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PRESERVATION OF FRUITS AND VEGETABLES |>RESERVATION OF FRUITS AND VEGETABLES BY GIRDHARI L.\L, Ph.D. (Lond.), D.I.C, (Lond.) AsSOrTANT DntBCTOR, DrVTSlON OF FRITT TKCKSOLOCV CBJ.TRA1. FOOD TECBNOLOGICAI. RBIBABCI' '• — - ^ ^ j MYbOith r ^ D A P P A . M.A. (Hou^.}. Madras. Ph.D. (Bristol), A.R.I.C. (Lond.) SBMOR SctBNTmc OrncEs, DkvisoN cr FiBir TICIOIOIJOGT CxirTRAi. FOOD TsciccouxacAL RBCABCH IIMIIIIJIB, MYXmi- PRc I.. I\\NDO.\ (Horn.), Punjab ^t..-.:cR N ihNnnc OFTICKR, Diviiio.s OF OOY L".ENTK.\L too:) TBCHNOLOGICAI. RESKARC: .'t'SCMLB [XDIAN COUNCIL OF AGRICULTT R \T T?F<;F\RrH NEW DELHI Fmir^WNTED JANUARY 1950 REPRINTED DECEMBER 1967 Cluef Editor : C. G. RAGHAVA KURUP /Usisiant Editor : M. K. JAIX Production Officer : KRISHAN KUMAR ANGRAU 634.046 N60GIR Ace No. 11043 All Rights Rescued (C) J959 and 1967 by Indian Council of Agricultural Research A'ew Delhi Printed in India by V. Ananda Krishna Cliclty at Hoc & Co., Madras 1 and published by T. S. Prulhi, Under-Sccrctar>-, for the Indian Council of Agricultural Research, N'evv Delhi. FOREWORD FRUITS and vegetables are among the most important foods of mankind as they arc not only nutritive but are also indispensable for the maintenance of health. From tlie point of \ie\v of the agriculturist also, they are of great importance as he is assured of high rettims from tlieir cultivation even on a small area. The total estimated production of fruits in India is about 129 million mauuds, bul as a substantial quantity is wasted, only about one ounce per individual per day is the net availability. Thk contrasts markedly with tlic consumption in other advanced countries \\'hich ranges between 4 to 16 ounces per day. Development of horticulture \s-ill be uneconomical in a country- with poor communications and marketing facilities, unless the fruit and vegetable presenation industrj' keeps pace witli tlie de%elopmental work. Its progress in India has been rather slonv, mainly because of lack of adequate scientific knowledge about the various processes of food pre- sen'ation. It is, therefore, ver\- necessan' that this knowledge should be disseminated on a countrN-wide scale. It is only a hundred years since Pasteur's discovery of the microbes -which cause spoilage of food revolutionised the canning industr\' in the \Vest, But during this short period tlie industry has been de\eloped to such a degree of perfection that fruits, vegetables and other foods produced b\' any countr\- in any season arc available all over the \vorld at all times. Over 350 different kinds of canned foods are found in the market, and tlie total annual pack of die major producmg countries of the world is estimated at more than 15,000 million pounds. The production of canned fruits and vegetable products in the U.S.A.. alone is over 7 nulUon ions. The canning industry in India has yet to exploit its full poicntialities. A number of entrepreneurs have no doubt established modern plants for the manufacture of various food products, but considering the great scope which exists for the development of the industr\-, the pace of progress is not as fast as it should be. The Central Food Technological Research Institute, M\-sore, is striving hard to find solution for the problems which stand in the way of development of the industry-. The book Prescrvalion of Fruits and Vegetables is the outcome of long experimentation and study in which three of the senior officers* of the Central Technological Research Institute have been engaged. I congratulate them and the Indian Council of Agricultural Research for bringing out this valuable book. It embodies the results of the research conducted on various aspects of the preser\aUon of fruits and vegetables, and aims at providing practical guidance both to the cottage worker and the large-scale producer, fhe book will also be of great use to the Extension Workers and FOREWORD teachers as well as students in Home Science Colleges in popularising scientific methods of preparing fruit juices, squashes, cordials, jams, jellies, marmalades, pickles, etc., and of preserving seasonal vegetables. I am sure it •ivill serve a long-felt need for a comprehensive treatment of the subject and wll promote the interests of the horticulturists in the countrv. S. K. PATIL New Delhi iONisTER FOR FOOD AND AGRICULTURE October 20, 1959 GOVERNMENT OF INDIA * Designations indicated against llie names of the authors show their official position at the time of writing the chapters of the first edition. PREFACaE PRESERVATION of food in one form or the other has been practised in all parts of the \vorld since time immemorial, though scientific methods for it came to be developed only about a hundred years back. However, as in the . case of many other industries, technological progress in food preservation gained momentum mainly after the outbreak of the First World W^ar when supply of large quantities of vegetables, frtiits, meat, etc., had to be arranged for the armed forces. World War II pro\aded another strong impetus to the growth of the industry. The wide assortment of the canned products avail- able in the market and their easy portabilit)' have created a fast increasing demand for preserved foods. In many advanced countries today even the poorer sections of the population have become used to consuming canned or botded fnuts and vegetables as these are available all the year round, and arc often cheaper than even the fresh cortmiodities. Thus, an industry which has its beginning in the scarcity conditions of war, is now considered to be of perennial importance. It also assures a stable market to farmers and horticulturists, and enables them to expand their production without fear of a fall in demand. Fruit and vegetable preservation industry- is still in its infancy in this country. The total annual production of all kinds of preserved fruits and vegetables does not amount to more than Rs. 2 crores in value, and most of the products are too expensive for a majority of the people. Again, the preser\ed products consist mainly of jams and pickles which continue to be produced by traditional methods. Till only about 20 years ago, other well- known methods of preser\-ation, such as making of juices, squashes, cordials, jellies, marmalades, etc., -were confined only to a few larger industries. In the early thirties, the Indian Council of Agricultural Research financed a number of schemes under which a band of workers started pioneering work for the popularisation of these methods. It is a matter of great satisfaction that rapid progress has been made since then, and the production of fruit preserves of all types is now carried on even on cottage scale. One of the main difficulties in the way of the gro\vth of the fruit and vegetable preservation industry has been the inadequacy of knowledge of the modem methods and techniques of preservation. To overcome thb difficulty, the Central Food Technological Research Institute, Mworc, has been undertaking intensive studies and research on various aspects of pre- servation methods. Research ^^•orke^s in other parts of the countr>- have also been devoting attention to these problems. But most of the available know- ledge is scattered in scientific papers, departmental reports and other highly •O PREFACE technical publications. This information has to be disseminated on a country- wide scale so that full advantage of it can be taken by all those interested in the industr}\ To meet this need, the Indian Council of Agricultiural Research has brought out Preservation of Fruits and Vegetables which is a compre- hensive book on the subject. T h e authors. Dr. Girdhari Lai, Dr. G. S. Siddappa and Shri G. L. Tandon, who are senior officers of the Central Food Technological Research Insdtute, and are known for their experience and knowledge, have made the book highly useful by treating the subject in all its essential aspects in a simple and interesting st^'le. I congratulate them for this, and hope that the book ^^•ould meet the needs of Extension 'Workers, Home Science Colleges, manufacturers of preserved fruits and vegetables, and others interested in this subject. M . S. RANDHA\V'A New Delhi \ICE-PRESIDENT December 30, 1959 IXDL\N cotJXCiL OF AGRICULTURAL RESEARCH ACKNOWT^EDGEMENTS The authors are indebted to Dr. V. Subralimanyan, Director, Central Food Technological Research Institute, Mj-sore, for the help and guidance given by him in the preparation of this book, and for his permitting them to make use of unpublished research data. Through his courtesy a number of photographs of the machinery' and equipment in the Institute have also been reproduced in the book. They are grateful to Messrs Pure Products and Madhu Camiing, Ltd., Bombay, Central Hindustan Orange and Cold Storage Company Ltd., The Afetal Box Company of India, Ltd., Mather and Piatt Ltd., India, and Teg Products, Patiala, for permission to use pliotographs of their equipment. GIRDHARI L M , G. S, SlDD.A.PP.\ G. L. TAN-DON CONTENTS PAGE FOREWORD : 5 PREFACE 7 ^CH.\PTER(Da\NNIXG .\XD BOTTLING FRUITS .\KD VEGETABLES... 15 PRINCIPLES OF FOOD PROCESSING. CONTAINERS FOR PACKING. C H A P T E R 2. C O M M E R C L \ L C ; \ X X I N G •' i9_X FACTORY SITE. FACTORY BUILDING. W A T E R SUPPLY ANT)DRAIN.A.GE. SORTING AND GRADING. PEELING, CORING AND PITTING. Q \ N FILLING. H E A T PEN^TR.\TION IN CANS. COOLING. TESTING FOR DEFECTS. LABELLING, SORTING AND PACKING. - ' C T L - V F T E R ^ C O X T A I N E R S 38 T I N CONTAINERS. LACQUERING. MANLTACTURE OF Q \ N S . TESTING CANS. SIZES OF G \ N S . GUVSS CONTAINERS. CFLVPTERi^SYRUPS AND BRINES FOR a-VXXING 51 SUGAR S'i'RUPS. TESTING S'i'RUP STRENGTH. S'i'RUP CALCULATIONS. CHAPTER 5. CAN^NING FRUITS CO APPLES, APRICOTS. BANANAS. BLACK^ BERRIES. CHERRIES. FIGS. GRAPES. GRAPEFRUIT. GREENGAGE. GU.W.AS. JACKFRUTT. LTTCHIS. LOQUATS. MANGOES. ORANGES. PAPAYA. PEACHF^. PEARS. PIN-E- APPLES. PLUMS. BERRY FRUITS. CH.APTER C^Q,^L»;jNG;-JrTGETA£LE.S.... 71 ASPAR.\GUS. BEANS. BEAT. G \ B B A G E . CARROT. CAUUFLOW^ER, GRAM. MUSHROOM. O K R A (LMDY'S FINGER). PEAS. POTATO. TOM.\TO. TURNIP. CURRIED \'EGETABLES. CH.\PTER/7lsiiOILAGETl^e-e.\NNED'roODS ' ^ ^ 76 DISCOLOUR,\TION OF FRLTT PRODUCTS. COLOURING M A T T E R IN FRLTFS ANT) \'EGETABLES. DISCOLOLTIATION IN \'ARIOUS C-ANNED FOOD PRODUCTS. CORROSION AND PERFORATION OF TINPLATES. SPOILAGE BY MICRO-ORGANISMS. STORAGE LIFE OF CAN-NED FRLTTS AND VEGETABLES. 9 1 0 CONTENTS PAGE CHAPTER 8. FRUIT JUICES, SQUASHES AND CORDLU^ 84 EQurpME^•T FOR FRUIT JUICES. DOUBLE OPERATION. PULPING EQUIPMENT. DEAERATOR AND FLASH PASTEURIZER. FRUIT BEVER- AGES. GLARIFiaA.TION BY FREEZING. CLARIFICATION BY HEATING. PRESERVATION OF FRUIT JUICES. PASTEURIZATION^^^PRESERVAHON WTTH C H E I U C A L S . P R E S E R V A T I O N - B Y ADDITION OF SuG.A.R. P R E S E R - V.A.TION BY FREEZING. PRESERVATION BY DRITNG. PRESERVATION BY GAjiBO.v.^TiON. PRESERVATION BY FILTRATIO.V. O T H E R METHODS OF PRESERVATION. CHAPTER 9. FRUIT BEVERAGES } ' : . . V ' ... ... m s ) - SQUASHES AND CoRDL«.s. jLHCES.SvTiups. CARBONATED BEVERAGES. ' J U I C E CONCENTR.\TES. FRUIT JXHCE. POWDER. CHAPTER 10. FERMENTED. BEyERAGES 135 G R A P E W I N E . FERSiEJtavTioN. CHAMPAGNE. P O R T . MUSCAT. TOKAY. SHERRY. CIDER. PERRY. ORANGE W I N E . BERRY WIN-ES. 'CH.\PTER 1K]^^J^23EIXIES j«ID MARNMJL-UJES JAMS. F R U I T "PRESESSXD-^Y HSJci T R E A T ^ N T . PREPARING THE FRUIT FOR JAM-MAKING. JELLIES. EXTRACTIO.N OF PECTIN. STRAINING AND CLARIFICATION. T H E O R Y OF J E L L Y FORJIATION. STRENGTH O F PECTIN JELLIES. COOKING OF J E L L Y . PACKING. SEALING AND STERILI- ZATION. SOME TYPICAL JAMS AND JELLIES. JAJI-LIKE PRODUCTS. \L\RiL\i_^DEs. JAM MARIL\L.\DE. * CHAPTER 12. PRESERVES, OVN'DIES -VXD CRYST.\LLIZED FRUITS ... 172 PRELIMINARY PROCESSING. C O O U N G .^ND P.\CKING. CANDIED, GL.\CED .\ND CRYSTALLIZED FRUITS. SOME COMMON PREPAR-^WTIONS. CHAPTER 13. I P M A J P PRODUCX'> > '85 TOMATO JUICE. TOMATO PUREE. TOMATO PASTE. TOMATO COCKTAIL. TojiATO K E T C H U P . CHILI S.A.UCE. TOXIATO SAUCE. TOMATO SOUP. A'IICROBIOLOGY. V CHAPTER 14. CHUTNEYS, S.\UCES AND PICKLES ." — 202 CHUTNEYS. T H I N SAUCES. T H I C K SAUCES. PICKLES. PICKLING PROCESS. CAUSES OF SPOILAGE. VARIOUS PICKLES. CftVPTER 15. VINEG.AR 230 VINEGAR VARIETTES. J/IETHODS OF PREPARATION. POST-PRODUCTION PROCESSES. CHECKING SPOILAGE. CONTE^'TS 11 PAGE CHAPTER 16. DRYING OF FRUITS AND VEGETABLES ... .^/24I /,, SUN-DRYES'G. MECHANICAL DEHYDRATION. PROCESS VARLVTIOXS. PROCESSES FOR VEGETABLES. PACKING AND STORAGE. CH-APTER 17. BY-PRODUCT^ ... \ / 257 UTILIZING WASTE MATTER^ GitvvA CHEESE. O T H E R \^EGETABLES. X^ CiTRiTs BY-PRODUCTS. CH.;U>TER 18. ^LA^•UF.\CTURE OFvPECTIK 265 PECTIN FROM APPLES. PECTIN FROxr CITRUS FRUITS. PECTIN FROM O T H E R ^'IATERIALS. PECTIN PREPARATION. USES OF PECTIN. CH.APTER 19. W.\TER FOR A a\NNERY 2 7 3 , QjJALmES OF W A T E R . PROCESSING OF W A T E R . ANALYSIS OF W A T E R . ^ M A J O R MIN-ERAL CONSTITUENTS: ^B.\CTERiOLOGia\L EXAIIINATION. CHAPTER 20. FOOD COLOURS 281 CERTIFIED COLOURS. BANNED COLOURS. CHAPTER 21. Vrr.VMIIsS 288 PROCESSING AND \'^iTAxnNsK CHAPTER 22. LIMITS FOR USP OF PRESERV.^TIVES 292 HARDNESS OF ^V.\TER. Soire USEFUL D A T . \ . SOME CONSTANTS. DOMESTIC ME-ASURF-S. .\PPR\D1X I. REFERENCE TABLES ... ... ... -%,. ... 295 ! \ V - APPENDIX II. FRUIT PRODUCTS ORDER 1955 \ .Ti ' ^ ... ... 311 BIBLIOGRAPHY 355 T.ABLE FOR IMPERIAL TO METRIC CONVERSIONS 366 INTiEX 367 LIST OF ILLUSTRATIONS PAGE A battery of vertical retorts in a fruit and vegetable Preservation factory ... ... ... ... ... Frontispiece 1. Plan of a fruit preservation factory ... ... ... ... 20 2. Layout plan of a canning line 3. Layout plan of a juice plant 4. Preparation and grading of fruits in a canning factory 5. Peeling, pitting and coring knives ... 6. Filling cans wth syrup in a canning factory 7. Peeling, slicing and coring machines 8. Steam exhaust line in a canning factor)' 9. A double seamer in a canning lactory 10. Open batch-type exhaust, cooking and cooling tanks ... 11. Continuotis moving belt, exhaust, cooking and cooling tanks 12. Can reforming unit: Can body reformer 13. Vacuum can tester for double seam 14. Roller action of a double seamer ... 15. Double seam measurements 16. Can seaming technology: Graphic explanation of seams 17. Can reforming unit: flanger 18. Can reforming unit: M. B. IA double seamer 19. A Brix hydrometer for measuring syrup strength 20. A pocket refractometer for measuring syrup strength ... 21. Preparation of papaya fruit for canning 22. A small power-driven pineapple slicing machine 23. Power-driven potato peeler 24. Halving and burring machines 25. Burring machine for extraction of juice from oranges 26. Juice extraction room in Central Food Technological- Research Institute, Mysore 27. Laboratory screw tj-pe juice extractor 28. Screw type juice extractor 29. Grape crusher ... 30. A small hydraulic press ... 31. A basket press ... 32. Diagram of a laboratory flash pasteurizer 33. A.P.V. pulping machine ... 34. A hand operated juice filter press ... 35. Laboratory juice deacration imit ... 21 22 23 23 24 29 29 30 39 39 40 40 42 44 45 49 49 50 50 67 68 68 85 85 86 86 89 89 90 90 93 95 96 99 12 U S T OF nXUSTRATIOKS 13 36. Laboraton' flash pasteurizer ... ... ... ... 99 37. Deacrating and pasteurizing plant ... ... ... ... 100 38. Bottle washing machine ... ... ... ... ... 100 39. Vacuum operated bottle filling machine ... ... ... 117 40. S\xup mixing tank ... ... ... ... ... 117 41. Bottle filling machine (Sj-phon pipe filler) ... ... ... 118 42. An automatic filler (Asco filler) ... ... ... ... 118 43. Cro%\Ti corking machine ... ... ... ... ... 119 44. Bottle corking machine ... ... ... ... ... 119 45. A.P.Y. laboratory' two-stage fi^it juice concentration unit ... 120 46. Capsuling machine ... ... ... ... ... 133 47. Steam—jacketed jam boiling pans ... ... ... ... 133 48. Sharpies super centrifiige ... ... ... ... ... 134 49. Testing fi^it extract for pectin contents ... ... ... 156 50. Sketch of a jelmeter ... ... ... ... ... 157 51. Jelmeter test for pecdn content ... ... ... ... 158 52. Jelly thermometer ... ... ... ... ... 163 53. Flake Test: Condidon of jam or jelly flakes ready for pouring ... 163 54. Vinegar generator for quick process ... ... ... 237 55. Tomato crusher, pre-heating pans, pulpcr and cooking pans ... 243 56. .\naljtical and research laboratory-, Central Food Technological Research Institute, Mysore ... ... ... ... 243 57. .^ Home-made drier ... ... ... ... ... 244 58. A dehydration trolley being loaded ... ... ... 244 59. .\n experimental 3-trolley unit tunnel dehydrater {re-circulating, air-blast tjpe) for dehydration of fi-uits and vegetables ... 248 60. Circulating-air-blast n-pe funnel dehydrater ... ... 250 61. An electrically operated cabinet drier ... ... ... 261 62. Extraction of oil from oranges by using a plate with spikes ... 261 63. Two-roller mill for extraction of oil from citrus peels ... ... 262 64. Extraction of oil from oranges in a fruit juice factory- ... ... 262 CHAPTER 1 CANNING AND BOTTLING FRUITS AND VEGETABLES IT is a common axperience that fruits, vegetables, meats, and many otiier articles of food spoil rapidly unless specially cared for. Various methods for preserving these, such as pickling in salt or vinegar, drying, smoking, preserving in sugar or honey, etc., have been developed since time immemorial. But canning is comparatively a modem technique. It deve- loped under the stress of war conditions towards the close of the 18th centurj. During the Napoleonic wars, the French Government announced a pnzc of 12,000 francs for the discovery of a satisfactory method of preservation so that food could be transported to the fighting forces over long distances without spoiling. In 1810, Nicholas Appert. a Paris confectioner and.djstiller, invented a process for preserving foods in glass containers, took out a patent for his process, and won the prize. He also published a book cntided The^J Art of Preserving Animal and Vegetable Substances for Many Years which is the first kno^v'n work on modem canning. In honour of its discoverer, canning is still known as ' Appertiang'. w^^ Appert packed nis food in glass containers, added sufficient water to cover the food, placed the corks loosely on top and heated the containers in a \vater-bath to obtain a temperature of 190"—^212^. at the centre of the containers. The containers were finally sealed' air-tight by driving in the corks. By this method, he succeeded in preserving several kinds ^ of foods. He ascribed this preerving action to the exclusion of outside ^ir.^Gav-Lussac,. who studied Appert's process at the instance of tT^e French Gf^v^rn^TiLent, concluded that spoilage in foods was essentially a process of oxidation which could be prevented by the exclusion of air from the rftn^ainf-r- This hypothesis was universally accepted till the time of Louis Pasteur who provided correct explanation of the change through his discovery of microbes round about 1860. By his experiments on heat treatment, he proved that micro-organisms arejthe_real cause of spoilage,* and that by destroying these, foods can be preserved in suitable coritamers. He introduced the word ' Pasteurization '|which means heat-treatment of a food at a sufficientiy high temperature to kill the majority, though not all, of the micro-organisms thereby prolonging the normal keeping quality of that food^NTiat Appert did was to destroy, by heating, micro-organisms such as bacteria, moulds and yeasts present in food, \vatcr and air, \vhich were responsible for fermentation and decay, by .greycing their access to the food inside the container by sealing it hermeti^Il>-(-^/ In England, _Thoroas-.SnJdincrton. who Tiag~"pid;ed up the general principles of tiic" iHethod of Appert while travelling in France, was the 15

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