Microwave Synthesis: Chemistry at the Speed of Light PDF
Preview Microwave Synthesis: Chemistry at the Speed of Light
Microwave Synthesis Chemistry at the Speed of Light Brittany L. Hayes, Ph.D. Microwave Synthesis Chemistry at the Speed of Light by Brittany L. Hayes, Ph.D. opi 202 CER Phin silghss reseed. No paz ths pubeslon nay be reproduced “Sared in tetrew system, or transite ans fm or By a Printed HS Ex ooraoL “CRW Punching onus) ROR zON Marthesss, Nt: 28105 Contents Foreword Chap.or t-Inroducten te Microwevs Cori. Chap or 2- Solvents ‘Chap.or 3 - Chemical Roactons in the resonco and Absence ol Sok ‘enap:or¢ - Synthetic Appleatons, ‘Chap:er$ - Getting Started with malcrawave Syminoss Chaps 8 Microwave Safety Considerations, ‘Chap:er 7 - Microwave ardware Anerson Glossary Re‘ereroes Ire. 2a n es a7 15 181 4191 197 208 289 Foreword By Alan Katriteky, Ph.D. reactions can be accelerated by microwaves: additions, cyeloadditions, substitutions, elimina tions. fragmnentations..the list goes on. ‘This book, saitten by a practicing organic chem'st far practicing organtc chemis:s, shows how this powerful technique can be applied in laboratory situations, It utters advice on the selection of conditions. solvents, temperatures. t explains the manitold possibilities of modern instrumentation, andl prewieles a pensertl tool for the practieal application Of che technique to enhance the range 0! synthesis and the prorhuctivity ot synthetic chemists, Although microwaveenhanced organic. chemistry has been around since the mic-1980s, until recently, it trenuently utilized domestic microwave avers and co VE all types of thermally driven chemical sequently lackeel control anal reproducibility, thus for te most part it was unsafe. Noss, in karge part de to the development of cfivient technology, is rapielly gaining acceptance and papularily The number of ube Teations on mnicrowaveassistedd organic cunistey is ing exponentially, as it is being realized that Britany b Hayes, PRD. lerowave systems provide the opportunity to complete reactions In minutes, and have manifold applications in academle and Industrial environments ale. ‘with the advent of new single mode technology at a reasonable cost, together with the simplicity of Its use and installation in a normal synthetic laboratory, chemists now have access to greater enhancements. feedback control, and repeatability. Avallable commercial systems contain temperature and pressure sensors, builtin magnetic string, cooling mechanisms. power control, software operation, and even automation, Miordable instruments are safe, reliable, and effective Microwave Instrumentation Is. as easy 10 install and ‘operate as 2 hatplste..place it im a hood, phig itn, and This book provides an educational tool which can benefit chemists at all leve's from grachate students to sbninr lovel section leaders with rmch experience. in sgynthetie chemistry. The eelHngwn ability of microwa: energy to increase the internal temperatunes bi organic substances more rapidly than eoneentional thermal heat ‘can greatly profit synthetic chemistry. An unelerstanding ‘the basics of microwave energy can be used i ee innction with general chersicl knowledge to enhance synths, This hook is the firs! lo reser: erie: ‘Gemistry from the point of view af an organi chemist al i will Ie uch appreciate Alun KatriLeky, Ph.D, Kenan Brnessor of Chemisty and Director ofthe Ces Jor Betamncyric Componnas a he University of Fowido
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