische Verbindungen (1971). Vanadium B (1967) Zr Organozirconium Compounds (1973) Gmelin Handbook of Inorganic and Organometallic Chemistry 8th Edition Sn Organotin Compounds Part 18 Organotin-Nitrogen Compounds R3Sn-Nitrogen Compounds with R = Methyl, Ethyl, Propyl, and Butyl With 12 illustrations by Herbert Schumann and Ingeborg Schumann AUTHORS Herbert Schumann, Ingeborg Schumann Technische Universitiit Berlin FORNULA INDEX Bernd Kalbskopf, Uwe Nohl, Hans-Jurgen Richter-Ditten, Gmelin-Institut, Frankfurt am Main EDITOR Ulrich Kruerke, Gmelin-Institut, Frankfurt am Main i Springer-Verlag Berlin Heidelberg GmbH 1990 LITERATURE CLOSING DATE: 1988 IN SOME CASES MORE RECENT DATA HAVE BEEN CONSIDERED Library of Congress Catalog Card Number: Agr 25-1383 ISBN 978-3-662-09149-4 ISBN 978-3-662-09147-0 (eBook) DOl 10.1007/978-3-662-09147-0 This work is subject to copyright. All rights are reserved, whether the whole or part of the material is concerned, specifically those of translation, reprinting, reuse of illustrations, broadcasting, reproduction by photocopying machine or similar means, and storage in data banks. Under § 54 of the German Copyright Law where copies are made for other than private use, a fee is payable to "Verwertungsgesellschaft Wort", Munich. © by Springer-Verlag Berlin Heidelberg 1990 Originally published by Springer-Verlag Berlin Heidelberg New York London Paris Tokyo in 1990 Softcover reprint of the hardcover 8th edition 1990 The use of registered names, trademarks, etc., in this publication does not imply, even in the absence of a specific statement, that such names are exempt from the relevant protective laws and regulations and therefore free for general use. Preface The present voLume continues the series on "Organotin Compounds", which first appeared in 1975, and now comprises a collection of eighteen voLumes. The overall pLan of the series has been given in the preface of VoLume 1. The present Volume 18 begins the description of the mononucLear organotin compounds with tin-nitrogen bonds (Section 1.5.1). Treatment of organotin compounds with tin-suLfur, -seLenium, and -tellurium bonds appeared earlier in Sections 1.4.2 to 1.4.4 of VoLumes 9,1982, and 10, 1983. VoLume 18 describes triorganotin-nitrogen compounds containing onLy R3Sn groups with R = methyL, ethyL, n- and iso-propyL, and n-, iso-, sec-, and tert-butyL groups. Abbreviations and symboLs are expLained on pp. X/XI aLong with other remarks. We thank Prof. Dr. h.c. Ekkehard Fluck and his coworkers at the GmeLin Institute for their excellent cooperation. In particuLar, we thank Dr. ULrich Kruerke for his accurate and sympa thetic editing, Drs. Baker and Hockings for reading the English text, and Mr. Hans-Georg Karrenberg for drawing the numerous formuLas and moLecuLar structures. We thank Mrs. Ellen Redlinger for her meticuLous handling of the Literature index, and the members of the chemicaL department of the Library at the Technische Universitat Berlin for their assistance in searching and acquiring the references from the Literature. BerLin-Lichtenrade Herbert Schumann August 1990 Ingeborg Schumann

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