IS 7635: 2-Nitroaniline-Specification

11 Pages·1992·1.2 MB·English

by  Bureau of Indian Standards

इंटरनेट मानक
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timely dissemination of this information in an accurate manner to the public.
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IS 7635 (1992): 2-Nitroaniline-Specification [PCD 9:
Organic Chemicals Alcohols and Allied Products and Dye
Intermediates]
“!ान $ एक न’ भारत का +नम-ण”
Satyanarayan Gangaram Pitroda
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“Knowledge is such a treasure which cannot be stolen”

IS 7636 : 1992

Indian Standard
2-NITROANILINE-SPECIFICAT4ON
( Second Revision
)
UDC 667.21 : 547.551-54
8 BIS 1992
BUREAU OF INDIAN STANDARDS
UANAK BHAVAN, 9 BAHADUR SHAH ZAEAR MARG
NEW DEL HI 110002
December 1992 Price Group 2
eyD setaidemretnI lanoitceS ,eettimmoC PCD 11
FOREWORD
sihT naidnI dradnatS ( tsriF noisiveR ) was detpoda yb eht uaeruB fo naidnI Standards, retfa eht tfard
dezilanif yb eht yrD setaidemretnI lanoitceS eettimmoC had neeb devorppa yb eht ,muelorteP laoC
and detaleR stcudorP noisiviD .licnuoC
enilinaortiN-2 ( CJ-I,N,O, ) is an etaidemretni desu ni eht erutcafunam fo sffutseyd and .stnemgip tI is
osla desu as a ozaid tnenopmoc ni cioza gnieyd ni hcihw esac ti is nwonk as tsaf egnaro RG .esab tI
is osla nwonk as .eneznebonima-1-ortin-2 tI has eht gniwollof larutcurts :alumrof
L
z”N
I
( Molecular ssaM 831 )
C. .A .S Registration .oN [ 88-74-4 ]
2-NITROANILINB
sihT standard was issued ni 1975. ehT eettimmoc elbisnopser rof eht noitaraperp dediced ot esiver ti
ni redro ot etaroprocni eht stnemeriuqer as rep eht devorpmi ytilauq fo eht lairetam gnieb decudorp
ni eht .yrtnuoc nI eht tneserp noisrev eht stnemeriuqer fo yassa and gnizillatsyrc tniop evah neeb -pu
detad and eht tnemeriuqer fo seitirupmi enilinaortiN-3( and enilinaortiN-4 tnetnoc ) evah neeb
.detaroprocni
roF eht esoprup fo gnidiced rehtehw a ralucitrap tnemeriuqer fo this standard is deilpmoc ,htiw eht
lanif ,eulav devresbo ro ,detaluclac gnisserpxe eht tluser fo a tset ro ,sisylana shall eb dednuor ffo
ni ecnadrocca htiw SI 2 : 1960 seluR‘ rof gnidnuor ffo laciremun seulav (revised )‘. ehT rebmun fo
tnacifingis secalp deniater ni eht dednuor ffo eulav dluohs eb eht emas as that fo eht deificeps eulav ni
this standard.
IS 7635 : 1992
Indian Standard
2-NITROANILINE-SPECIFICATION
(S econd Revision )
1 SCOPE enelyhteylop ,mlif ro as deerga ot neewteb eht
resahcrup and eht .reilppus
sihT standard sebircserp eht stnemeriuqer and
eht sdohtem fo sampling and tset rof -inaortiN-2 4.2 Marking
.enil
hcaE reniatnoc shall raeb ylbigel and ylbiledni
2 SECNEREFER eht gniwollof !noitamrofni
ehT gniwollof naidnI Standards era yrassecen 4 emaN fo eht ;lairetam
stenujda ot this standard:
b) noitacidnI fo eht ecruos fo ;erutcafunam
SI .oN eltiT
cl ssorG and ten mass;
1070 : 1992 tnegaeR edarg retaw - -acificepS
noit ( third revision ) d) hctaB ;rebmun and
e>
1997 : 1982 setteruB (second revision ) ehT muminim yranoituac eciton dedrow
as :rednu
2552 : 1939 leetS drums ( dezinavlag and -nu
dezinavlag ) ( third revision ) REGNAD‘ ! SUODRAZAH DILOS AND
VAPOURS YLDIPAR DEBROSBA
5299 : 1969 sdohteM fo sampling and stset HGUORHT ’NIKS
rof eyd setaidemretni
4.2.1 ehT sreniatnoc yam osla eb dekram htiw-
3 STNEMERIUQER eht dradnatS Mark.
3.1 noitpircseD
5 GNILPMAS
ehT lairetam shall eb ni eht mrof fo egnaro ot
nedlog wolley enillatsyrc .seldeen 5.1 evitatneserpeR samples fo eht lairetam shall
eb drawn as debircserp ni 3 fo SI 5299 : 1969.
3.2 ehT lairetam shall eb ylthgils elbulos ni
retaw and elbulos ni lohocla and .rehte
5.2 rebmuN fo stseT
3.3 ehT lairetam shall osla ylpmoc htiw eht
stnemeriuqer nevig ni elbaT 1. gnizillatsyrC ,tniop yassa and seitirupmi fo hcae
laudividni elpmas shall eb denimreted .yletarapes
elbaT 1 tnemeriuqeR rof enilinaortiN-2
5.3 airetirC rof ytimrofnoC
S1 Characteristic Requirement Method of Test, ehT tol shall‘ eb deralced as gnimrofnoc ot eht
No. Ref to standard fi eht tset stluser as deniatbo ni 5.2
(1) (2) (3) (4) yfsitas eht gnidnopserroc stnemeriuqer nevig ni
)i gFkl!lag;rC ,tniop 69’0 7.1.2 of elbaT 1.
3 IS 5299 : 1969
)ii sil”nssA ’n;;p yb 98’5 xennA A 6 TSET SDOHTEM
)iii enilihortiN-3 -noc 0’2 xennA B 6.1 stseT shall eb detcudnoc gnidrocca ot
,tnet tnecrep yb
sdohtem debircserp ni 1oc 4 fo elbaT 1.
,ssam Max
)vi -noc_enilynaortiN-4 0’2 xennA B
,tnet tnecrep yb 6.2 ytilauQ fo stnegaeR
,ssam Max
Unless deificeps esiwrehto erup‘ ’slacimehc and
4 GNIKCAP AND GNIKRAM dellitsid retaw ees( SI 1070 : 1392 ) shall eb
deyolpme ni .stset
4.1 gnikcaP
ehT lairetam shall eb dekcap ni leets drums NOTE - eruP‘ ’slacimehc llahs naem slacimehc taht
od ton niatnoc seitirupmi hcihw tceffa eht stluser fo
( ees 1s 2552 : 1989 ) denil htiw elbatius .sisylana
1
IS 7635 : 1992
ANNEX A
[ Tuble 1, Item (ii) ]
METHOD OF DETERMINATION OF ASSAY
A-l ~OUTLINE OF THE METHOD refsnart ot a 1 lm-OOO .rekaeb evlossiD ni 500
lm fo retaw and 50 lm fo a detartnecnoc -ordyh
A nwonk ytitnauq fo eht elpmas is detartit ’htiw cirolhc dica and ,taeh fi .yrassecen Add dehsurc
muidos etirtin noitulos ni dica .muidem ehT
eci otni eht rekaeb and rits eht erutxim -ahcem
tnuoma fo muidos etirtin noitulos demusnoc
yllacin litnu eht erutarepmet is tuoba 0 ot
yam eb desserpxe ni smret fo eht tnuoma fo eht
5°C. elihW gnirrits yllacinahcem add eht -ulos
enima .tneserp
noit fo standard muidos etirtin morf eht etterub
2-A REAGENTS as yldipar as eht tops tset stimrep gnipeek eht
erutarepmet woleb .%5 tseT eht noitulos yb
A-2.1 muidoS etirtiN noituloS -- 0.1 N, ylhserf gnittops no hcrats &idoi .repap fI eht etar fo
dezidradnats against erup cilinahplus .dica noitazitozaid is ,wols add a wef lm fo muissatop
edimorb noitulos ot niatbo reprahs dne .tniop
2.2-A detartnecnoC cirolhcordyH dicA - 30
ehT dne tniop is dehcaer fi an etaidemmi tniaf
tnecrep ( m/v ).
eulb deruoloc gnir sraeppa nehw eht noitulos is
A-2.3 Starch Iodide Test Papers dettops no hcrats :hcidoi repap and hcihw -rep
sists rof a doirep fo 5 setunim ro os tuohtiw
A-2.4 Potassium Bromide Solution - 25 tnecrep rehtruf noitidda fo etirtin .noitulos
( v/m .)
5-A NOITALUCLAC
3-A SUTARAPPA
1.3-A lacinahceM rerritS ,yassA tnecrep yb mass = V x N x 13.8
M
2.3-A etteruB - ees SI 1997 : 1982.
erehw
3.3-A srekaeB
V = ,emulov ni ,lm fo standard muidos
4.3-A retemomrehT - elbatiuS ot erusaem
etirtin noitulos ;desu
erutarepmet ni eht egnar fo 0 ot 5°C.
N =, ytilamron fo eht muidos etirtin -uios
4-A PROCEDURE ;noit and
hgieW yletarucca tuoba 1 g fo eht elpmas and M = mass, ni g, fo eht elpmas nekat rof .tset
ANNEX B
[ Table 1, Item )ii( and )vi( ]
NOITANIMRETED FO ENILINAORTIN-3 AND ENILINAORTIN-4
l-B ENILTUO FO EHT DOHTEM 4.2-B siortiN semuF rebmahC
enilinaortiN-3 and enilinaortin-4 era denimreted A glass rebmahc fo ezis 250 mm x 250 mm htiw
yb niht reyal .yhpargotamorhc a rekaeb fo yticapac lm-OOl gniniatnoc -ixorppa
yletam 50 lm fo detartnecnoc lCH ( 30 tnecrep
2-B STNEGAER m/v ). ehT suortin semuf era detareneg yb -dda
gni a ttil e sdlid muidos etirtin emityreve erofeb
1.2-B enilinaortiN-3 eruP 1 eraperP 0.004 gnitresni eht .etalp
( ecnerefeR ) ,tnecrep
0.008 ,tnecrep 5.2-B yarpS tnegaeR
I
2.2-B enilinaortiN-4 eruP 1 0.02 tnecrep -ulos
0.1 tnecrep ( noitulos fo naciremA esaB
( ecnerefeR ) ? snoit fo hcae m/v )
1 enilinaortin-3 and enelyhtelyhthpaN-1-N( )edirolhcordyhidenimaid
enilinaortin-4 ni ni .lonahtem
1 .lonahtem
3-B SUTARAPPA
3.2-B tneulE
1.3-B Thin Layer Chromatographic Chamber -
enezneB : etatecalyhte ( 96 : 4 ) 250 mm x 100 mm x 250 .mm
2
IS 7635:1 992
B-3.2 Micropipette of 10 Microlitre Capacity tuoba 03-52 setunim gnirud hcihw emit eht -los
tnev tnorf slevart yletamixorppa 10 mc past eht
B-3.3 Pre-coated Thin Layer Chromatography start .enil evomeR eht etalp morf eht rebmahc
Plates and yrd ni .ria retfA gniyrd tup eht etalp ni eht
CLT setalp ( 200 mm x 200 mm ) detaoc htiw suortin semuf rebmahc rof tuoba 30 .sdnoces
acilis ,leg tuoba 52-O mm ssenkciht and htiw a evomeR eht ssecxe suortin semuf yb gniwolb ria
ecnecseroulf fo 452-F .mn no .ti yarpS eht etalp htiw naciremA esab )5.2-B(
nehw eht stops der( teloiv ) scitsiretcarahc fo
4-B PROCEDURE enilinaortin-3 and enilinaortin4 emoceb elbisiv
at Rf 34-O and 92-O .ylevitcepser
B-4.1 hgieW yletarucca tuoba 4 g fo eht elpmas
{ 100 tnecrep basis ) and evlossid ni 100 ,lm
.lonahtem ekaT a etalp detaoc htiw acilis leg B-4.2 Reporting
and tops 10 sertil fo hcae fo eht tset noitulos
and ecnerefer snoitulos gnola eht start enil at a etamitsE eht seititnauq fo eht seitirupmi yb
ecnatsid fo 3 mc morf eno .rehtona etarutaS eht gnirapmoc eht ruoloc i ytisnet fo eht stops fo
cihpargotamorhc rebmahc htiw .tneule tresnI eh-t lairetam rednu set pt htiw esoht fo eht
eht etalp ni eht rebmahc and wolla ot nur rof samples.
reference
3
Standard Mark
ehT esu fo eht dradnatS Mark is denrevog yb eht snoisivorp fo eht Bureau of Indian
Standards Act, 689I and eht seluR and snoitalugeR edam .rednuereht ehT dradnatS Mark no
stcudorp derevoc yb an naidnI dradnatS syevnoc eht ecnarussa that yeht evah neeb
decudorp ot ylpmoc htiw eht stnemeriuqer fo that standard rednu a llew denifed metsys fo
,noitcepsni gnitset and ytilauq lortnoc hcihw is desived and desivrepus yb SIB and detarepo
yb eht .recudorp dradnatS dekram stcudorp era osla ylsuounitnoc dekcehc yb STB rof -noc
ytimrof ot that standard as a rehtruf .draugefas sliateD fo snoitidnoc rednu hcihw a ecnecil
rof eht esu fo eht dradnatS Mark yam eb detnarg ot srerutcafunam ro srecudorp yam eb
deniatbo morf eht uaeruB fo naidnI Standards.
Barea~ of Indian Standarda
SIB is a yrotutats noitutitsni dehsilbatse rednu eht Bureau of Indian Stand&is Act, 1986 ot etomorp
suoinomrah tnempoleved fo eht seitivitca fo ,noitazidradnats gnikram and ytilauq noitacifitrec fo sdoog
and gnidnetta ot detcennoc srettam ni eht .yrtnuoc
thgirypoC
SIB has eht thgirypoc fo all its .snoitacilbup oN trap fo eseht snoitacilbup yam eb decudorper ni any
mrof tuohtiw eht roirp noissimrep ni gnitirw fo .SIB sihT seod ton edulcerp eht eerf ,esu ni eht esruoc fo
gnitnemelpmi eht standard, fo yrassecen ,sliated hcus as slobmys and ,sezis epyt ro edarg .snoitangised
seiriuqnE gnitaler ot thgirypoc eb desserdda ot eht rotceriD ( snoitacilbuP ,) .SIB
Revision of Indian Standards
naidnI Standards era deweiver yllacidoirep and ,desiver nehw yrassecen and ,stnemdnema fi ,yna era
issued morf emit ot .emit sresU fo naidnI Standards dluohs niatrecsa that yeht era ni noissessop fo eht
tsetal stnemdnema ro .noitide stnemmoC no this naidnI dradnatS yam eb tnes ot SIB gnivig eht
gniwollof :ecnerefer
toD : .oN PCD 11 ( 908 )
Amendments Issued Since Publication
dnemA .oN etaD fo issue txeT detceffA
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