One-pot synthesis of 2-aminoquinoline-based alkaloids from acetonitrile PDF
Preview One-pot synthesis of 2-aminoquinoline-based alkaloids from acetonitrile
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry This journal is © The Royal Society of Chemistry 2012 Supporting Information One-pot synthesis of 2-aminoquinoline-based alkaloids from acetonitrile Takashi Tomioka*, Yusuke Takahashi, and Toshihide Maejima Department of Chemistry and Biochemistry, University of Mississippi, University, Mississippi 38677, USA [email protected] Table of Contents 1H and 13C NMR Spectra of Compounds.….…...……………………………………….S2 S1 Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry This journal is © The Royal Society of Chemistry 2012 N NH 2 1a 1HNMR,300MHz,CDCl 3 N NH 2 1a 13CNMR,75MHz,CDCl 3 S2 Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry This journal is © The Royal Society of Chemistry 2012 Cl N NH 2 1b 1HNMR,300MHz,CDCl 3 Cl N NH 2 1b 13CNMR,75MHz,CDCl 3 S3 Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry This journal is © The Royal Society of Chemistry 2012 MeO MeO N NH 2 1c 1HNMR,300MHz,CDCl 3 MeO MeO N NH 2 1c 13CNMR,75MHz,CDCl 3 S4 Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry This journal is © The Royal Society of Chemistry 2012 O O N NH 2 1d 1HNMR,300MHz,CDCl 3 O O N NH 2 1d 13CNMR,75MHz,CDCl 3 S5 Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry This journal is © The Royal Society of Chemistry 2012 F N NH 2 1e 1HNMR,300MHz,CDCl 3 F N NH 2 1e 13CNMR,75MHz,CDCl 3 S6 Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry This journal is © The Royal Society of Chemistry 2012 (Me) N N NH 2 2 1f 1HNMR,300MHz,CDCl 3 (Me) N N NH 2 2 1f 13CNMR,75MHz,CDCl 3 S7 Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry This journal is © The Royal Society of Chemistry 2012 N NH 2 1g 1HNMR,300MHz,CDCl 3 N NH 2 1g 13CNMR,75MHz,CDCl 3 S8 Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry This journal is © The Royal Society of Chemistry 2012 N NH 2 8a 1HNMR,300MHz,CDCl 3 N NH 2 8a 13CNMR,75MHz,CDCl 3 S9 Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry This journal is © The Royal Society of Chemistry 2012 N NH 2 8b 1HNMR,300MHz,CDCl 3 N NH 2 8b 13CNMR,75MHz,CDCl 3 S10
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