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Mechanical, Thermal and Hygric Properties of Buildings Materials Edited by Eva Vejmelková Jan Zatloukal Pavel Reiterman Mechanical, Thermal and Hygric Properties of Buildings Materials Selected, peer reviewed papers from the 1st International Doctoral Conference on Advanced Materials, July 23-25, 2014, Zahrádky, Czech Republic Edited by Eva Vejmelková, Jan Zatloukal and Pavel Reiterman Copyright  2014 Trans Tech Publications Ltd, Switzerland All rights reserved. No part of the contents of this publication may be reproduced or transmitted in any form or by any means without the written permission of the publisher. Trans Tech Publications Ltd Churerstrasse 20 CH-8808 Pfaffikon Switzerland http://www.ttp.net Volume 982 of Advanced Materials Research ISSN print 1022-6680 ISSN cd 1022-6680 ISSN web 1662-8985 Full text available online at http://www.scientific.net Distributed worldwide by and in the Americas by Trans Tech Publications Ltd Trans Tech Publications Inc. Churerstrasse 20 PO Box 699, May Street CH-8808 Pfaffikon Enfield, NH 03748 Switzerland USA Phone: +1 (603) 632-7377 Fax: +41 (44) 922 10 33 Fax: +1 (603) 632-5611 e-mail: [email protected] e-mail: [email protected] Preface This book summarizes selected papers of student conference focused on the study of properties of building materials. Presented papers deal with investigation of materials properties of conventional and also innovative building materials. The knowledge of particular material properties is essentially for successful design of structures, that is the reason why studies of basic physical, chemical, mechanical, thermal, hygric, technological and transport properties were included into this book. Experimental programs of present contributions were performed according standard system of EN and ISO but for the design of building structures is important to predict behaviour of used materials on the end of their supposed lifetime which could be number of decades. That is the reason why nowadays is necessary to apply advanced numerical and computation methods to determine of long-term durability. Last mentioned sophisticated instrument based on the theoretical principals is important to be verified in real conditions; science would be extremely boring and sterile without an experiment. Presented papers bring wide database of testing methods and materials properties which could be used in all branches of civil engineering. Pavel Reiterman Scientific committee - chairman: Prof. Ing. Petr Konvalinka, CSc. - Prof. Ing. Robert Černý, DrSc. - Prof. Mrg. Jan Toman, DrSc. - Doc. Ing. Zbyšek Pavlík, Ph.D. - Doc. Ing. Karel Kolář, CSc. - Ing. Eva Vejmelková, Ph.D. - Ing. Martin Keppert, Ph.D. - Ing. Jan Zatloukal, Ph.D. - Ing. Pavel Reiterman, PhD. Acknowledgement Publishing of presented book was supported by CTU in Prague project No. SVK 02/14/F1, which is gratefully acknowledged. Table of Contents Preface, Committee and Acknowledgement Analysis of Thermal Conductivity of Lime Plaster with Pozzolanic Addition by Different Homogenization Techniques J. Fořt, L. Fiala, M. Pavlíková, Z. Pavlík and R. Černý 1 Moisture Transport Properties of Hydrophilic Mineral Wool J. Pokorný, M. Pavlíková, J. Žumár, Z. Pavlík and R. Černý 6 Application of TDR Method for Moisture Profiles Measurement in Cellular Concrete L. Fiala, M. Pavlíková and Z. Pavlík 11 Adsorption of Water Vapor in Selected Sandstone Influenced by Different Method of Measurement Using Dynamic Vapor Sorption Device J. Žumár and Z. Pavlík 16 Effect of Porosity on Mechanical and Hygric Properties of Concrete with Natural Pozzolan Addition T. Kulovaná, P. Rovnaníková, Z. Pavlík and R. Černý 22 Effect of Zeolite Admixture on Freeze/Thaw Resistance of Concrete Exposed to the Dynamic Climatic Conditions V. Kočí, M. Jerman, J. Maděra and R. Černý 27 Influence of Casting Direction on the Mechanical Properties of Cementitious Fiber Reinforced Composites M. Tvarog and J. Fornůsek 32 Restrained Shrinkage Test of High Performance Concrete Ring Specimen A. Zemanová, R. Sovják and J. Litos 38 Retention Curves of Different Types of Sandstone M. Záleská, M. Pavlíková, Z. Pavlík and R. Černý 44 Comparison of Two Different Modes of Inverse Analysis Used for Determination of Moisture Diffusivity of Building Materials J. Kočí, Z. Pavlík and R. Černý 49 Determination of Hygric Properties of Hollow Brick Block as a Function of Moisture Content T. Korecký, M. Jerman and R. Černý 54 Production and Use of the Textile Reinforced Concrete F. Vogel 59 Moisture Migration in High Strength Concrete M. Benáková, T. Kulovaná and M. Jerman 63 Application of Digital Optical Microscopy in Materials and Mechanical Engineering: Optical Porosimetry and Crack Detection K. Ďurana and R. Černý 68 Mechanical Behavior of the Cement Mortar with High Amount of Municipal Solid Waste Incineration (MSWI) Bottom Ash as an Alternative Aggregate K. Polozhiy, M. Keppert, M. Jogl and R. Černý 74 A Comparative Study on Thermal Properties of Two Types of Concrete Containing Fine Ceramic Waste and Burnt Clay Shale as a Supplementary Material L. Scheinherrová, A. Trník, E. Vejmelková, P. Reiterman, I. Medved and R. Černý 79 Numerical Study of the Influence of Internal Blast on the Earth Covered Composite Arch J. Fornůsek and J. Zatloukal 84 Heat and Water Vapor Transport Properties of Selected Commercially Produced Plasters M. Čáchová, D. Koňáková, E. Vejmelková, M. Keppert, K. Polozhiy and R. Černý 90 Fracture Surface Measurement of Concrete with Respect to Loading Speed M. Mára and P. Maca 94 Thermal Properties of Selected Timbers D. Koňáková, M. Čáchová, E. Vejmelková, M. Keppert and R. Černý 100 Pore Structure and Thermal Characteristics of Clay Bricks M. Čáchová, D. Koňáková, E. Vejmelková, M. Keppert, K. Polozhiy and R. Černý 104 New Type of Lightweight Gypsum-Based Material A. Vimmrová 108 b Mechanical, Thermal and Hygric Properties of Buildings Materials Residual Strength of Thermally Loaded Mortars with Treated Municipal Solid Waste Incineration Fly Ash Used as Supplementary Cementitious Material M. Keppert and K. Polozhiy 114 Influence of Different Mechanical Properties to the Concrete Penetration Resistance T. Vavřiník and J. Zatloukal 119 Influence of High-Temperature on Polycarboxylate Superplasticizer in Aluminous Cement Based Fibre Composites M. Jogl, P. Reiterman, O. Holčapek and J. Koťátková 125 Development and Mix Design of HPC and UHPFRC P. Reiterman, M. Jogl, V. Baumelt and J. Seifrt 130 Properties of Cement Composites Containing Coir Pith E. Vejmelková, D. Koňáková, A. Krojidlová, V. Hovorková, M. Čáchová, P. Reiterman and R. Černý 136 Mechanical and Rheological Properties of Aluminous Cement under High Temperatures O. Holčapek, P. Reiterman and P. Konvalinka 141 Destructive and Non-Destructive Testing of High Temperature Influence on Refractory Fiber Composite O. Holčapek, P. Reiterman, M. Jogl and P. Konvalinka 145 Differences in the Properties of Arenaceous Marlstones from Different Quarries E. Vejmelková, M. Čáchová, D. Koňáková, M. Keppert, P. Reiterman and R. Černý 149 Cement Composites for High Temperature Applications D. Koňáková, E. Vejmelková, V. Spedlova, K. Polozhyi and R. Černý 154 Advanced Materials Research Vol. 982 (2014) pp 1-5 © (2014) Trans Tech Publications, Switzerland doi:10.4028/www.scientific.net/AMR.982.1 Analysis of Thermal Conductivity of Lime Plaster with Pozzolanic Addition by Different Homogenization Techniques Jan Fořt1, a, Lukáš Fiala1, b, Milena Pavlíková1, c, Zbyšek Pavlík1, d and Robert Černý1, e 1Czech Technical University in Prague, Faculty of Civil Engineering, Thákurova 7, 166 29 Prague, Czech Republic [email protected], [email protected], [email protected], [email protected], [email protected] Keywords: lime-pozzolan plaster, thermal conductivity, moisture content, effective media theory, transient impulse method, homogenization formulas Abstract. Thermal conductivity of lime-pozzolan plaster is analyzed in the paper. At first, determination of basic physical properties of tested material is done for its basic characterization, as well as for the assessment of input parameters in the subsequent analysis of measured data by different homogenization techniques. The measurements of thermal conductivity are performed in dependence on moisture content from the dry state to the fully water saturated state using transient pulse method. Among the homogenization techniques based on effective media theory, Lichtenecker’s and Dobson’s models are used. The measured data presented in this paper can find utilization in practical applications of the studied plaster. The analyzed homogenization techniques are found to be applicable for a rapid evaluation of moisture dependent thermal conductivity. Introduction Thermal conductivity as the main parameter describing the heat transport in building materials appears to be of particular importance for their practical applications. For their use in building structures there is necessary to take into account that their thermal performance is strictly dependent on total pore volume, distribution and cross connections of pores. In materials research, thermal conductivity of dry materials is mainly studied. However, absolutely dry materials never occur in the conditions of building sites. Also the materials already inbuilt in the structures and exposed to the climatic loading exhibit the dependence of their properties on moisture changes. If the material is wet, heat transferred by moisture in the capillaries adds to the density of heat flow rate. Thermal conductivity of water is approximately 0.560 W/mK [1] which is more than 20 times higher than of the air (0.025 W/mK). Therefore, if water is present in the pore space, its effect competes with the effect of air, and the thermal conductivity of a composite material can be considered as a result of this competition, together with the effect of the solid matrix. On this account, from the practical point of view, there is necessary to have information on the dependence of thermal conductivity on moisture content. Experimental measurement of thermal conductivity of several samples having different moisture content is quite time consuming and in consequence expensive, new approaches for the assessment of moisture dependent thermal conductivity have to be explored and tested in materials research. Homogenization theories working with the concept of an effective medium have proven very useful in a variety of applications in mechanics and in the theory of electricity and magnetism where they already belong to well established treatments (see, e.g., [2, 3]). Within the last couple of years, some references appeared on using the effective media theories for estimation of thermal conductivity of refractory materials, foams, and polymer-based composites. In spite of very promising results, the use of homogenization theory for the assessment of thermal conductivity of lime-based composite materials is still exceptional until now. 2 Mechanical, Thermal and Hygric Properties of Buildings Materials In this paper we refer about application of homogenization techniques for the assessment of the moisture dependent thermal conductivity of lime-pozzolan plaster. The measured values of thermal conductivity are analyzed using homogenization formulas originally derived for application in electromagnetic field theory taking into account the limiting bounds. Experimental Lime-pozzolan plaster that should find use in restoration and reconstruction of historical buildings was the analyzed material. The plaster was composed of lime hydrate, silica sand (fraction 0 – 2 mm), metakaolin and batch water. Composition of studied material is given in Table 1. Table 1. Composition of studied plaster Lime hydrate Water Metakaolin Silica sand (kg) (kg) (kg) (kg) 4.8 4.8 0.8 14.4 Studied plaster was characterized by bulk density, matrix density and total open porosity, whereas these material properties served also as input data for homogenization. Bulk density was determined on gravimetric principle, matrix density using helium pycnometry. Total open porosity was then calculated from these two quantities [4]. The experiments were done on 5 cubic samples of side 70 mm. The relative expanded uncertainty of applied testing method was expected 5%. The measured values of basic material parameters are given in Table 2. Table 2. Basic physical properties of tested plaster Bulk density Matrix density Total open porosity (kg/m3) (kg/m3) (% m3/m3) 1 695 2 620 35.3 For thermal conductivity measurement, the commercially produced device ISOMET 2114 (Applied Precision, Ltd.) was used as a representative of transient pulse methods. The measuring device applies a dynamic measurement method which enables to reduce the period of thermal conductivity measurements to approximately 10 - 15 minutes [5]. The measurement is based on analysis of the temperature response of the analyzed material to heat flow impulses. The heat flow is induced by electrical heating using a resistor heater having a direct thermal contact with the surface of the sample. The measurement accuracy is in thermal conductivity range 0.015 – 0.70 W/mK 5 % of reading + 0.001 W/mK and 10 % of reading in measurement range 0.7 – 6.0 W/mK. The measurements were done in laboratory conditions at average temperature 23 ± 1°C using surface circular sensor. The material samples were first dried and after that exposed to liquid water for specific time intervals. In this way, the different moisture content of the studied samples was reached. The sample size for thermal conductivity measurement was 70 x 70 x 70 mm.

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