Magnetic Resonance in Chemistry 2002: Vol 40 Table of Contents

11 Pages·2002·3.6 MB·English

Contents of volume 40
NUMBER | JANUARY 2002
This Issue is Dedicated to Professor Robin K. Harris
on the Occasion of his 65th Birthday
Editorial
H. GUNTHER
Review
Connectivities in molecules by INADEQUATE: recent developments
J. BUDDRUS AND J. LAMBERT
Contact vs solvent-separated ion pairs: a "Li and °C solid-state NMR study of organolithium
compounds
M. KUHNEN, H. GUNTHER, J.-P. AMOUREUX AND C. FERNANDEZ
Molecular structures of organotin tropolonato complexes with tin coordination numbers 5-7, seen
by single-crystal X-ray diffraction and solid- and solution-state |'°Sn NMR
C. CAMACHO-CAMACHO, R. CONTRERAS, H. NOTH, M. BECHMANN, A. SEBALD, W. MILIUS AND
B. WRACKMEYER
'H and '0 relaxometric investigations of the binding of Mn(II) ion to human serum albumin
S. AIME, S. CANTON, S. G. CRICH AND E. TERRENO
Conformational analysis: Part 37. A 'C and 'H NMR and theoretical investigation of the
conformational equilibrium of 2-methylcyclohexanone oxime and of its O-methyl ether
D. S. RIBEIRO AND R. J. ABRAHAM
Variable-temperature high-pressure investigation of the cobalt-59 NMR spectroscopy of aqueous
K,[Co(CN),]
D. G. GILLIES, L. H. SUTCLIFFE AND A. J. WILLIAMS
'H,"'7Sn J-HMBC spectroscopy as a tool for the determination of long-range "J('H,''’Sn) coupling
constants in the investigation of intramolecular donor-acceptor interaction in [2-(N,N-
dimethylaminomethyl)pheny!|stannanes
M. BIESEMANS, L. C. MARTINS, R. WILLEM, A. LYCKA, A. RUZICKA AND J. HOLECEK
Modelling one- and two-dimensional solid-state NMR spectra
D. MASSIOT, F. FAYON, M. CAPRON, [. KING, S. LE CALVE, B. ALONSO, J.-O. DURAND, B. BUJOLI, Z. GAN AND
G. HOATSON
Carbon isotopomers of tetrafluoroethylene: laser-induced synthesis and NMR spectroscopic
characterization
J. H.H UHN-VELTEN, G. HAGELE, W. FUSS, P. HERING AND M. M. IVANENKO
7A} and ’Li spin-echo and spin-echo double resonance NMR applications to the study of lithium
depletion and surface oxidation in Al-Li alloy
Y. BA AND J. A. RIPMEESTER
Coordination equilibrium in an Ln(III) macrocyclic chelate modulated by a reversible interaction
with a weakly donor substituent
F. A. DUNAND, S. AIME, S. G. CRICH, G. B. GOVENZANA AND A. E. MERBACH
Note
STRAFI imaging of paramagnetic solids: *'P paramagnetic displacements
E. W. RANDALL, A. A. SAMOILENKO AND R. FU
CONTENTS OF VOLUME 40
NUMBER 2 FEBRUARY 2002
Solid-state 'H'°F/'°F-5'H CP/MAS NMR study of poly(vinylidene fluoride)
S. ANDO, R. K. HARRIS AND S. A. REINSBERG
'87Qs subspectra in 'H and *!P {'H} spectra of triosmium carbonyl clusters
M. J. STCHEDROFF, S. AIME, R. GOBETTO, L. SALASSA AND E. NORDLANDER
C—H°:-:X (X =N, O, S) intramolecular interaction in 1-vinyl-2-(2’-heteroaryl)pyrroles as monitored
by 'H and °C NMR spectroscopy
A. V. AFONIN, I. A.U SHAKOV, S. Yu. KUZNETSOVA, O. V. PETROVA, E. Yu. SCHMIDT AND A. I. MIKHALEVA
Dynamic and magnetic susceptibility effects on the MAS NMR linewidth of a tetrapeptide bound
to different resins
J. FURRER, K. ELBAYED, M. BOURDONNEAU, J. RAYA, D. LIMAL, A. BIANCO AND M. PIOTTO
Modern proton-detected 1D 'H-'SN NMR experiments. Application to the measurement of
'H,'5N coupling constants at natural abundance
lr. PARELLA AND J. BELLOC
Multinuclear magnetic resonance study of some imidovanadium complexes
D. GUDAT, U. FISCHBECK, F. TABELLION, M. BILLEN AND F. PREUSS
Structural studies of benzophenanthridine alkaloid free bases by NMR spectroscopy
P. SECKAROVA, R. MAREK, J. DOSTAL, R. DOMMISSE AND E. L. ESMANS
Complexation of selenium to (R)-Rh,(MTPA),: thermodynamics and stoichiometry
H. DUDDECK, S. MALIK, T. GATI, G. TOTH AND M. I. CHOUDHARY
'3C PHIP NMR spectra and polarization transfer during the homogeneous hydrogenation of alkynes
with parahydrogen
M. STEPHAN, O. KOHLMANN, H. G. NIESSEN, A. EICHHORN AND J. BARGON
Notes
7H NMR spin relaxation study of the soft segment motion in alternating ethylene—propylene
copolymers
T. NAKAJIMA, T. AKIYAMA AND H. FURUYA
Diels-Alder reaction of 2,7-dichloroquinoline-5,8-dione with a thiazole o-quinodimethane.
Assignment of the regiochemistry by 'H-'*C HMBC correlations
R. A. TAPIA, Y. PRIETO, F. PAUTET, B. FENET AND H. FILLION
Book review, 168
NUMBER 3 MARCH 2002
3D Heteronuclear long-range 'H-'C scalar correlation at natural abundance: application to
oligosaccharide analysis
G. HERNANDEZ AND D. M. LeMASTER
'H, ‘°C and *!P NMR spectral analysis of monoalkyl(@-anilinobenzyl)phosphonates and their
dipalladium(II) metallocyclic complexes
L. TUSEK-BOZIC AND A. LYCKA
‘SN NMR spectroscopy of 3-substituted 5-trichloromethyl-1,2-dimethyl-1H-pyrazolium chlorides
M. A. P. MARTINS, C. M. P. PEREIRA. A. P. SINHORIN, A. ROSA, N. E. K. ZIMMERMANN, H. G. BONACORSO
AND N. ZANATTA
Non-empirical calculations of NMR indirect carbon-carbon coupling constants: 1. Three-membered
rings
L. B. KRIVDIN, S. P. A. SAUER, J. E. PERALTA AND R. H. CONTRERAS
Study of the temperature-dependent conformational averaging of 'H NMR resonances in
vinylcyclopropane through the use of ab initio methodology and Boltzmann statistics
C. W. SWALINA. E. P. O°BRIEN AND G. MOYNA
Characterization of para-substituted benzamidoximes and benzamidinium salts by '"N NMR
spectroscopy
U. GIRRESER, M. KONIG AND B. CLEMENT
CONTENTS OF VOLUME 40
Long-range '’F-'°N heteronuclear shift correlation: examination of J-modulations associated with
broad range accordion excitation
D. J. RUSSELL, C. E. HADDEN, G. E. MARTIN AND K. KRISHNAMURTHY
A rare occurrence of a B-turn in an amyloid BA4 peptide
S. TAURO, E. COUTINHO AND S. SRIVASTAVA
Structural characterization of monomeric and oligomeric arylamides by solution and solid-state
NMR spectroscopy
S. CAVALLARO, G. CUM, R. GALLO, A. SPADARO AND G. VISALLI
Temperature dependence of proton—proton residual dipolar couplings in adenosine dissolved in
charged phospholipid bicelles. Application of a two-dimensional selective refocusing method
P. KRAJEWSKI AND M. BARDET
'H and ''C NMR and X-ray diffraction data for a diosgenyl N,O-protected glucopyranoside
H. MYSZKA, D. BEDNARCZYK, Z. CIUNIK AND W. KACA
Hydroacridines: Part 23. 'H and °C NMR spectra of sym-octahydroacridine, its 9-(3-pyridyl) and
9-(4-pyridyl) derivatives and the corresponding N(10)-oxides. An experimental approach to the
diamagnetic anisotropy of the pyridine nucleus
F. POTMISCHIL, C. DELEANU, M. MARINESCU AND M. D. GHEORGHIU
A relationship between the half-width of Ge NMR signals and hypercoordination in some phenyl-
germanes
Y. TAKEUCHI, K. TANAKA, S. AOYAGI AD H. YAMAMOTO
Configuration and conformation of a novel uridine analogue: 'H and °C NMR spectra of (5’S)-1-
[2’-(2-hydroxyethyl)tetrahydropyran-5’-yl]-1H-pyrimidine-2,4-dione
G. BALAYIANNIS, D. PAPAIOANNOU AND A. TROGANIS
NUMBER 4 APRIL 2002
Editorial: Forty Volumes of Magnetic Resonance
H. GUNTHER
An NMR study of cyclodextrin complexes of the steroidal neuromuscular blocker drug Rocuronium
Bromide
K. S. CAMERON, D. FLETCHER AND L. FIELDING
General model of assignment of the relative stereochemistry in the Nicholas reaction products
resulting from chiral dicobalthexacarbonyl-1-alkoxy-propargylium cations
A. M. MONTANA AND M. CANO
Distribution of the methyl radical adduct of N-benzylidene-1-diethoxyphosphoryl-1-methyl-
ethylamine N-oxide-type nitrones in water-sodium dodecyl sulfate micelles: an electron para-
magnetic resonance spin trapping study
C. RIZZI, R. LAURICELLA, J.-C. BOUTEILLER, V. ROUBAUD AND B. TUCCIO
A 'H NMR and molecular modelling investigation of diastereotopic methylene hydrogen atoms
C. F. TORMENA, M. P. FREITAS, R. RITTNER AND R. J. ABRAHAM
Electron paramagnetic resonance study of nitroxides generated from nitric oxide by reaction with
transient radicals
J. JIN, L.W U AND Z. ZHANG
70 NMR spectra of some butyltin(IV) acetates
A. LYCKA AND J. HOLECEK
Spectral Assignments and Reference Data
'H and °C NMR spectral assignments of 2,4-diaryl-substituted cycloalkyl[d|pyrimides
A. HERRERA, R. MARTINEZ-ALVAREZ, M. CHIOUA, A. SANCHEZ, D. MOLERO AND R. CHIOUA
A '5N NMR investigation of a series of benzotriazinones and related antitumour heterocycles
K. VAUGHAN, D. E. V. WILMAN, R. T. WHEELHOUSE AND M. F. G. STEVENS
'H_ and °C spectral assignment of o-chloroformy! substituted 1,4-dihydropyridine derivatives
M. SUAREZ, N. MARTIN, R. MARTINEZ, Y. VERDECIA, D. MOLERO, L. ALBA, C. SEOANE AND E. OCHOA
Vi CONTENTS OF VOLUME 40
Structural elucidation and complete assignment of a novel class of sulfonamides: bridgehead tri-
cyclic sultams
C. JOLIVET, D. D. LONG, R. S. DAHL AND A. P. TERMIN
a-Pinene and myrtenol : complete 'H NMR assignment
S.-G. LEE
Assignment of the ‘°C and "N NMR spectra of the antitumor antibiotic streptonigrin
P. 1. ANDERBERG, I. J. LUCK AND M. M. HARDING
Book review, 316
NUMBER 5 MAY 2002
Review
A tutorial comparison of the NMRIT and LAOCOON approaches for analyses of complex solution-
phase nuclear magnetic resonance spectra
S. L. MANATT
A new approach to automated first-order multiplet analysis
S. GOLOTVIN, E. VODOPIANOV AND A. WILLIAMS
35C] NQR studies of 1-chloro-2,4-dinitrobenzene and 1,2-dichloro-3-nitrobenzene as a function of
pressure and temperature
J. SRINIVAS, R. K. SUBRAMANIAN, K. P. RAMESH, J. RAMAKRISHNA, K. S. SURESH AND C. RAGHAVENDRA RAO
EPR study of radicals generated from bioactive S-nitrosothiols and related thiols
J. JIN, L. WU AND Z. ZHANG
N’- and N°-substituted purine derivatives: a "N NMR study
R. MAREK, J. BRUS, J. TOUSEK, L KOVACS AND D. HOCKOVA
Modified, pulse field gradient-enhanced inverse-detected HOESY pulse sequence for reduction of f,
spectral artifacts
T. M. ALAM, D. M. PEDROTTY AND T. J. BOYLE
Notes
Epikatonic acid from Austroplenckia populnea: structure elucidation by 2D NMR spectroscopy and
X-ray crystallography
G. D. F. SILVA, L. P. DUARTE, S. A. VIEIRA FILHO, A. C. DORIGUETTO, Y. P-. MASCARENHAS, J. ELLENA,
E. E. CASTELLANO AND A. B. COTA
NMR analysis of 6-(2’,3’-dihydro-1’H-inden-1’-yl)-1H-indene
P. SPITELLER, M. SPITELLER AND J. JOVANOVIC
Temperature dependence of internucleotide nitrogen—nitrogen scalar couplings in RNA
D. BYTCHENKOFF, E. CHIARPARIN, D. FRUH, $. RUDISSER AND G. BODENHAUSEN
Book review, 380
NUMBER 6 JUNE 2002
Heterogeneity of surface colour centres on alkaline earth metal oxides as revealed through
EPR/ENDOR spectroscopy
I. J. PURNELL, M. CHIESA, R. D. FARLEY, D. M. MURPHY, C. C. ROWLANDS, M. C. PAGANINI AND E. GIAMELLO
Phosphoryldithioformates: Part V. Unusual linewidth variations in the ESR spectra of some spin
adducts of (dimethoxy)phosphory! methyl! dithioformate
\. ALBERTI, M. BENAGLIA, D. MACCIANTELLI, A. HUDSON AND S. MASSON
PGSE-WATERGATE, a new tool for NMR diffusion-based studies of ligand-macromolecule
binding
W. S. PRICE, F. ELWINGER, C. VIGOUROUX AND P. STILBS
Structure of metal adducts of anthracyclines probed by absorption, circular dichroism and
paramagnetic NMR
L. DI BARI. G. PINTACUDA, S. RIPOLI AND P. SALVADORI
Isotope-induced chemical shifts 7A'”"'B(°Si) in alkenylsilanes containing three- and four-coordinate
boron. A new teol for studying weak intramolecular boron—element bonds
B. WRACKMEYER AND O. L. TOK
CONTENTS OF VOLUME 40
Revised structures of Arillatanosides A—-C from Polygala arillata
R.-W. TENG, Z.-J. WU, Y.-E. HE, D.-Z. WANG AND C.-R. YANG
Notes
NMR analyses of two isomeric cyclobutanes from a [2+2] photocycloaddition
D. E. MINTER, C. D. WINSLOW, W. H. WATSON AND S. BODIGE
Two new acylated flavonoid glycosides from Morina nepalensis var. alba Hand.-Mazz.
R.-W. TENG, H.-Y. XIE, H.-Z. LI, X.-K. LIU, D.-Z. WANG AND C.-R. YANG
Molecular motion in some radiolabelled dipeptides: a muon spin relaxation study
C. J. RHODES, T. C. DINTINGER, H. MORRIS AND C. A. SCOTT
Book review, 430
NUMBER 7 JULY 2002
Editorial
R. K. HARRIS
An NMR tool for cyclodextrin selection in enantiomeric resolution by high-performance liquid
chromatography
A. LAVERDE JR., G. J. A. DA CONCEICAO, S. C. N. QUEIROZ, F. Y. FUJIWARA AND A. J. MARSAIOLI
NMR study on 9-S and 9-R oxirane derivatives of ascomycin
K. BAUMANN, K. HOGENAUER, G. SCHULZ AND A. STECK
Substituent effects on 'H and '*C NMR chemical shifts in o-monosubstituted ethyl acetates:
principal component analysis and 'H chemical shift calculations
L. TASIC, R. J. ABRAHAM AND R. RITTNER
Spectral Assignments and Reference Data
Complete assignment of 'H and '°C NMR spectra of new pentacyclic triterpene acid benzyl esters
R. WIES AND W. SEEBACHER
Structure of an unexpected trimer from the reaction of ageratochromene II with aluminum chloride
C. CHU, J. HU, T. XU. H. XIAO AND X. LIANG
'H and °C NMR assignments of new oligo-bipyridine-phenanthroline hybrids as potential
precursors of helicate complexes
R. ANNUNZIATA, M. BENAGLIA AND A. BOLOGNA
'H, °C and SN NMR spectroscopic characterization of unexpected degradation products of the
nifedipine analogue bis(2-cyanoethyl) 2,6-dimethyl-4-(2-nitrophenyl)-1,4-dihydro-3,5-pyridinedicar-
boxylate
E. GOSSNITZER, K. GORLITZER AND H. J. BALTRUSCH
Reassignment of the 'H NMR spectrum of fusidic acid and total assignment of 'H and 'C NMR
spectra of some seiected fusidane derivatives
N. RASTRUP-ANDERSEN AND T. DUVOLD
A new stereoisomer of stemmadenine alkaloid from Tabernaemontana heyneana
R. K. GROVER, S. SRIVASTVA, D. K. KULSHRESHTHA AND R. ROY
'H and °C NMR spectral characterization of some antimalarial in vitro 2,4-diamino-10-
methylpyrimido[4,5-b]-5-quinolone derivatives
J. E. CHARRIS, J. N.D OMINGUEZ. N. GAMBOA, J. ANGEL, N. PINA, M. GUERRA, E. MICHELENA AND S. E. LOPEZ
'H, '3C and "N NMR chemical shifts of substituted pyrazolo[1,5-a]pyrimidines
E. KOLEHMAINEN. K. LAIHIA, A. V. FIRSOV, V. I. ZAYZEV, E. E. EMELINA AND A. A. PETROV
Complete assignment of 'H and ‘°C NMR data for nine protopanaxatriol glycosides
R.-W. TENG, H.-Z. LI, J.-T. CHEN, D.-Z. WANG, Y.-E. HE AND C.-R. YANG
Appendix
NMR nomenclature: nuclear spin properties and conventions for chemical shifts. TUPAC
Recommendations 2001
R. K. HARRIS, E. D. BECKER, S. M. CABRAL DE MENEZES, R. GOODFELLOW AND P. GRANGER
Announcement, 506
CONTENTS OF VOLUME 40
NUMBER 8 AUGUST 2002
Multinuclear magnetic resonance study of the structure and tautomerism of azide and
iminophosphorane derivatives of chloropyridazines
P. CMOCH
NMR analysis of novel ganglisoside GM4 analogues containing de-N-acetyl and lactamized sialic
acid: probes for searching new ligand structures for human L-selectin
l. HAMADA, H. HIROTA, S. YOKOYAMA, N. OTSUBO, H. ISHIDA, M. KISO, A. KANAMORI AND R. KANNAGI
Use of '°9F NMR spectroscopy to probe enzymatic oxidation of fluorine-tagged sulfides
B. BEHROUZIAN, D. HODGSON, C. K. SAVILE, B. DAWSON, P. H. BUIST AND J. SHANKLIN
'H{'5N} GHMQC study of 5,7-diphenyl-1,2,4-triazolo[1,5-a]pyrimidine and 'H, °C and "N NMR
coordination shifts in Au(II]) chloride complexes of 1,2,4-triazolo[1,5-a]pyrimidines
E. SZLYK, L. PAZDERSKI, I. EAKOMSKA, L. KOZERSKI AND J. SITKOWSKI
Note
'H and °C NMR study of 2-hydroxyglutaric acid and its lactone
D. BAL AND A. GRYFF-KELLER
Spectral Assignments and Reference Data
Configuration of functional trifluoromethylated dienoates, aryldienoates and trienoates
P. PALMAS, J. THIBONNET, J.-L. PARRAIN, M. ABARBRI, F. DAVID-QUILLOT AND A. DUCHENE
NMR analysis of mono- and difructosyllactosucrose synthesized by 1'-fructosyltransferase purified
from roots of asparagus (Asparagus officinalis L.)
A. YAMAMORI, E. FUKUSHI, S. ONODEA, J. KAWABATA AND N. SHIOMI
'H_ '3C chemical shifts for acridines: Part XVII. (1,3-Benzothiazol-2-yl)amino-9(10H)-acridinone
derivatives
A. AVELLANEDA, M. ROBIN, R. FAURE, A. PERICHAUD AND J.-P. GALY
Complete assignment of the 'H and '*C NMR spectra of some N-benzyl-(piperidin or pyrrolidin)-
purines
M. I. RODRIGUES-FRANCO AND M. I. FERNANDEZ-BACHILLER
Structure elucidation and antibacterial activity of a new coumarinolignoid from Daphne gnidium L.
F. COTTIGLIA, L. BONSIGNORE, G. LOY, D. GARAU, C. FLORIS AND M. CASU
'H_ and '°C chemical shifts for bis(benzopyridinium) dibromides with semirigid aromatic linkers
J. CAMPOS, J. J. DIAZ, M. C. NUNEZ, A. ENTRENA, M. A. GALLO AND A. ESPINOSA
NUMBER 9 SEPTEMBER 2002
Announcement
H. GUNTHER
Rapid Communications
Identification of bound waters in the solution structure of ribonuclease T, using the double pulsed
field gradient spin-echo NMR technique for selective water excitation
M. TASHIRO, K. FURIHATA, S. SHIMOTAKAHARA AND H. SHINDO
An improved *°S nuclear magnetic shielding scale from the gas-phase study of COS
K. JACKOWSKI, W. MAKULSKI AND W. KOZMINSKI
Papers
Conformational analysis of some 1R,4S-2-arylidene-p-menthan-3-ones by 'H NMR spectroscopy and
molecular simulation
N. S. PIVNENKO, T. G. DRUSHLYAK, L. A. KUTULYA, V. V. VASHCHENKO, A. O. DOROSHENKO AND J. W. GOODBY
The first automated 470.59 MHz !°F NMR-controlled titration: dissociation constants and
ion-specific chemical shifts of 2-amino-4-fluoro 2-methylpent-4-enoic acid
C. E. UHLEMANN, C. G. PFAFF, G. HAGELE, K. W. LAUE, M. LUBKE AND G. HAUFE
Stereochemical analysis of the 3a- and 3B-hydroxy metabolites of tibolone through NMR and
quantum-chenical investigations. An experimental test of GIAO calculations
D. COLOMBO, P. FERRABOSCHI, F. RONCHETTI AND L. TOMA
CONTENTS OF VOLUME 40
The bonding situation in 1,3,2-diazaphospholene derivatives as studied by solid-state NMR
spectroscopy
D. GUDAT, A. HAGHVERDI AND W. HOFFBAUER
70, '3C and 'H NMR and IR spectral study of crowded ketones: possible intramolecular
C—H. .. .O interactions
X.-R. QIN, Y. ISHIZUKA, J. S. LOMAS, T. TEZUKA AND H. NAKANISHI
Notes
Structure of a calotropagenin-derived artifact from Calotropis procera
A. G. HANNA, N. M. M. SHALABY, N. A. M. MORSY, A. SIMON, G. TOTH, S. MALIK AND H. DUDDECK
Four new ursane-type saponins from Morina nepalensis var. alba
R. W. TENG, H. Y. XIE, D. Z. WANG AND C. R. YANG
Two new complex triterpenoid saponins from Gledistsia dolavyi Franch.
R. W. TENG, W. NI, D. Z. WANG, J. K. DING AND C. X. CHEN
Spectral Assignments and Reference Data
Complete assignment of the NMR spectra of [p-Leu']-microcystin-LR and analysis of its solution
structure
J. SCHRIPSEMA AND D. DAGNINO
Total assignment of 'H and °C NMR spectra of three triterpene saponins from roots of Silene
vulgaris (Moench) Garcke
S. BOUGUET-BONNET, M. ROCHD, P. MUTZENHARDT AND M. HENRY
Addendum, 622
NUMBER 10 OCTOBER 2002
Towards the automatic analysis of 'H NMR spectra: Part 3. Confirmation of postulated chemical
structure
L. GRIFFITHS AND J. D. BRIGHT
Aluminium-27 NMR investigation of the influence of cation type on aluminosilicate solutions
N. AZIZI, R. K. HARRIS AND A. SAMADI-MAYBODI
One-bond C-'C coupling constants in alkyl-substituted cyclopropenes: experimental and
theoretical studies
K. KAMIENSKA-TRELA, P. BERNATOWICZ, W. LUTTKE, R. MACHINEK AND M. TRA:TTEBERG
One-dimensional TOCSY 'H NMR experiments on adducts of amino acid esters with cobalt(II}
tetramethylchiroporphyrin. Prospects for the analysis of amino acid mixtures
M. CLAEYS-BRUNO, M. BARDET AND J.-C. MARCHON
A [Pd(n?-PhCHCHCHPh)(phosphino-oxazoline)|* complex with almost identical P- and N-trans
influences. '°C chemical shifts and allylic alkylation chemistry
P. DOTTA, P. G. A. KUMAR AND P. S. PREGOSIN
Phenylselenenylmenthane derivatives and their enantiomeric discrimination by 'H and °C NMR
spectroscopy in the presence of a chiral dirhodium complex
S. MALIK, S. MOELLER, H. DUDDECK AND M. I. CHOUDHARY
Effect of pH on the rotational conformations of 1,3-diamino-2-hydroxypropane
J. M. CHENG, J. P- HELLER, K. A.P ETTERSON AND J. D. ROBERTS
Notes
NMR study of E/Z isomerism in N-alkoxybenzoimidic acid derivatives
J. SCHRAML, V. BLECHTA, J. KARBAN AND J. MINDL
Conformational studies on indole alkaloids from Flustra foliacea by NMR and molecular modeling
M. S. MORALES-RIOS, N. F. SANTOS-SANCHEZ, O. R. SUAREZ-CASTILLO AND P. JOSEPH-NATHAN
CONTENTS OF VOLUME 40
NUMBER 11 NOVEMBER 2002
Rapid Communication
An ENDOR study of oxomolybdenum(V) tris(pyrazolyl)borate complexes; identification of
couplings to boron and other heteroatoms
R. D. FARLEY, P. HOEFER, J. P. MAHER, J. A. MCCLEVERTY, D. M. MURPHY, C. C. ROWLANDS, V. A. UNG AND
M. D. WARD
Papers
Isoquinoline alkoloids: a '"N NMR and x-ray study. Part 2
R. MAREK, J. MAREK, J. DOSTAL, E. TABORSKA, J. SLAVIK AND R. DOMMISSE
2D NMR analysis for unambiguous structural elucidation of phenolic compounds formed through
reaction between (+)-catechin and glyoxylic acid
N.-E. ES-SAFI, C. LE GUERNEVE, V. CHEYNIER AND M. MOUTOUNET
Quantitative determination of aliphatic hydrocarbon compounds by 2D NMR
H. KOSKELA AND T. VAANANEN
Thallium(II1) coordination compounds: chemical information from 7°Tl NMR longitudinal
relaxation times
A. BODOR, I. BANYAI, J. KOWALEWSKI AND J. GLASER
Solid-state CP/MAS '8C NMR studies on conformational polymorphism in sertraline hydrochloride,
an antidepressant drug
A. NOVOSELSKY AND R. GLASER
J-modulated 1D directed COSY for precise measurement of proton-proton residual dipolar coupling
constants of oligosaccharides
T. N. PHAM. T. LIPTAJ, P. N. BARLOW AND D. UHRIN
Notes
Structure elucidation and conformational analysis of a fused cyclopentanopyrazolidinol
C. A. TSOLERIDIS AND J. STEPHANIDOU-STEPHANATOU
NMR studies on 1,2-dihydro-2-(4-aminophenyl)-4-[4-(4-aminophenoxy)-4-phenyl]-(2H)phthalazin-
l-one
T. WANG, L. CHENG, T. ZHANG, H. YUAN AND S. MAO
'H, '5C and SN NMR analysis of Tréger’s base and of some of its ['°N,] labelled precursors
F. SALORT, C. PARDO AND J. ELGUERO
Spectral Assignments and Reference Data
A 3C NMR study of the methylol derivatives of 2,4’- and 4,4’-dihydroxydiphenylmethanes found in
resol phenol-formaldehyde resins
I. H. FISHER, P. CHAO, C. G. UPTON AND A. J. DAY
Complete assignments of the 'H and '°C NMR spectra of five rearranged abietane diterpenoids
B. RODRIGUEZ
NUMBER 12 DECEMBER 2002
Pulsed field gradient NMR investigation of solubilization equilibria in amino acid and dipeptide
terminated micellar and polymeric surfactant solutions
R. S. HICKOK, S. A. WEDGE, A. L. HANSEN, K. F. MORRIS, F. H. BILLIOT AND I. M. WARNER
Quantitative ‘Hi NMR spectroscopic determination of the E/Z isomer ratio of the antidepressant
drug fluvoxamine for usage in pharmaceutical analysis
R. DEUBNER AND U. HOLZGRABE
Interpreting 7"J(F,N), '»J(H,N) and 'J(F,H) in the hydrogen-bonded FH-collidine complex
J. E. DEL BENE, R. J. BARTLETT AND J. ELGUERO
Radiofrequency-induced temperature increase as a function of cross polarization contact time in
8CB
A. K. CHATTAH, F. M. CUCCHIETTI, M. HOLOGNE, J. RAYA AND P. R. LEVSTEIN
CONTENTS OF VOLUME 40
™7§e,!°F 2D NMR correlation spectroscopy of fluoro(organylseleno)alkenes and -alkanes
H. POLESCHNER AND K. SEPPELT
An ab initio study of solvent polarity and hydrogen bonding effects on the nitrogen NMR shieldings
of N,N-dimethylacetamidine
M. N. MANALO AND A. C. DE DIOS
Spectral Assignments and Reference Data
Structural determination and complete NMR spectral assignments of a new bufadienolide glycoside
M. YE, J. HAN, H. GUO AND D. GUO
Total assignments of NMR spectral lines of synthezised mono- and diacyl derivatives of diosgenyl
saponins
M. LI, X. W. HAN, X. M. LIU, B. YU, G. W. XING, Y. Z. HUI AND X. BAO
Total assignment of 'H and 'C NMR spectra of a new prenylated flavanone from Dioclea
grandiflora
V. S. LEMOS, M. H. DOS SANTOS, L. A. RABELO AND S. F. CORTES
'3C cross-polarization magic angle spinning NMR of ferrocene derivatives
Y. OKADA, K. OGURI, K. SAKAMOTO, Y. MIYAKO AND T. HAYASHI
NMR assignments of selected bacterial carotenoids
B. F. LUTNAES, J. KRANE AND S. LIAAEN-JENSEN
Book review, 800; Volume author index, 801; Volume subject index, 805; Volume contents, i
SPECIAL ISSUE DECEMBER 2002
SPECIAL ISSUE: NMR and Diffusion
GUEST EDITOR: Professor G. A. Morris, University of Manchester, UK
Editorial
H. GUNTHER
Guest Editor’s Foreword: NMR and Diffusion
G. A. MORRIS
Review
NMR methods applied to anisotropic diffusion
I. FURO AND S. V. DVINSKIKH
Papers
Locally anisotropic motion in a macroscopically isotropic system: displacement correlations
measured using double pulsed gradient spin-echo NVR
P. T. CALLAGHAN AND M. E. KOMLOSH
Investigation of thin surface-wetting films in two-phase saturated porous media
W. M. HOLMES AND K. J. PACKER
Diffusion NMR methods applied to xenon gas for materials study
R. W. MAIR, M. S. ROSEN, R. WANG, D. G. CORY AND R. L. WALSWORTH
Probing interactions within complex colloidal systems using PGSE-NMR
P. C. GRIFFITHS, A. Y. F. CHEUNG, J. A. DAVIES, A. PAUL, C. N. TIPPLES AND A. L. WINNINGTON
Scope of droplet size measurements in food emulsions by pulsed field gradient NMR at low field
J. PR. M. VAN DUYNHOVEN, G. J. W. GOUDAPPEL, G. VAN DALEN, P. C. VAN BRUGGEN, J. C. G. BLONK AND
A. P. A. M. EJKELENBOOM
The use of PGSE NMR and DECRA for determining polymer composition
B. ANTALEK, J. M. HEWITT, W. WINDIG, P. D. YACOBUCCI, T. MOUREY AND K. LE
Determining the molecular weight, aggregation, structures and interactions of natural organic
matter using diffusion ordered spectroscopy
A. J. SIMPSON
Use of 'H NMR-determined diffusion coefficients to characterize lipoprotein fractions in human
blood plasma
M. LUI, H. TANG, J. K. NICHOLSON AND J. C. LINDON
Xi CONTENTS OF VOLUME 40
Translation diffusion measured by PFG-NMR on full length and fragments of the Alzheimer
AB(1-40) peptide
J. DANIELSSON, J. JARVET, P. DAMBERG AND A. GRASLUND
1°F diffusion NMR analysis of enzyme-inhibitor binding
T. S. DERRICK, L. H. LUCAS, J.-L. DIMICOLI AND C. K. LARIVE
NMR diffusion coefficient study of steroid—cyclodextrin inclusion complexes
K. S. CAMERON AND L. FIELDING
Monitoring the non-specific interactions of catechin through diffusion measurements based on
pulsed-field gradients
C. MONTEIRO, C. MAECHLING AND C. HERVE DU PENHOAT
PGSE NMR diffusion study of the self-association of N-methylacetamide in carbon tetrachloride
D. G. REGAN, B. E. CHAPMAN AND P. W. KUCHEL
HR-DOSY as a new tool for the study of chemical exchange phenomena
E. J. CABRITA AND S. BERGER
NMR diffusion measurements of strong signals: the PGSE-Q-switch experiment
W. S. PRICE AND M. WALCHLI
HR-DOSY experiments with radiofrequency field gradients (RFG) and their processing according
to the HD method
C. MOURO, P. MUTZENHARDT, B. DITER AND D. CANET
Artefacts and pitfalls in diffusion measurements by NVR
G. H. SORLAND AND D. AKSNES
A one-shot sequence for high-resolution diffusion-ordered spectroscopy
M. D. PELTA, G. A. MORRIS, M. J. STCHEDROFF AND S. J. HAMMOND