Proceedings of the 16th Annual Conference on Composites and Advanced Ceramic Materials, Part 2 of 2: Ceramic Engineering and Science Proceedings, Volume 13, Issue 9/10 PDF
Preview Proceedings of the 16th Annual Conference on Composites and Advanced Ceramic Materials, Part 2 of 2: Ceramic Engineering and Science Proceedings, Volume 13, Issue 9/10
Ceramic Proceedings SEPTEMBER-OCTOBER 1992 Proceedings of the 16th Annual Conference on Composites and Advanced Ceramic Materials Me1 I. Mendelson Program Chair January 7-1 0,1992 Cocoa Beach, FL Published by The American Ceramic Society 735 Ceramic Place Westerville, 4308 1-613 6 OH Copyright 0 1992 The American Ceramic Society ISSN 0 196-62 19 Executive Director Editor W. Paul Holbrook John B. Wachtman Director of Publications Production Assistant Linda S. Lakemacher Lori A. Kozey Committee on Publications: Delbert Day, chair; Richard Hommel; J.T. Adrian Roberts; David W. Johnson, Jr., ex officio; John B. Wachtman, ex officio; David Green, ex officio; W. Paul Holbrook, ex officio. Editorial and Subscription Offices: 735 Ceramic Place, Westerville, Ohio, 43081 -613 6. Subscription $69 a year; single copies $1 5 (postage outside U.S. $5 additional). Published bimonthly. Printed in the United States of America. Allow four weeks for address changes. Missing copies will be replaced only if valid claims are received within four months from date of mailing. Replacements will not be allowed if the subscriber fails to notify the Society of a change of address. CESPDK Vol. 13, NO. 9-10, pp. 571-1102, 1992 The American Ceramic Society assumes no responsibility for the statements and opinions advanced by the contributors to its publications, or by the speakers at its programs. The opinions expressed are not necessarily those of the Society, its trustees and officers, its staff, or its general membership. Copyright 0 1992, by the American Ceramic Society. Permission to photocop for personal or internal use beyond the limits of Sections 107 and 108 of the 'C.S. Copyright Law is granted b the American Ceramic Society for libraries and other users registered with the Eoprright Clearance Center, rovided that the fee of $2.00 per cop of each artice IS paid directly to CC8, 21 Con ress Street, Salem, MA Ol&O. The fee for articles published before 1991 is afso $2.00 per copy. This consent does not extend to other kinds of copying, such as copying for general distribution, for advertising or promotional purposes, or for creating new collective works. Requests for special permission and reprint requests should be addressed to the Reprint Dept., The American Ceramic Society (01 96-621 9/91 $2.00). Each issue of Ceramic Engineering and Science Proceedings includes a collection of technical articles in a general area of interest. These articles are of gr actical value for the ceramic industries and the general public. The issues are ased on the proceedings of a conference. Both American Ceramic Society and non-Society conferences provide these technical articles. Each issue is organized by an editor who selects and edits material from the conference proceedings. The opinions expressed are entirely those of the presentors. There is no other review prior to publication . Foreword The 16th Annual Conference on Composites and Advanced Ceramics was held in Cocoa Beach, FL, January 7-10, 1992. It was indeed an international conference, with ten countries represented: the United States, Japan, the United Kingdom, Denmark, Sweden, France, Germany, Canada, the Netherlands, and Italy. The conference was attended by 501 participants from universities, government, and industry, representing all sectors of the materials community-science, engineering, manufacturing, marketing, and sales. The highlights of the conference were the James I. Mueller Memorial Lecture, presented by Don Messier, on "High-Temperature Chemistry of Fibers and Composites," the plenary session on "Trends in Engineering Ceramics," the technical program covering topics, a panel discussion on "Legislative and 13 Policy Bases of Technology," and an exposition sponsored by industry. The technical program featured over 160 oral and poster presentations. These were organized into various session topics: ceramic reinforcements, composite interfaces, particulate and whisker composites, composite testinglevaluation, composite fracture/fatigue, composite processing and properties, functionally gradient materials, materials manufacturing, critical technologies, covalent ceramics/diamond films, and processing/structure/property relations in ceramics. The proceedings are organized by session topic as they appeared in the program, and contain over 100 papers from the conference. These papers were published in record time, due to the adoption of a new procedure at the meeting. The manuscripts were written prior to the conference, peer reviewed on site, and prepared in "camera-ready'' format. I would like to thank the authors and reviewers for adhering to strict deadlines, which enabled these proceedings to be published early, and Lori Kozey (ACerS Publications Department) for coordinating the on-site review. In addition, I would like to thank the ACerS Meetings Department and the 1992 Cocoa Beach Program Committee, who assisted me in organizing the meeting. They include John Petrovic for the plenary session, Ron Barks for the Business of Technology panel discussion, Victor Greenhut and his evaluators for determining the "best paper" awards, and the session chairs. Me1 I. Mendelson Program Chair, Engineering Ceramics Division ... 111 Editor's Note: Proceedings of the 16th Annual Conference on Composites and Advanced Ceramic Materials appear in both this issue and Ceramic Engineering and Science Proceedings, Volume 13, Number 7-8. 16th Annual Conference on Composites and Advanced Ceramic Materials Composite Processing Reinforced Si3N4 Matrix Composites Formed by the Directed Metal OxidationPro cess........................................ 573 W.B. Johnson Fabrication of ZnObletal Matrix Composites by Oxidation of LjquidZn ........................................ 581 Alloys D.W. Yuan and G. Simkovich Synthesis of Composites In Situ Using Displacement Reactions ...... 5% C.H. Henager, Jr., J.L. Brimhall, and J.P. Hirth Process for the Fabrication of Ceramic Fiber Reinforced Titanium . Aluminide ............................................. 605 I. Horsfall and S.J. Cundy Preparation of Carbon Fiber Reinforced Composite by Impregnation ......... with Perhydropolysilazane Followed by Pressureless Firing 614 K. Sato, T. Suzuki, 0. Funayama, T. Isoda, and T. Itoh Sic Continuous Fiber Reinforced Si,N, by Infiltration and Reaction Bonding ............................................... 622 J. Brandt, K. Rundgren, R. Pompe, H. Swan, C. O’Meara, R. Lundberg, and L. Pejryd .................... Slurry Infiltration of 3-D Woven Composites 632 S.-M. Sim and R.J. Kerans Effect of Solid Particles Addition in Sol-Gel Processing of Ceramic ....................................... Matrix Composites 642 H.-K. Liu and A. Parvizi-Majidi Whisker ComDosites ................... Silicon Carbide Whisker Reinforced Alumina 653 B.J. Wrona, J.F. Rhodes, and W.M. Rogers V Green Processing Effects on Sic Whisker Textures in Alumina Body Matrix Composites ....................................... 661 M.S. Sandlin and K.J. Bowman Fracture Behavior of Sic Whisker Reinforced A1203w ith Modified .............................................. Interfaces 669 T.E. Sleyer and K.T. Faber Effects SIC Whisker Treatments on the Performance of SIC of ......................... Whisker/Alumba Matrix Composites 678 D. Qi and R.T. Coyle Property Optimization of A1203D ouble Reinforced with ZrO, and ........................................... SiCWhiskers 688 P.K. Mehrotra and D.P. Ahuja Boron Carbide Whisker and Platelet Reinforced Ceramic Carbide Matrix Composites ....................................... 6% J. Liu, P.D. Ownby, and S.C. Weaver ............. Fabrication of Sic Whisker Reinforced Sic Ceramics 704 K. Miyahara, T. Watanabe, S. Koga, and T. Sasa Indentation Fracture Silicon Carbide Whisker Reinforced Silicon of Nitride Ceramic Matrix Composites .......................... 712 AG. Solomah and L. Esposito Whisker Growth and Composite Fabrication in the Si,N4-C System ... 722 H. Wang and G.S. Fischman Microstructure, Strength, and Toughness of Si,N,SiC Whisker ............................................ Composites 732 E. Champion, P. Goursat, J.L. Besson, V. Madigou, M. Monthioux, and P. Lespade ComDosite Properties Synthesis, Characterization, and Tensile Strength of CVI C/SiC, ...................... SiCBiC, SiC/B4C, and C/B4C Composites 743 M.A. Kmetz, J.M. Laliberte, S.L. Suib, and F.S. Galasso Effect of Test Temperature, Oxygen Attack, Thermal Transients, and Protective Coatings on Tensile Strength of Silicon Carbide Matrix Composites ............................................ 752 D.A. Woodford, D.R. Van Steele, J. Brehm, and J.E. Palko Strength of Nicalon Fiber Reinforced Glass-Ceramic Matrix Composites After Corrosion with NQO, Deposits ............... 760 S.-W. Wang, R.W. Kowalik, and R. Sands vi Mechanical Characterization of Unidirectional Carbon/Carbon ...................... Composites for Engine Valve Application 770 A.V. Kerkar, E.D. Kragness, and R.W. Rice .......................... Fiber-Reword Al,Ti Composites 788 J. Farraro, N.S. Stoloff, and M. Otsuki Mechanical Properties of Layered and Laminated Ceramic Matrix CompositeSystem s....................................... 7% T.L. Jessen, B.A. Bender, and D. Lewis I11 Effect Sustained High-Temperature Exposure on the Mechanical of ....................... Properties of Nicalon/&03 Composites 804 A.S. Fareed, B. Sonuparlak, P.A. Craig, and J.E. Gamier Covalent Ceramics and Diamond Films Covalent Ceramic Materials Thin Films and Coatings .......... as 821 R.F. Davis Oxidation Kinetics CVD Silicon Carbide and Silicon Nitride ...... 836 of D.S. Fox New 11-JY-V, Family of Periodic Compounds Synthesized Under High Pressure .......................................... 844 T. Endo, H. Takizawa, and M. Shimada ProcessindStructureProDerty Relationships Microstructures and Interfaces in A1203-5 wt% Al CMC Synthesized ............... by Plasma Sintering of Attrition-Milled Precursors 855 S.H. Kim and S.N. Sinha of Composite ProcesSing on the Performance of Effects .....................C.a.r.b.o.n. ... Fiber/Glass Matrix Composites 863 D. Qi and C.G. Pantano Tape Cast A1203/2r02C omposite Laminates ................... 873 K.P. Plucknett, C.H. Cgceres, F. Fremont, and Wilkinson D.S. Microcracking and Elastic Moduli in Unidirectional Reductions Nicalon-CAS Composites Under cyclic Fatigue Loading ........... 881 P.G. Karandikar and T.-W. Chou High-Temperature Exposure BN-Coated Polymer-Derived Sic ...o.f .............................. Fiber/ZrTiO, Composites 889 B.A. Bender, T.L. Jessen, R.P. Ingel, and D. Lewis I11 vii Matrix Cracking Behavior in Fi’ber and Whisker Reinforced Ceramic Composites ............................................ 897 R.N. Singh Development of pSi,N, for Self-Reinforced Composites ........... 907 D.E. Wittmer, D. Doshi, and T.E. Paulson SIMS-Auger and Thermal Conductivity Characterization of SiSiC .............................................. Materials 918 E. Scafk, G. Grillo, L. Fabbri, and Vittori V. ....................... Thermal Stability of Yttrium Numinates 929 T. Mah, Kk Keller, and R.J. Kerans .............. Pseudo-Binary Eutectic Between Y4A1209 and Y203 930 T. Mah and D. Petry Effects of the Interfaces Between Floes in Wet Processed Zirconia- Alumina on the Mechanical Properties of Sintered Composites ...... 931 K.J. Konsztowicz and R. Langlois ........ Cyclic Fatigue Life and Crack Growth Behavior of Alumina 939 S. Raghurarnan, K-Y. Hour, and J.F. Stubbins In Situ Observation of Crack Growth in Glassy Alumina at ... 948 1275°C M. Heinzelmann, J.E. Ritter, and K. Jakus Application of Indentation Strength Method to R-Curve .......................................... Measurements 957 S.V. Nair, P.Z.Q. Cai, and J.E. Ritter ............... Hardness and Toughness of HIP’ed Silicon Nitride 966 R. Berriche, R.T. Holt, S.N. Kurnar, and T.M. Maccagno Tensile Testing in the Development of Processing Methods for High- ....................... Strength/High-Reliability Silicon Nitride 978 M.R. Foley and V.K. Pujari Microstructure and Oxidation Behavior of HIP’ed Silicon Nitride .... 991 K.P. Plucknett and M.H. Lewis Strength and Flaw Elimination Assessment in Tape Cast Ceramic ............................................ Laminates 10oO R. Ham-Su and D.S. Wilkinson .................... Anelastic Recovery in Crept Silicon Nitride 1008 S. Haig, W.R. Cannon, and P.J. Whalen Relationships Between Toughness and Microstructure of Reaction ........................................... BondedSi3N 1024 A. Lightfoot, J. Sigalovsky, and J.S. Haggerty ... Vlll Effect of Silicon Carbide Addition on a Self-Reinforced Silicon Nitride ............................................... 1032 C.J. Hwang, K. Yang, D. Bearnan, and H. Klassen Development and Structural Stability of a Rare Earth Titanate Powder .............................................. 1040 O.G. Bailey, D.P. Matheis, and G.S. Fischman .................... Cavitation in Thick Joints: A Special Case 1048 M.H. O’Brien Codispersion of Mullite and Wollastonite in Aqueous ... 1058 Suspensions R. Bryden, K.J. Konsztowicz, W.F. Caley, and P.W. Kingston ........... Novel Technique for Surface Modification of Ceramics 1066 2. Fathi, A.D. Cozzi, and D.E. Clark Use of AlOOH Gel in Microwave Joining of Alumina ............ 1073 S. A-Assafi and D.E. Clark Polymethyl Methacrylate Binder Removal from Alumina by Microwave Heating ..................................... 1081 E.H. Moore and D.E. Clark ........... Processing of Mullite Using Microemulsion Technology 1089 G. Klassen and G. Fischman Improved Technique for Young’s Modulus Determination by Flexural Resonance ..................................... 1094 E. Scare, L. Fabbri, G. Grillo, and L. Di Reese ix Ceramic Engineering and Science Proceedings(cid:13)(cid:10) John B. Wachtman(cid:13)(cid:10) © 1992 The American Ceramic Society(cid:13)(cid:10) Composite Processing
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