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IS 4467: Caramel PDF

24 Pages·1996·2.2 MB·English
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इंटरनेट मानक Disclosure to Promote the Right To Information Whereas the Parliament of India has set out to provide a practical regime of right to information for citizens to secure access to information under the control of public authorities, in order to promote transparency and accountability in the working of every public authority, and whereas the attached publication of the Bureau of Indian Standards is of particular interest to the public, particularly disadvantaged communities and those engaged in the pursuit of education and knowledge, the attached public safety standard is made available to promote the timely dissemination of this information in an accurate manner to the public. “जान1 का अ+धकार, जी1 का अ+धकार” “प0रा1 को छोड न’ 5 तरफ” Mazdoor Kisan Shakti Sangathan Jawaharlal Nehru “The Right to Information, The Right to Live” “Step Out From the Old to the New” IS 4467 (1996): Caramel [FAD 8: Food Additives] “!ान $ एक न’ भारत का +नम-ण” Satyanarayan Gangaram Pitroda ““IInnvveenntt aa NNeeww IInnddiiaa UUssiinngg KKnnoowwlleeddggee”” “!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता हहहहै””ै” Bhartṛhari—Nītiśatakam “Knowledge is such a treasure which cannot be stolen” IS4467:1996 *m 4tTm-- R .Rfm (w@m) Indian Standard CARAMEL-SPECIFICATION ( Second Revision ICS 67.220.20 0 BIS 1996 BUREAU OF INDIAN STANDARDS MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG NEW DELHI 110002 October 6991 Price Croup 8 dooF sevitiddA lanoitceS ,eettimmoC FAD 8 FOREWORD sihT naidnI dradnatS dnoceS( )noisiveR was detpoda yb eht uaeruB fo naidnI Standards, retfa eht tfard dezilanif yb eht dooF sevitiddA lanoitceS eettimmoC had neeb devorppa yb eht dooF and erutlucirgA noisiviD .licnuoC ehT mret lemarac seod ton etoned a elgnis lacimehc .ecnatsbus A ediw egnar fo tnereffid sepyt fo lemarac era derutcafunam ot suit eht stnemeriuqer fo ralucitrap .sresu sihT standard, ,erofereht seificeps stimil rof lufmrah seitirupmi and hcus scitsiretcarahc as lliw erusne an elbatpecca standard fo .ythauq ,revewoH deliated snoitacificeps gnipeek ni weiv eht cificeps sdeen yam eb deerga ot neewteb eht sresu and eht .srerutcafunam ehT standard was tsrif issued ni 1967. tI was desiver ni 1980 and dehsilbup ni 3 parts, hcae trap gnirevoc a tnereffid epyt fo ,lemarac yleman plain, ainomma ssecorp and ainomma etihplus .ssecorp gnipeeK ni weiv eht stnempoleved ni edart ecitcarp and htiw a weiv ot gningila ti htiw lanoitanretnI Standards, this standard is won gnieb desiver ot revoc lemarac ni eno standard rednu eht gniwollof 4 .sepyt epyT I ,nialP citsuac ;lemarac eP5 II Caustic etihplus ;lemarac epyT III ainommA ssecorp ;lemarac and epyT VI ainommA etihplus .lemarac nI eht noitaraperp fo this standard, eud noitaredisnoc has neeb nevig ot eht snoisivorp rednu eht 1955. ,revewoH this standard is tcejbus ot eht snoitcirtser desopmi Prevention of FoodAdulteration Rules, rednu eseht ,seluR reverehw .elbacilppa esehT selur aila-retni ebircserp llA doof sruoloc gnidulcni( larutan gniruoloc srettam and dettimrep citehtnys doof ,sruoloc rieht snoitaraperp ro serutxim tpecxe norffas and )nimucrac shall eb dlos ylno rednu eht uaeruB fo naidnI Standards noitacifitreC Mark’. lemaraC is a larutan gniruoloc .rettam elbaredisnoC assistance has neeb devired morf eht gniwollof noitacilbup ni noitaraperp fo siht :dradnats noitacificepS rof ytitnedi and ytirup fo emos doof ,sevitidda FAO noitirtuN gniteeM tropeR seireS .oN 38. ,OHWOAF ,emoR 1958. roF eht esoprup fo gnidiced rehtehw a ralucitrap tnemeriuqer fo this standard is deilpmoc ,htiw eht lanif ,eulav devresbo ro ,detaluclac gnisserpxe eht tluser fo a tset ro ,sisylana shall eb dednuor ffo ni ecnadrocca htiw SI 2 : 1960 seluR‘ rof gnidnuor ffo laciremun seulav (revised)‘. The rebmun fo tnacifingis secalp deniater ni eht dednuor ffo eulav dluohs eb eht emas as that fo eht deificeps eulav ni this standard. IS 4467 : 1996 Indian Standard CARAMEL - SPECIFICATION ( Second Revision ) 1 EPOCS ,setagergga derutcafunam yb gnitaeh setardyhobrac rehtie enola ro ni eht ecneserp fo edargdoof -xe( 1.1 sihT standard sebircserp eht stnemeriuqer and ylemert doog )ytilauq ,sdica alkalis, ro salts -dulcni sdohtem fo sampling and tset rof lemarac rof esu ni gni muidos and muissatop salts. yehT era deifissalc .sffutsdoof gnidrocca ot eht stnatcaer desu ni rieht -cafunam 2 SECNEREFER erut as :swollof ehT naidnI Standards detsil woleb niatnoc 4.1.1 Type I, Plain, Caustic Caramel snoisivorp hcihw hguorht ecnerefer ni this ,txet tI shall eb deraperp yb gnitaeh setardyhobrac htiw etutitsnoc noisivorp sihtfo standard. At eht emit fo ro tuohtiw ,sdica alkalis ro salts. oN muinomma ro ,noitacilbup eht snoitide detacidni erew .dilav llA etihplus sdnuopmoc era .desu tI is yltsom desu ni standards era tcejbus ot noisiver and seitrap ot tirips .yrtsudni stnemeerga desab no this standard era degaruocne ot etagitsevni eht ytilibissop fo gniylppa eht tsom 41.2 Type II, Caustic Sulphite Caramel tnecer snoitide fo eht standards .detacidni tI shall eb deraperp yb gnitaeh setardyhobrac htiw IS No. eltiT ro tuohtiw ,sdica alkalis ro salts ni eht ecneserp fo etihplus ;sdnuopmoc on muinomma sdnuopmoc 1070 : 1992 tnegaeR edarg retaw (third era .desu revision) 1699: 1995 sdohteM fo sampling and tset rof 4.1.3 Type II& Ammonia Process Caramel citehtnys doof sruoloc dnoces( tI shall eb deraperp yb gnitaeh setardyhobrac htiw eY vision) ro tuohtiw ,sdica alkalis ro salts ni eht ecneserp fo muinomma .sdnuopmoc oN etihplus sdnuopmoc :1942 1972 edoC rof cineigyh snoitidnoc rof era .desu tI is yltsom desu ni egareveb and reeb doof gnissecorp units (jirst .yrtsudni revision) 4.1.4 Tylle Iv Ammonia Sulphite Caramel 3 YGOLONIMRET tI shall eb deraperp yb gnitaeh setardyhobrac htiw roF eht esoprup fo this standard, eht gniwollof ro tuohtiw ,sdica alkalis ro salts ni eht ecneserp fo snoitinifed shall .ylppa htob etihplus and muinomma .sdnuopmoc tI is 3.1 epyT stseT yltsom desu ni eht tfos knird .yrtsudni stseT ot evorp ytimrofnoc ot eht slnemeriuqcr fo this standard. yehT era dednetni ot evorppa eht 5.1 ehT etardyhobrac raw slairetam desu era -doof noitalumrof and ytilauq fo eht tcudorp at tsael ni edarg evitirtun sreneteews gnitsisnoc fo ,esorcus eht gninnigeb fo gnitekram ro/dna .noitacifitrec ,esoculg ,esotcurf trevni sugar, ,esotcal tlam ,purys esehT stset era osla detcudnoc yllacidoirep ot sup- ,sessalom hcrats setasylordyh and snoitcarf foereht tnemelp eht enituor stset ro revenehw eht cisab ro/dna sremylop .foereht alumrof ro dohtem is .degnahc 5.2 ehT sdica desu era doof edarg ylemertxe( doog 3.2 enituoR stseT )ytilauq ciruhplus ,dica cirohpsohp ,dica citeca ,dica stseT deirrac tuo no hcae tol ot kcehc eht laitnesse ro cirtic dica and eht alkalis desu era doof edarg stncmcriuqer that era ylekil ot yrav gnirud -cudorp ylemertxe( doog )ytilauq ,muidos muissatop ro -lac .noit muic edixordyh ro serutxim .foereht 4 SEPYT 5.3 ehT salts desu era doof edarg muidos ro -satop sium ,etanobrac ,etanobracib setahpsohp -dulcni( 4.1 lemaraC sruoloc era xelpmoc serutxim fo -moc gni cisabid etahpsohp and cisabonom )etahpsohp sdnuop emos fo hcihw era ni eht mrof fo ladiolloc and sulphates. 1 SI 6991:7644 4.5 erehW muinomma sdnuopmoc era ,desu yeht 1.1.6 Description shall eb eno ro erom fo eht :gniwollof lemaraC shall eb a krad nworb ot kcalb diuqil ro muinommA edixordyh dilos lairetam gnivah eht citsiretcarahc ruodo fo muinommA etanobrac and etanobracib tnrub sugar and a ,tnasaelp rettib .etsat tI shall eb muinommA etahpsohp elbicsim htiw .retaw Its ,snoitulos nehw daerps ni a muinommA etahplus niht reyal no a glass etalp dluohs raeppa muinommA ,etihplus etihplusib and ,suonegomoh tnerapsnart and evah nworb-hsidder etihplusibatem .ruoloc lemaraC shall eb eerf morf yna rehto -xe suoenart gniruoloc .rettam 5.5 etihpluserehW sdnuopmoc era ,desu yeht shall eb eno ro erom fo eht :gniwollof 6.1.2 ehT lairetam shall osla mrofnoc ot eht -er stnemeriuq nevig ni elbaT 1. llA stnemeriuqer era suoruhpluS dica no dilos basis, tpecxe cillatem .seitirupmi ,muissatoP muidos ro muinomma setihplus ro 6.2 epyT tseT .setihplusib 6.2.1 ehT lairetam shall osla mrofnoc ot eht -er 5.6 lorecylgyloP sretse fo yttaf ,sdica nroc lio ro stnemeriuq nevig ni elbaT 2. llA stnemeriuqer era rehto doof edarg smaofitna dettimrep rednu eht no dilos basis tpecxe cillatem .seitirupmi AFP seluR yam eb desu as gnimaofitna stnega gnirud .erutcafunam 6.3 roF noitaluclac no dilos basis, refer xennA J. 6 STNEMERIUQER 6.4 ehT tcudorp shall eb ,dessecorp ,dekcap derots and detubirtsid rednu cineigyh snoitidnoc ni 6.1 enituoR stseT desnecil sesimerp ees( SI 2491 : 1972). elbaT 1 enituoR tseT stnemeriuqeR rof lemaraC esualC( )2.1.6 Sl Chnrncterislics Melhod of ,tseT feR ol epyT II epyT III epyT VI citsuaC ainommA etihpluS of sihT SI 1699 : etihpluS ssecorP ainommA dradnatS 1995 6 )1( )2( ( 3) (4) (5) (6) (7) (8) 0 diloS ,tnetnoc 62 - 77 65-72 53-83 40 - 75 A - percent yb ssam )ii ruoloC ,ytisnetni 0.01 - 0.12 0.06 - 0.10 0.08 - 0.36 0.10 - 0.60 B - tnecrep yb ssam )iii lacainommA 0.01 10.0 0.4 0.5 c - ,negortin tnecrep yb ,ssam MUX (see setoN 1 dna 2) )vi elozadimilyhteM-4 - - 300and200on lOOOand250on D - ,)IEM-4( ,gk/gm Max na tnelaviuqe na tnelaviuqe (see setoN 1 dna 2) colour sisab ruoloc sisab )v daeL sa( ,)bP 5 5 5 5 - 15 ,gkgm Mm )iv cinesrA sa( ,)sA 3 3 3 3 - 15 ,gkigm Mar NOTES 1 tnemeriuqeR fo lacinomma negortin si desab no a tcudorp gnivah a muminim ruoloc ytisnetni debircserp at IS .oN ;)ii yletanoitroporp rehgih seulav rof lacinomma negortin ylppa rof stcudorp fo rehgih ruoloc .ytisnetni 2 roF stimil desserpxe no tnelaviuqe ruoloc ,sisab ees snoitaluclac nevig at xennA .B 2 IS 4467 : 1996 Table 2 Type Test Requirements for Caramel (Clause 6.2.1) SI scitsiretcarahC stnemeriuqeR dohteM fo Test, Ref to No. l)pe II epyT III VIepyT ’ rAnnex citsuaC ainommA etihpluS fo sihT SI 1699 : etihpluS ssecorP ainommA dradnatS 1995 )1( )2( (3) (4) (5) (6) (7) (8) 0 Total ,ruhpfus ,raM 0.3 1.3 - 2.5 Mm, 0.3 1.4 - 10.0 E - tnecrep yb ssam )ii ruhpluS edixoid sa( &OS - 0.2 - 0.5 F - tnecrep yb ,ssam Mar )iii Total ,negortin Max, 0.1 Mar, 0.2 1.3 - 6.8 0.5 - 5.1 G - tnecrep yb ssam )vi yvaeH ,slatem ,gkgm Mau 25 25 25 25 - 16 )v yxordyhartet-4-lytecA-2 - - 40and25onan - H - elozadimilytub (THI), tnelaviuqe ruoloc ,gkgm Max sisab (see setoN 1 dna 2 woleb elbaT 1) )iv yrucreM sa( ,)gH ,gk/gm Ma 0.1 0.1 0.1 0.1 - 15 )iiv ,reppoC ,gkgm Mau 20 20 20 20 - 15 7 PACKING AND MARKING 7.2.1 BIS Certification Marking tcudorp yam osla eb dekram htiw eht dradnatS 7.1 Packing The Mark. ehT lairetam shall eb dellif ni deruoloc-rebma glass ro hgih ytisned enelyhteylop sreniatnoc ro yna 7.2.1.1 ehT esu fo eht dradnatS Mark is denrevog rehto desolc-llew elbatius sreniatnoc htiw as elttil yb eht snoisivorp fo eht Bureau of Indian Standards ria ecaps as .elbissop ehT sreniatnoc shall eb hcus and eht seluR and snoitalugeR edam Act, 1986 as ot edulcerp noitanimatnoc fo eht stnetnoc htiw .rcdnucreht ehT sliated fo snoitidnoc rednu hcihw slatem ro rehto .seitirupmi eht ecnecil rof eht esu fo dradnatS Mark yam eb detnarg ot srerutcafunam ro srecudorp yam eb 7.2 Marking deniatbo morf eht uaeruB fo naidnI Standards. hcaE reniatnoc shall eb ylbigel and ylbiledni 8 GNILPMAS dekram htiw eht gniwollof :noitamrofni 8.1 selpmasevitatneserpcR rof stset shall eb drawn a> emaN and epyt fo eht ;lairetam gnidrocca ot eht dohtem debircserp ni 4 fo SI 1699 : b) ecruoS fo ;erutcafunam 1995. C> muminiM ten tnetnoc ni g ro ;gk 9 YTILAUQ FO STNEGAER d) hctaB ro edoc ;rebmun e> etaD fo ;erutcafunam Unless deificeps ,esiwrehto erup slacimehc and dis- 0 ruoloC ytisnetni ;)egnar( and dellit retaw ees( SI 1070 : )2991 shall eb deyolpme 8) ynA rehto stnemeriuqer rednu eht -dnnlS ni .stset a& of Weights and Mensures (Packaged NOTE - eruP‘ ’slacimehc llahs naem slacimehc taht od ton Commodities) Rules, 1977/Prevention of niatnoc seitirupmi hcihw tceffa eht tset dohtem stluser fo .sisvlana , Food Adullerntion Rules, 1955. 3 SI 4467 : 1996 ANNEX A ])i( [Table 1, Item NOITANIMRETED FO DILOS TNETNOC erehT era owt sdohtem rof gninimreted eht dilos ksalf ni tnatsnoc erutarepmet bath at 20°C rof 30 .tnetnoc dohteM I desab no cificeps ytivarg .nim etuliD ot emulov at that erutarepmet htiw noitanimreted nac eb desu as a enituor .dohtem .retaw evomeR eht ksalf morf eht bath, epiw ti yrd dohteM II shall eb eht eerefer .dohtem and .hgiew morF this tcuded eht thgiew fo elpmas and etaluclac cificeps .ytivarg Obtain eht -roc DODTEM I - CIFICEPS YTIVARG DOIITBM gnidnopser tnecrep sdilos and eerged emuaB morf Pycnometer - A elbatius yticapac ylbareferp a eht elbaT 3. detarbilac 100 lm cirtemulov ksalf htiw kcen fo Calculation: 8 mm lanretni dia. thgieW fo retaw tnetnoc fo ksalf = x erudecorP - ylluferaC naelc retemoncyp yb gnillif at 20°C htiw cimorhc dica gninaelc noitulos and gnittel thgieW fo elpmas at 20°C = y stand rof a wef .sruoh ytpmE retemoncyp and esnir thgieW fo elpmas plus retaw at = z ylhguoroht htiw .retaw lliF htiw ylhserf deliob 20°C retaw ylsuoiverp delooc ot tuoba 15°C and ecalp ni a tnatsnoc erutarepmet bath at 20°C. retfA 30 ,nim thgieW fo retaw gniypucco ecaps = x - )y-z( adjust retaw level ot detaudarg emulov no -cyp fo elpmas retemon and ;reppots evomer morf bath, epiw yrd cificepS ytivarg 02/02 fo elpmas :z y htiw naelc htolc and .hgiew ytpmE ,retemoncyp x - )Y-Z( esnir lareves semit htiw lohocla and neht ,rehte tel yrd ,yletelpmoc evomer rehte ruopav and .hgiew DOHTEM II enimreteD eht thgiew fo retaw at 20°C yb -tcartbus gni thgiew fo retemoncyp morf its thgiew nehw ehT dilos tnetnoc fo lemarac ruoloc is denimreted dellif htiw .02H yb gniyrd a elpmas nopu a reirrac desopmoc fo erup ztrauq sand that passes a .oN 40 tub ton a .oN 60 lliF eht deird retemoncyp htiw ,elpmas ylsuoiverp eveis and has neeb deraperp yb noitsegid htiw delooc ot 15°C using a mets-gnol lennuf gnihcaer cirolhcordyh ,dica washed ,eerf-dica deird and woleb noitaudarg ,kram litnu level fo eht elpmas is .detingi xiM 30.0 g fo deraperp sand yletarucca otpu rewol dne fo kcen fo eht .ksalf wolF( yam eb dehgiew htiw 0.2-5.1 g lemarac ruoloc yletarucca deppots yb gnitresni glass dor fo elbatius ezis otni dehgiew and yrd ot tnatsnoc thgiew at 60°C rednu lennuf os as ot esolc mets ).gninepo decuder erusserp 50 gH/mm 7.6( .)aPk droceR eht ylluferaC evomer lennuf ot tneverp elpmas morf lanif thgiew fo eht sand plus .lemarac etaluclaC eht gnimoc ni tcatnoc htiw .kcen ecalP ti ni tnatsnoc tnecrep sdilos as :swollof erutarepmet bath at 20°C rof 30 ,nim evomer morf eht bath, epiw ti yrd and hgiew ksalf and .elpmas tnecreP sdilos = fW x 100 WC Add retaw ylsuoiverp delooc and deniatniam ot erehw tuoba 15°C tsomla ot noitaudarg ,kram gninnur ti rw = lanif thgiew fo sand plus ,lemarac edis-nwod fo kcen ot tncvcrp gnixim htiw .elpmas thgiew fo sand, and evomeR ria selbbub fi yna yb eltneg tapping. ecalP WS = thgiew fo lemarac yllaitini .dedda WC = 4 IS 4467 : 1996 Table 3 Degrees k-ix, Specific Gravity, and Degrees Baume of Sugar Solutions (Plato Table)’ - - r r- r Specitic Gravity at Specific Gravity at =i “Brix or % -- “Baume “Brix or % “Bnume by Wt of (Modulus by Wt of (Modulus SUCrOSe 20/20” 2014” 145) Sucrose 2Ot20” 2014” 145) 0.0 1.00000 0.998234 00.0 . 11.0 413 2288 .13 .2 078 9010 .ll .2 497 3121 .24 4 155 9786 .22 .4 580 3954 .35 .6 233 1.000563 34 .6 664 4788 .46 .8 311 1342 .45 .8 747 5625 .57 1.0 389 2120 56 12.0 831 6462 .68 .2 467 2897 .67 .2 915 7300 .79 .4 545 367.5 .79 .4 999 8140 .90 .6 623 4453 .90 .6 5084 8980 7.02 .8 701 5234 1.01 .8 168 9822 .13 2.0 779 601.5 .12 13.0 252 50665 .24 .2 858 6796 .23 .2 337 1510 .35 .4 936 7580 .34 .4 422 2356 .46 .6 1015 8363 .46 .6 506 3202 .5J .8 093 9148 .57 .8 591 4050 .68 3.0 172 9934 .68 14.0 677 4900 .79 .2 251 10721 .79 .2 762 5751 .90 .4 330 1510 .90 .4 847 6602 8.01 6 409 2298 2.02 .6 933 7455 .12 .8 488 3089 .13 .8 6018 8310 23 4.0 567 3881 .24 15.0 104 9165 34 .2 647 4673 .3.5 .2 190 60022 .45 .4 726 5467 .46 .4 276 0880 .56 6 806 6261 57 .6 362 1738 .67 .8 886 7058 .68 .8 448 2598 .78 5.0 965 7854 .79 16.0 534 3460 .89 .2 2045 8652 .91 .2 621 4324 9.00 .4 125 9451 3.02 .4 707 5188 .ll .6 206 20251 .13 .6 794 6054 .22 .8 286 1053 .24 .8 881 6921 .33 6.0 366 1855 .35 17.0 968 7789 .45 .2 447 2659 .46 .2 7055 8658 .56 .4 527 3463 $57 .4 142 9529 .67 .6 608 4270 .69 .6 229 70400 .78 .8 689 5077 .80 .8 317 1273 .89 7.0 770 5885 .91 18.0 1.07404 1.072147 10.00 .2 851 6694 4.02 .2 492 3023 .ll .4 932 7504 .13 .4 580 3900 .22 .6 3013 8316 .24 .6 668 4777 .33 .8 095 9128 .35 .8 756 5657 .44 8.0 176 9942 .46 19.0 844 6537 .55 .2 258 30757 .58 .2 932 7419 .66 .4 340 1573 .69 .4 8021 8302 .77 .6 422 2391 .80 .6 110 9187 .88 .8 504 3209 .91 .8 198 80072 .99 9.0 1.03586 1.034029 5.02 20.0 287 0959 11.10 .2 668 4850 .13 .2 376 1848 .21 .4 750 5671 .24 .4 465 2737 .32 .6 833 6794 .35 .6 554 3628 .43 .8 915 7318 .46 .8 644 4520 .54 10.0 998 8143 .57 21.0 733 5414 .65 .2 4081 8970 .68 .2 823 6309 .76 .4 164 9797 .80 .4 913 7205 .87 .6 247 40626 .91 .6 9003 8101 .98 .8 330 1456 6.02 .8 093 9000 12.09 ‘) Nurf Bur. Std Ck. C440, pp. 614, 626 (1942). Based upon figures prepared by Kalserliche Normal-Eichungs-Kommission and accepted by International Commission for Uniform Methods of Sugar Analysis. 5

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