Table Of Content

Journal of Fluorine Chemistry, 51 (1991) 439 Author Index of Volume 51 Abney, K. D., 165 Garcia, C., 245 Portella, C., 1 Albizo, J. M., 277 Gerdes, J. M., 149 Porwisiak, J., 131 Alessi, P., 103 Gould, R. O., 305 Amatore, C., 357 Qing-Yun Chen, 21 Ang, H. G., 83 Habibi, M. H., 217, 291 Haddach, M., 197 Rankin, D. W. H., 305 Ball, G. R., 165 Haywood, L., 419 Reuter, P., 53 Banks, R. E., 407 Hovanec, J. W., 277 Riess, J. G., 197 Barbusse, D., 245 Rock, M., 381 Beaudry, W. T., 277 Iznaden, M., 1 Rohlike, W., 53 Bell, G. A., 305 Roman, L., 155 Benomar, S. M., 207 Jianxun Wen, 75, 229, 433 Saidi, K., 217 Bishop, J. E., 149 Jones, C. J., 283 Blake, A. J., 305 Sampath Kumath, H. P., 171 Blanchard, S. H., 93 Katrizky, A. R., 33 Sauvétre, R., 223, 397 Burdon, J., 179 Khaffaff, S. N., 407 Sawada, H., 117 Kolomietz, A. F., 323 Scipioni, A., 103 Calas, P., 357 Kwik, W. L., 83 Smith, J. A., 179 Cambon, A., 141, 155 Srivastava, R. S., 93 Chang-Ming Hu, 295 Leeper, F. J., 381 Suzuki, A., 299 Chkanikov, N. D., 323 Szafraniec, L. L., 277 Claire, P. P. K., 283 McCleverty, J. A., 283 Szényi, F., 155 Coe, P. L., 179, 283 McKee, S., 419 Commeyras, A., 357 Mader, J., 53, 335 Takamora, K., 299 Mallouk, T. E., 291 Tatlow, J. C., 179 Dapremont-Avignon, C., Manivannan, V., 93 Tellier, F., 397 357 Mathis, C. A., 149 Tipping, A. E., 207 Dean, P. A. W., 93 Mei-Jin Chen, 21 Tyutin, V. Y., 323 Dieng, S. Y., 155 Meinert, H., 53, 335 Tzeng, G. S., 257 Dmowski, W., 43, 131 Middleton, W. J., 419 Ducourant, B., 245 Morrison, E., 83 Vittal, J. J., 93 Eller, P. G., 165 Nakayama, M., 117 Wan, C. C., 257 Napoli, M., 103 Ward, J. R., 277 Fabron, J., 141 Normant, J.-F., 223 Wei-Qiang Fan, 33 Fackler, R., 53 Feng-Ling Qing, 295 O’Reilly, N. J., 207 Yadong Zhang, 75, 229, 433 Fokin, A. V., 323 Yanchang Shen, 349 Fourcade, R., 245 Padma, D. K., 171 Yao-Ling Qiu, 295 Fraccaro, C., 103 Pastor, R., 141, 197 Yoneda, N., 299 Fukuhara, T., 299 Plenkiewicz, H., 43 Yuejun Xiang, 349 Elsevier Sequoia/Printed in The Netherlands Journal of Fluorine Chemistry, 51 (1991) 441-446 Subject Index of Volume 51 Addition synthesis of 1,4-bis(p-aryloxy-tetrafluoro- of 1,2-dibromotetrafluoroethane to al- phenyl)butadiyne monomers for non- kynes by means of redox system, linear optics, 75 295 synthesis of fluoro-diacetylene mono- Alkanes mers: 1,4-bis(2,4,6-triaryloxy-difluoro- addition of 1,2-dibromotetrafluoroethane phenyl)butadiynes, 433 to alkynes by means of redox system, Amides 295 fluoroalkylbenzenes: synthesis of (S)-2,3- perfluorodimorpholinoalkanes as stabiliz- dimethoxy-5-[(3-fluoro)propyl-6- ing additives in perfluorocarbon- hydroxy-N ](1-ethyl-2-pyrrolidi- emulsions, 335 nyl)methyl benzamide, 149 synthetic utility of 3-(perfluoro-1,1-di- Amines methylbutyl)-1-propene: reactions of amine(polyfluoroalkoxyacyl)imide surfac- 3-(perfluoro-1,1-dimethylbutyl)-1,2- tants, 419 epoxypropane with inorganic anions, preparation, novel, of polyfluoroalkyl thiourea and guanidine, 43 secondary and tertiary amines, 33 Alkenes synthesis of esters of 3,3-dicyano-2-(tri- fluorocarbon derivatives of N: synthesis fluoromethyl)acrylic acid and their of fluorinated indolizines through re- reactions with arylamines, 323 actions of pyridinium ethoxycarbonyl- unsaturated N compounds containing F: methylide or pyridinium phenacylide reaction of 2,5-dichloro-1,1,1,6,6,6- with perfluoropropene, perfluorobut- hexafluoro-3,4-diazahexa-2,4-diene 2-yne and 3,3,3,-trifluoropropyne, 407 with triethylamine and related reac- synthetic utility of 3-(perfluoro-1,1-di- tions, 207 methylbutyl)-1-propene: reactions of Amino acids 3-(perfluoro-1,1-dimethylbutyl)-1,2- synthesis of new F-alkyl amino-acid de- epoxypropane with inorganic anions, rivatives of lysine, arginine and cys- thiourea and guanidine, 43 teine, 197 unsaturated N compounds containing F: Aminoaevulinic acid reaction of 2,5-dichloro-1,1,1,6,6,6- synthesis of fluorinated analogue of hexafluoro-3,4-diazahexa-2,4-diene 5-aminoaevulinic acid, potential in- with triethylamine and related reac- hibitor of porphyrin biosynthesis, 381 tions, 207 Aminophenols Alkylation preparation of p-fluorophenols from p- perfluoro-, of 2-mercaptobenzothiazole aminophenols: diazotization and fluo- and its analogues with perfluoroalkyl rodediazoniation in pyridine-HF, 299 iodides by Spy! reaction, 21 Anthonomus grandis pheromone Alkynes preparation of fluorinated analogues of, addition of 1,2-dibromotetrafluoroethane 397 to, by means of redox system, 295 Antimony fluorocarbon derivatives of N: synthesis vapour pressure studies of hydrogen of fluorinated indolizines through re- fluoride—antimony pentafluoride sys- actions of pyridinium ethoxycarbonyl- tem, 165 methylide or pyridinium phenacylide Aromatic compounds with perfluoropropene, perfluorobut- 3,5-bis(trifluoromethyl)pyrazole and 2-yne and 3,3,3-trifluoropropyne, some N-substituted derivatives, 283 407 convenient and high-yield synthesis for synthesis of asymmetric polyfluoro-diace- pyridinium and metal hexafluoro- tylene monomers, 229 complexes of V, Cr, Fe and Co, 171 Elsevier Sequoia/Printed in The Netherlands 442 fluoroalkylbenzenes: synthesis of (S)-2,3- Bromine dimethoxy-5-[(3-fluoro)propyl-6- addition of 1,2-dibromotetrafluoroethane hydroxy-N](1-ethyl-2-pyrrolidi- to alkynes by means of redox system, nyl)methyl benzamide, 149 295 fluorocarbon derivatives of N: synthesis reactions of difluoro and dibromo- of fluorinated indolizines through re- ketenes with silylated ketene acetals, actions of pyridinium ethoxycarbonyl- 217 methylide or pyridinium phenacylide with perfluoropropene, perfluorobut- Carboxylic acids 2-yne and 3,3,3-trifluoropropyne, synthesis of perfluoroalkyl carboxylic 407 acids by reaction of perfluoroalkyl io- instant ligands: structures of gaseous dides with electrogenerated superox- (F,P)S(CH,)3;S(PF,) and (F,P)SEt by ide ion, 357 electron diffraction; preparation of Chlorine [RuCl.(p-cymene)]2[u-(F2P)Y¥(CH2)q- instant ligands: structures of gaseous Y(PF.)] (Y =O, S; n=3-6) and (F,P)S(CH,);S(PF,) and (F,P)SEt by structure of [RuCl,(p-cymene)],[- electron diffraction; preparation of (F,P)O(CH;),O(PF,)] by X-ray crys- [RuCl,(p-cymene)]2[u-(F2P)Y(CH2),- tallography, 305 Y(PF;)] (Y =O, S; n=3-6) and perfluoroalkylation of 2-mercaptobenzo- structure of [RuCl,(p-cymene)],[[u- thiazole and its analogues with per- (F,P)O(CH2),O(PF2)] by X-ray crys- fluoroalkyl iodides by Sgnl reaction, tallography, 305 21 synthesis of ethylene a-chloro(2-F-alkyl polyhaloaromatics: synthesis of poly- and ethyl thio)acetates with a view to ob- perfluoro-1,3,5,7-tetrahydrobenzo[1,2- taining F-alkyl bicaudal surfactant c:4,5-c'] difurans, 131 precursors, 155 preparation of p-fluorophenols from unsaturated N compounds containing F: p-aminophenols: diazotization and reaction of 2,5-dichloro-1,1,1,6,6,6- fluorodediazoniation in pyridine—HF, hexafluoro-3,4-diazahexa-2,4-diene 299 with triethylamine and related reac- substitution of some fluoroaromatics us- tions, 207 ing [Pb(EPh),]” (E=S or Se) as Chromium source of EPh™ nucleophile, 93 convenient and high-yield synthesis for synthesis of: pyridinium and metal hexafluoro- aromatic compounds containing per- complexes of V, Cr, Fe and Co, fluoro-oxa-alkyl groups, 117 171 1,4-bis(p-aryloxy-tetrafluoropheny]l)- Clusters butadiyne monomers for nonlinear synthetic, spectroscopic and HPLC stud- optics, 75 ies of some substituted Os clusters esters of 3,3-dicyano-2-(trifluoro- containing pentafluorobenzoate li- methyl)acrylic acid and their reac- gand, 83 tions with arylamines, 323 Cobalt F-alkyl pyrazolo[1,5-a]pyrimidines, convenient and high-yield synthesis for 141 pyridinium and metal hexafluoro- fluoro-diacetylene monomers: 1,4- complexes of V, Cr, Fe and Co, 171 bis(2,4,6-triaryloxy-difluoro- Copper phenyl)butadiynes, 433 influence of fluoride ion on current effi- synthetic, spectroscopic and HPLC stud- ciency of pulse plating of, 257 ies of some substituted Os clusters Cysteine containing pentafluorobenzoate li- and arginine and lysine; synthesis of gand, 83 new F-alkyl amino-acid derivatives Arginine of, 197 and lysine and cysteine; synthesis of new F-alkyl amino-acid derivatives Decomposition of, 197 of phosphonofluoridates on glass, 277 Diazotization Fluorination and fluorodediazoniation in pyridine- Electrochemical, of derivatives of morpho- HF; preparation of p-fluorophenols line and piperidine, 53 from p-aminophenols, 299 Photochemical selective, of organic molecules using Hg(II) fluoride, 291 Electrochemistry | electrochemic.i fluorination of deriva- Fluorine tives of morpholine and piperidine, Unsaturated N compounds containing: re- 53 action of 2,5-dichloro-1,1,1,6,6,6-hexa- Electrogenerated superoxide ion fluoro-3,4-diazahexa-2,4-diene with tri- synthesis of perfluoroalkyl carboxylic ethylamine and related reactions, 207 acids by reaction of perfluoroalkyl iodides with, 357 Fluoro-compounds Electron diffraction Experimental surface activity measurements instant ligands: structures of gaseous of some fluorinated compounds in non- (F,P)S(CH,);S(PF,) and (F,P)SEt by aqueous medium, 103 electron diffraction; preparation of Fluoroalkylbenzenes: synthesis of (S)-2,3-di- [RuCl,(p-cymene)]>[4-(F2P)¥(CH2)q- methoxy-5-[(3-fluoro)propyl-6-hydroxy- Y(PF:)] (Y =O, S; n=3-6) and N](1-ethyl-2-pyrrolidinyl)methyl-benza- structure of [RuCl,(p-cymene)],[u- mide, 149 (F,P)O(CH,),O(PF,)] by X-ray crys- Fluorocarbon derivatives of N: synthesis of tallography, 305 fluorinated indolizines through reactions Emulsions of pyridinium ethoxycarbonylmethylide perfluorodimorpholinoalkanes as stabiliz- or pyridinium phenacylide with per- ing additives in perfluorocarbon- fluoropropene, perfluorobut-2-yne and emulsions, 335 3,3,3-trifluoropropyne, 407 Esters Highly fluorinated heterocycles: 2-difluoro- one-pot synthesis, novel, of trifluoromethyl- and 2-trifluoromethyl- hexa- and penta-fluoro-oxolans, 179 methylated £,y-unsaturated esters Instant ligands: structures of gaseous and nitriles, 349 (F,P)S(CH,)3;S(PF,) and (F,P)SEt by synthesis of, of 3,3-dicyano-2-(trifluoro- electron diffraction; preparation of methyl)acrylic acid and their reactions with arylamines, 323 [RuCl,(p-cymene)],[u-(F2P)Y(CH2),- Y(PF,)] (Y =O, S; n=3-6) and struc- synthesis of B-enaminoperfluoroesters, ture of [RuCl,(p-cymene)],[u-(F2P)O- B-imino-a-hydroperfluoroesters and (CH,),O(PF,)] by X-ray crystallography, B-amido-a-fluoroesters, 1 305 synthesis of ethylene a-chloro(2-F-alkyl Polyhaloaromatics: synthesis of poly- and ethyl thio)acetates with a view to ob- perfluoro-1,3,5,7-tetrahydrobenzo[1,2- taining F-alkyl bicaudal surfactant c:4,5-c’] difurans, 131 precursors, 155 Preparation of fluorinated analogues of Anthonomus grandis pheromone, 397 Fluorides Preparation of p-fluorophenols from p-ami- Decomposition of phosphonofluoridates on nophenols: diazotization and fluorodedi- glass, 277 azoniation in pyridine-HF, 299 Influence of fluoride ion on current effi- Substitution of some fluoroaromatics using ciency of pulse plating of Cu, 257 [Pb(EPh),;]~ (E=S or Se) as source of Photochemical selective fluorination of or- EPh~ nucleophile, 93 ganic molecules using Hg(II) fluoride, Synthesis of: 291 B-enaminoperfluoroesters, B-imino-a-hy- Preparation of p-fluorophenols from p-ami- droperfiluoroesters and B-amido-a- nophenols: diazotization and fluoro- fluoroesters, 1 dediazoniation in pyridine-HF, 299 ethylene a-chloro(2-F-alkyl ethyl Vapour pressure studies of hydrogen fluor- thio)acetates with a view to obtaining ide—antimony pentafluoride system, F-alkyl bicaudal surfactant precur- 165 sors, 155 444 F-alkyl amino-acid derivatives, new, of Preparation, novel, of polyfluoroalkyl sec- lysine, arginine and cysteine, 197 ondary and tertiary amines, 33 F-alkyl pyrazolo[1,5-a]pyrimidines, 141 Synthesis of asymmetric polyfluoro-diacety- fluorinated analogue of 5-aminoaevulinic lene monomers, 229 acid, potential inhibitor of porphyrin biosynthesis, 381 perfluoro-diacetylene monomers: 1,4- bis(2,4,6-triaryloxy-difluoro- Perfluoroalkylation of 2-mercaptobenzothia- phenyl)butadiynes, 433 zole and its analogues with perfluoroalkyl iodides by Spnl reaction, 21 di- Perfluorodimorpholinoalkanes as stabilizing additives in perfluorocarbon-emulsions, Reactions of difluoro and dibromoketenes with silylated ketene acetals, 217 335 Synthesis of aromatic compounds contain- tri- ing perfluoro-oxa-alkyl groups, 117 3,5-Bis(trifluoromethyl)pyrazole and some Synthesis of perfluoroalkyl carboxylic acids N-substituted derivatives, 283 by reaction of perfluoroalkyl iodides One-pot synthesis, novel, of trifluoromethy- with electrogenerated superoxide ion, 357 lated B,y-unsaturated esters and nitriles, 349 Synthetic utility of 3-(perfluoro-1,1-di- Synthesis of esters of 3,3-dicyano-2-(trifluo- methylbutyl)-1-propene: reactions of romethyl)acrylic acid and their reactions 3-(perfluoro-1,1-dimethylbutyl)-1,2-epoxypropane with inorganic anions, thiourea with arylamines, 323 and guanidine, 43 tetra- Addition of 1,2-dibromotetrafluoroethane Furans to alkynes by means of redox system, polyhaloaromatics: synthesis of poly- and 295 perfluoro-1,3,5,7-tetrahydrobenzof 1,2- Synthesis of 1,4-bis(p-aryloxy-tetrafluoro- c:4,5-c'] difurans, 131 phenyl)butadiyne monomers for nonlinear optics, 75 Glass penta- decomposition of phosphonofluoridates Synthetic, spectroscopic and HPLC studies on, 277 of some substituted Os clusters contain- Guanidine ing pentafluorobenzoate ligand, 83 synthetic utility of 3-(perfluoro-1,1-dimethylbutyl)-l-propene: reactions of hexa- 3-(perfluoro-1,1-dimethylbutyl)-1,2- Convenient and high-yield synthesis for epoxypropane with inorganic anions, pyridinium and metal hexafluoro- thiourea and guanidine, 43 complexes of V, Cr, Fe and Co, 171 Unsaturated N compounds containing F: reaction of 2,5-dichloro-1,1,1,6,6,6-hexa- Halo-compounds fluoro-3,4-diazahexa-2,4-diene with tri- polyhaloaromatics: synthesis of poly- and ethylamine and related reactions, perfluoro-1,3,5,7-tetrahydrobenzof 1,2- 207 c:4,5-c’] difurans, 131 preparation of perhaloacrylic derivatives, octa- 223 Synthesis and structural study of dihydra- Heterocycles zinium octafluorostannate(IV): (N>H,)>- highly fluorinated: 2-difluoromethyl- and SnF,F,, 245 2-trifluoromethyl- hexa- and penta- fluoro-oxolans, 179 poly- HPLC studies Amine(polyfiuoroalkoxyacyl)imide sur- and synthetic and spectroscopic studies factants, 419 of some substituted Os clusters con- 445 taining pentafluorobenzoate ligand, with perfluoropropene, perfluorobut- 83 2-yne and 3,3,3-trifluoropropyne, 407 one-pot synthesis, novel, of trifluoro- lodine methylated B,y-unsaturated esters perfluoroalkylation of 2-mercaptobenzo- and nitriles, 349 thiazole and its analogues with per- unsaturated N compounds containing F: fluoroalkyl iodides by Spxl reaction, reaction of 2,5-dichloro-1,1,1,6,6,6- 21 hexafluoro-3,4-diazahexa-2,4-diene synthesis of perfluoroalkyl carboxylic with triethylamine and related reac- acids by reaction of perfluoroalkyl io- tions, 207 dides with electrogenerated superoxide ion, 357 Optics Iron nonlinear; synthesis of 1,4-bis(p-aryloxy- convenient and high-yield synthesis for tetrafluorophenyl)butadiyne mono- pyridinium and metal hexafluoro- mers for, 75 complexes of V, Cr, Fe and Co, 171 Osmium synthetic, spectroscopic and HPLC studies of some substituted Os clusters Ketene acetals containing pentafluorobenzoate li- silylated; reactions of difluoro and di- gand, 83 bromoketenes with, 217 Pheromone Lead preparation of fluorinated analogues of substitution of some fluoroaromatics us- Anthonomus grandis pheromone, 397 ing [Pb(EPh),]” (E=S or Se) as Phosphonofluoridates source of EPh™ nucleophile, 93 decomposition of, on glass, 277 Lysine Photochemistry and arginine and cysteine; synthesis of photochemical selective fluorination of new F-alkyl amino-acid derivatives organic molecules using Hg(II) fluor- of, 197 ide, 291 Piperidine Mercury and morpholine; electrochemical fluori- photochemical selective fluorination of nation of derivatives of, 53 organic molecules using Hg(II) fluor- Porphyrin biosynthesis ide, 291 synthesis of fluorinated analogue of Monomers 5-aminoaevulinic acid, potential in- synthesis of asymmetric polyfluoro-diace- hibitor of, 381 tylene monomers, 229 Pulse plating synthesis of 1,4-bis(p-aryloxy-tetrafluoro- influence of fluoride ion on current effi- phenyl)butadiyne monomers for non- ciency of, of Cu, 257 linear optics, 75 synthesis of fluoro-diacetylene mono- Ruthenium mers: 1,4-bis(2,4,6-triaryloxy-difluoro- instant ligands: structures of gaseous phenyl)butadiynes, 433 (F,P)S(CH,);S(PF,) and (F,P)SEt by Morpholine electron diffraction; preparation of and piperidine; electrochemical fluorina- [RuCl,(p-cymene)],[u-(F2P)Y(CH2),- tion of derivatives of, 53 Y(PF,)] (Y =O, S; n=3-6) and structure of [RuCl,(p-cymene)],[- Nitrogen (F,P)O(CH;),O(PF2)] by X-ray crys- 3,5-bis(trifluoromethyl)pyrazole and tallography, 305 some N-substituted derivatives, 283 fluorocarbon derivatives of N: synthesis Selenium of fluorinated indolizines through re- substitution of some fluoroaromatics us- actions of pyridinium ethoxycarbonyl- ing [Pb(EPh),]” (E=S or Se) as methylide or pyridinium phenacylide source of EPh™ nucleophile, 93 446 Silylated ketene acetals Surface activity measurements reactions of difluoro and dibromo- experimental, of some fluorinated com- ketenes with, 217 pounds in non-aqueous medium, 103 Spectroscopy Surfactants amine(polyfluoroalkoxyacyl)imide surfac- synthetic, spectroscopic and HPLC stud- tants, 419 ies of some substituted Os clusters synthesis of ethylene a-chloro(2-F-alkyl- containing pentafluorobenzoate li- ethyl thio)acetates with a view to ob- gand, 83 taining F-alkyl bicaudal surfactant Structural study precursors, 155 and synthesis of dihydrazinium octafluorostannate(IV): (N2H,)2SnF,F2, Thiourea 245 synthesis utility of 3-(perfluoro-1,1-di- Sulphur methylbutyl)-1-propene: reactions of instant ligands: structures of gaseous 3-(perfluoro-1,1-dimethylbutyl)-1,2- (F,P)S(CH;);S(PF,) and (F,P)SEt by epoxypropane with inorganic anions, electron diffraction; preparation of thiourea and guanidine, 43 [RuCl,(p-cymene)]>[u-(F2P)Y(CH)2),- Tin Y(PF.)] (Y =O, S; n=3-6) and synthesis and structural study of di- structure of [RuCl.(p-cymene)],[yu- hydrazinium octafluorostannate(IV): (F,P)O(CH2),O(PF2)] by X-ray crys- (N,H,)2SnF,F2, 245 tallography, 305 perfluoroalkylation of 2-mercaptobenzo- Vanadium thiazole and its analogues with per- convenient and high-yield synthesis for fluoroalkyl iodides by Sgnl reaction, pyridinium and metal hexafluoro- 21 complexes of V, Cr, Fe and Co, 171 Vapour pressure studies substitution of some fluoroaromatics us- of hydrogen fluoride—antimony penta- ing [Pb(EPh);]” (E=S or Se) as fluoride system, 165 source of EPh™ nucleophile, 93 synthesis of ethylene a-chloro(2-F-alkyl X-ray crystallography ethyl thio)acetates with a view to ob- instant ligands: structures of gaseous taining F-alkyl bicaudal surfactant (F,P)S(CH,);S(PF,) and (F,P)SEt by precursors, 155 electron diffraction; preparation of synthetic utility of 3-(perfluoro-1,1-di- [RuCl,(p-cymene)]},[u-¥((FCH22P)),- methylbutyl)-1-propene: reactions of Y(PF,)] (Y =O, S; n=3-6) and 3-(perfiluoro-1,1-dimethylbutyl)-1,2- structure of [RuCl,(p-cymene)],[u- epoxypropane with inorganic anions, (F,P)O(CH2),O(PF2)] by X-ray crys- thiourea and guanidine, 43 tallography, 305