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IS 14742: Textile Auxiliaries - Silicone Emulsion PDF

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इंटरनेट मानक Disclosure to Promote the Right To Information Whereas the Parliament of India has set out to provide a practical regime of right to information for citizens to secure access to information under the control of public authorities, in order to promote transparency and accountability in the working of every public authority, and whereas the attached publication of the Bureau of Indian Standards is of particular interest to the public, particularly disadvantaged communities and those engaged in the pursuit of education and knowledge, the attached public safety standard is made available to promote the timely dissemination of this information in an accurate manner to the public. “जान1 का अ+धकार, जी1 का अ+धकार” “प0रा1 को छोड न’ 5 तरफ” Mazdoor Kisan Shakti Sangathan Jawaharlal Nehru “The Right to Information, The Right to Live” “Step Out From the Old to the New” IS 14742 (1999): Textile Auxiliaries - Silicone Emulsion [TXD 7: Textile Sizing and Finishing Materials] “!ान $ एक न’ भारत का +नम-ण” Satyanarayan Gangaram Pitroda ““IInnvveenntt aa NNeeww IInnddiiaa UUssiinngg KKnnoowwlleeddggee”” “!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता हहहहै””ै” Bhartṛhari—Nītiśatakam “Knowledge is such a treasure which cannot be stolen” IS14742:1999 vR?#vmF Twfemm-m~-m Indian Standard ELITXET SEIRAILIXUA - ENOCILIS NOISLUME - NOITACIFICEPS ICS 59.080.01; 71.100.40 0 BIS 1999 BUREAU OF INDIAN STANDARDS MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG NEW DELHI 110002 Price Group 2 elitxeT gniziS dna gnihsiniF slairetaM lanoitceS ,eettimmoC XT 07 DROWEROF sihT naidnI dradnatS was adopted yb the uaeruB of naidnI ,sdradnatS after the draft dezilanif yb the elitxeT gniziS dna gnihsiniF slairetaM lanoitceS eettimmoC had neeb devorppa yb the elitxeT noisiviD .licnuoC enociliS snoislume are ylevisnetxe desu ni the elitxet yrtsudni for elitxet gnihsinif as ,srenetfos water tnellelper dna water ,gnifoorp pilsitna gnitaoc dna enif gnitaoc of .selitxet ehT esu of enocilis noislume spleh elbaredisnoc gnivas ni gnissecorp cost dna sevig the lanif tcudorp na tnellecxe .hsinif roF elitxet gnihsinif two tnereffid sepyt of enocilis snoislume are .desu esehT :era )i A evitcaer lyhtemylop negordyh ,enaxolis dna )ii A evitcaer-non lyhtemidylop .enaxolis ehT evitcaer lyhtemylop negordyh snoislume are desu gnola htiw the renetfos or .rezicitsalp ehT evitcaer-non lyhtemidylop snoislume are desu ni noitcnujnoc htiw muinatit or muinocriz dnuopmoc for water .ycnelleper roF the esoprup of gnidiced whether a ralucitrap tnemeriuqer of siht dradnats si deilpmoc ,htiw the lanif ,eulav devresbo or ,detaluclac gnisserpxe the tluser of a test or ,sisylana llahs eb dednuor off ni ecnadrocca htiw SI 2 : 1960 seluR‘ for gnidnuor off laciremun seulav .‘)desiver( ehT rebmun of tnacifingis secalp deniater ni the dednuor off eulav dluohs eb emas as that of the deificeps eulav ni siht .dradnats SI 14742 : 1999 Indian Standard ELITXET SEIRAILIXUA - ENOCILIS NOISLUME - NOITACIFICEPS 1 SCOPE 4.1.3 ritS the stnetnoc of each ,reniatnoc as detceles ni 4.1.2, ylhguoroht for ton ssel naht 5 setunim htiw sihT dradnats sebircserp the stnemeriuqer for a naelc kcits erofeb .gnilpmas ehT gnirrits yam eb enocilis snoislume of lyhtemidylop enaxolis dna degnolorp ylralucitrap fi noislume si ton lyhtcmylop negordyh enaxolis desu ni elitxet .suonegomoh retfA gnirusne that the stnetnoc ni the yrtsudni as gnihsinif .stnega reniatnoc are yletelpmoc ,dezinegomoh- draw a 2 SECNEREFER elpmas of tuoba 100 g ni a naelc elttob hcihw dluohs eb stoppered yletaidemmi after .gnillif sihT ehT gniwollof sdradnats niatnoc snoisivorp hcihw llahs etutitsnoc the test .elpmas ehT test elpmas hguorht ecnerefer ni siht text, etutitsno-c noisivorp dluohs eb derrits niaga htiw a naelc ssalg rod tsuj of siht .dradnats tA the emit of ,noitacilbup the erofeb gnihgiew ni suoirav test sdohtem nevig ni snoitide detacidni were .dilav llA sdradnats are siht .dradnats tccjhus ot ,noisiver dna seitrap ot stnemeerga desab no siht dradnats are degaruocne ot etagitsevni the 4.2 Criteria for Conformity ytilibissop of gniylppa the tsom tnecer snoitide of 4.2.1 ehT tol llahs eb deredisnoc gnimrofnoc ot the the sdradnats detacidni :woleb stnemeriuqer of siht dradnats fi the etisopmoc SI No. Title elpmas steem the suoirav stnemeriuqer deificeps rednu 3. 1070: 1992 retaW for lareneg yrotarobal esu (third revision) 5 GNIKRAM 093I : 1983 Methods for noitanimreted of pH 5.1 Each package llahs eb dekram htiw the eulav of suoeuqa extracts of elitxet gniwollof :noitamrofni slairetam tsrif( revision) a) Net ssam of the ;noislume 3 STNEMERIUQER )b emaN of the ,lairetam ,yleman enocilis enociliS noislume llahs teem the stnemeriuqer as ;noislume nevig ni elbaT 1. c) diloS tnetnoc of the ;lairetam 4 GNILPMAS DNA AIRETIRC ROF YTIMROFNOC d) noitacidnI of the ecruos of ;erutcafunam dna 4.1 gnilpmaS e) htnoM dna raey of .erutcafunam 4.1.1 Lot 5.2 SIB noitacifitreC gnikraM llA the sreniatnoc of eno etinifed epyt dna ytilauq of enocilis noislume dna of the emas noitisopmoc Each package yam osla eb dekram htiw the dradnatS dereviled ot a reyub tsniaga eno despatch eton llahs Mark. etutitsnoc a .tol 5.2.1 ehT esu of the dradnatS Mark si denrevog yb 4.1.2 sselnU esiwrehto agreed ot neewteb the reyub the snoisivorp of Bureau of Indian Standards Act, dna the ,relles the rebmun of sreniatnoc ot ,eb 1986 dna the seluR dna snoitalugeR edam detceles morf each tol at modnar llahs eb as nevig .rednuereht ehT sliated of snoitidnoc rednu hcihw :woleb the ecnecil for esu of dradnatS Mark yam eb detnarg ot srerutcafunam or srecudorp yam eb deniatbo morf Lot Size Sample Size 2 ot 5I 2 uaeruB of naidnI .sdradnatS 16 ,, 25 3 6 GNIKCAP 26 ,, 50 4 51 ,, 100 5 ehT lairetam llahs eb packed ni yletauqeda 1OI )) 150 6 waterproof packages gnidivorp latot noitcetorp morf 1SI ,,300 7 ,erutsiom ,trid ,tsud etc, as deliated ni the tcartnoc 30 I dna evoba 8 or order. 1 ^___ _.. SI 14742 : 1999 Table 1 Requirements of Silicone Emulsion (Clause 3) 1S No. citsiretcarahC tnemeriuqeR rof dohteM fo Test r -1 lyhtemidyloP enaxoliS lyhtemyloP negordyH senaxoliS )1( )2( 3( (4) 3( )1 etihW noislume etihW noislume lausiV noitanimaxe Ii) 6-5 6-S Hp retem iii) elltalov-1IoN ,rettam tnecrep 2+03 2+03 xennA A IV) liO ,tnetnoc tnecrep 2&52 2+52 xennA B 01 aciliS ,tnetnoc sa ,zOiS tnecrep *02 I *52 1 xennA C )I‘\ evitcA ,rettam tnecrep desab( no ,)acilis tnecrep 2+52 2+52 xennA D ANNEX A [Table 1, SZ No. (iii)] ESTIMATION OF NON-VOLATILE MATTER A-l PRINCIPLE A-3 OVEN DRYING METHOD The noislume si deird ni na nevo ot a tnatsnoc ssam hgieW 2 ot 3 g of enocilis noislume ni a yrd,naelc dna selitalov-non dilos( )tnetnoc si detaluclac yb dna deral irtep hsid dna yrd ni na ria nevo at a gnisserpxe deird eudiser )sdilos( as egatnecrep of erutarepmet of 105 + 3’C for a muminim doirep of the lanigiro ssam of the elpmas rednu test. 4 ,sruoh tub ylbareferp ot tnatsnoc ssam (see Note). etaluclaC the elitalov-non rettam as :swollof A-2 APPARATUS 21) irteP ,hsid latoT elitalov-non riA gniyrd nevo elbapac of gnitarepo at 105 + b) Mass ni g of deird eudiser x 1oo YC, Matter, tnecrep = Mass ni g of elpmas nekat c) rotacciseD (20 mc )aid htiw muiclac edirolhc hgieW-ETON eht reniatnoc gnola htiw deird eudiser retfa 4 as ,tnaccised dna sruoh dna neht ta na lavretni fo 1 .ruoh fI eht ecnereffid ni si ssel naht 02.0 ,tnecrep neht eht emas dluohs eb nekat mass d) A gnihgiew ecnalab htiw ycarucca pu ot 1 .gm sa tnatsnoc .ssam ANNEX B [Table I, SZN o. (iv)] ESTIMATION OF SILICONE OIL CONTENT B-l PRINCIPLE for ruof .sruoh noislumE lliw kaerb otni three latsyrc raelc sreyal as :swollof ehT cage ekil erutcurts demrof ni the noislume yb 4 Water and 1, 4 dioxane - ,raelc sselruoloc gnigdirb of lio dna water htiw the pleh of diuqil at the mottob of ;rednilyc ,srci‘lislume si nekorb nwod yb ,1 4 enaxoid esuaceb ti has erom ytiniffa htiw water naht enocilis eud ot b) Emulsifiers - a niht reyal neewteb the water dna lio ;reyal dna sti tnevlos ytiralop dna .ytisned c) A latsyrc raelc reyal of lio no top (to eb tested 2-B ERUDECORP yltneuqesbus for .)ytirup Read off the ytitnauq of top reyal dna etaler siht ot oT a derusaem ytitnauq of enocilis ,noislume yas the ytitnauq of enocilis noislume tested. roF 30 ,lm add 30 lm of 1, 4 enaxoid ni ,detaudarg elpmaxe ni a 100 lm ,elpmas a 30 lm top reyal 00I lm .rednilyc Shake llew dna wolla ti ot dnats setacidni a 30 tnecrep lio~enocilis .tnetnoc 2 IS 14742 : 1999 ANNEX C [Table 1, SZ No. (v)]) ESTIMATION OF SILICA CONTENT C-l PRINCIPLE c) ylppA heat yllaudarg no hot etalp ni a emuf draobpuc dna tsegid htiw rehtruf noitidda of A dehgiew ytitnauq of enocilis noislume si decuder cirtin dica (see Note), fi ,yrassecen litnu the ot acilis yb gniyortsed the cinagro rettam wet gnihsa diuqil si .raelc .erudecorp ehT detatipicerp acilis si ,deretlif washed. deird dna ashed dna expressed as tnecrep )d etaropavE nwod 20 ot 25 .lm looC ot moor of the elpmas .nekat ,erutarepmet etulid ylsuoituac htiw @OI 05I lm of dellitsid water dna add 2-1 lm of 2-C APPARATUS cirolhcordyh .dica >e a) lacitylanA ecnalab htiw ycarucca pu ot 1 ,gm lioB the stnetnoc ot evomer cirtin .dica )b riA gniyrd no ,nevo elbapac of gnitarepo at f) retliF the noitulos elihw hot no a namtahW 10s * C°3 retlif paper No. 40 or sti .tnelaviuqe Make erus that the eritne etatipicerp si devomer morf the c) IOH ,etalp rekaeb as the acilis si yrev .tnerehda hsaW the d) rotacciseD (20 mc )aid htiw muiclac edirolhc etatipicerp lareves semit htiw hot water litnu as ,tnaccised free morf dica (check the etartlif htiw lyhtem egnaro rotacidni dna there lliw eb on red e) etacilisoroB ssalg ,srekaeb watch ,sessalg ruoloc fi free morf .)dica ,slennuf munitalp or acilis ,selbicurc dna g) yrD the etatipicerp htiw the lennuf ni the nevo 1‘) namtahW retlif paper No. 40 or sti .tnelaviuqe deniatniam at 105 + 3’C for 1 h. refsnarT the retlif 3-C REAGENTS paper htiw the etatipicerp ot a dehgiew munitalp or acilis .elbicurc nruB off the retlif paper no a ehT sdica desu for wet gnihsa dluohs eb of RA wols emalf dna refsnart the elbicurc ot a elffum grade of tsehgih ,ytirup ,yleman ciruhplus ,dica ecanruf dna ash at C°008 for 30 .setunim cirtin ,dica cirolhcrep dica dna cirolhcordyh .dica )h looC the elbicurc htiw the ash ni a rotaccised 4-C ERUDECORP ot moor erutarepmet dna .hgiew a ) hgieW yletarucca tuoba 0.5 ot 1 g of the aciliS tnetnoc as elpmas dna refsnart ti ot naelc yrd 500 lm ssalg thgieW of the ash x 1 .o 2OiS tnecrep = rekaeb derevoc htiw a watch .ssalg thgieW of elpmas )h ddA 30 lm of ciruhplus ,dica dewollof yb ETON - looC eht rekaeb dna sti stnetnoc ot a etaredom erutarepmet erofeb gnidda cirtin sdica ta raluger .slavretni laudarg noitidda of cirtin dica siht( emulov nac gniddA cirtin dica ot toh stnetnoc ni eht rekaeb lliw esuac yrav dna yam eb as hcum as 30 .)lm .gnitrups ANNEX D [Tube2 1, SZ No. (vi)] ESTIMATION OF ACTIVE MATTER, PERCENT D-l ehT evitca rettam yam eb detaluclac morf acilis 2) aciliS ,tnetnoc tnecrep = aciliS as 2OiS tnetnoc deniatho evoba as :swollof lyhtemylop( negordyh tnecrep X 1.006 1) ,tnetnoc~enociliS tnecrep = aciliS as zOiS enaxolis )epyt lyhtemidylop( enaxolis )epyt tnecrep x 1.241 __-__-__-_wp _ ._______ __ ~~ Bureau of Indian Standards SIB si a yrotutats noitutitsni dehsilbatse rednu the Bureau of Indian Standards Act, 1986 ot etomorp suoinomrah tnempoleved of the seitivitca of ,noitazidradnats gnikram dna ytilauq noitacifitrec of goods dna gnidnetta ot detcennoc srettam ni the .yrtnuoc Copyright SIB has the thgirypoc of lla sti .snoitacilbup No part of these snoitacilbup yam eb decudorper ni yna mrof tuohtiw the roirp noissimrep ni gnitirw of .SIB sihT does ton edulcerp the free ,esu ni the esruoc of gnitnemctpmi the ,dradnats of yrassecen ,sliated hcus as slobmys dna ,sezis epyt or grade .snoitangised seiriuqnE gnitaler ot thgirypoc eb addressed ot the rotceriD ,)snoitacilbuP( .SIB Review of India Standards stnemdnemA are deussi ot sdradnats as the deen sesira no the sisab of .stnemmoc sdradnatS are osla deweiver ;yllacidoirep a dradnals gnola htiw stnemdnema si demriffaer nehw hcus weiver setacidni that on segnahc are ;dedeen fi the weiver setacidni that segnahc are ,dedeen ti si nekat pu for .noisiver sresU of naidnI sdradnatS dluohs niatrecsa that yeht are ni noissessop of the tsetal stnemdnema or noitide yb gnirrefer ot the tsetal eussi of SIB‘ ’koobdnaH dna :sdradnatS‘ ylhtnoM .’snoitiddA sihT naidnI dradnatS has neeb depoleved morf Dot : No. XT 07 (0153). Amendments Issued Since Publication dnemA No. Date of eussI txeT detceffA UAERUB FO NAIDNI SDRADNATS sretrauqdaeH : kanaM ,navahB 9 rudahaB Shah rafaZ Marg, New ihleD 110 002 smargeleT : ahtsnaskanaM senohpeleT : 323 01 3 1, 323 33 75, 323 94 02 nommoC( ot lla )seciffo lanoigeR seciffO : enohpeleT lartneC kanaM ,navahB 9 rudahaB Shah rafaZ Marg 323 76 17 WEN IHLED 110 002 323 38 41 nretsaE 4l/l .C .I .T emehcS IIV M, V. .I .P Road, ihcagruknaK 337 84 99,337 85 61 ATTUCLAC 700 0.54 337 86 26,337 91 20 nrehtroN 0CS ,633-533 Sector ,A-43 HRAGIDNAHC 160 022 60 38 43 i 60 20 25 nrehtuoS .C .I .T ,supmaC VI Cross Road, IANNEHC 600 113 235 02 16,235 04 42 i 235 15 19,235 23 15 nretseW ,ayalakanaM E9 ,CDIM ,loraM irehdnA (East) 832 92 95,832 78 58 IABMUM 400 093 i 832 78 91,832 78 92 sehcnarB .DABADAMHA .EROLAGNAB .LAPOHB .RAWHSENABUHB .EROTABMIOC .DABADIRAF .DABAIZAHG .ITAHAWUG .DABAREDYH .RUPIAJ .RUPNAK .WONKCUL .RUPGAN .ANTAP .ENUP .TOKJAR .MARUPAHTNANAVURIHT detnirP at ,hpargotnirp New Delh, Ph.: 5726847

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