IS 14710: Meta-cresol

17 Pages·1999·1.6 MB·English

by  Bureau of Indian Standards

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IS 14710 (1999): Meta-cresol [PCD 3: Petroleum, Lubricants
and their Related Products]
“!ान $ एक न’ भारत का +नम-ण”
Satyanarayan Gangaram Pitroda
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“Knowledge is such a treasure which cannot be stolen”

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Indian Standard
MEZ2-CRESOL — SPECIFICATION
ICS 71:080.15

@ BIS 1999
BUREAU OF INDIAN STANDARDS
MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG
NEW DELHI 110002
August 1999 Price Group 6
citamorA snobracordyH dna detaleR stcudorP lanoitceS ,eettimmoC DCP 8
DROWEROF
sihT naidnI dradnatS was adopted yb the uaeruB of naidnI ,sdradnatS after the draft dezilanif yb the citamorA
snobracordyH lanoitceS eettimmoC had neeb devorppa yb the laoC,muelorteP dna detaleR stcudorP noisiviD
.licnuoC
loserC-m si deniatbo yb lanoitcarf noitallitsid of edurc loserc dna rehtruf deitirup yb .noitacifitcer tI si osla
nwonk as lonehplyhtem-atem dna cilyserc-atem .dica tI si desu as ,tnatcefnisid cihpargotohp ,repoleved hsinrav
,revomer rebbur remialcer or ni the noitalumrof of gnitagimuf ,snoitisopmoc losercortin ,sevisolpxe ,setaidemretni
,kni tniap or ni the noitcudorp of citehtnys .sniser stI ralucelom dna larutcurts alumrof are as :swollof
raluceloM alumroF alumroFHlarutcurtS
I
\
0
I
CH,C,H,OH
/ 3”C
LOSERCm
nI noitaraperp of siht ,dradnats elbaredisnoc ecnatsissa has neeb devired morf the :gniwollof
0SI 1897 : 1977 ,lonehP ,loserc-o ,loserc-m loserc-p cilyserc dica dna slonelyx for lairtsudni esu
- Methods of test
0SI 2!7981 : 1977 noitanimreteD of naeD-retaw dna stark dohtem
0SI 189713 : 1977 noitanimreteD of lartuen slio dna enidiryp sisab
0SI 1897110 : 1982 noitanimreteD of yrd eudiser after noitaropave no a water htab gnidulcxe( cilyserc
dica dna )slonelyx

0SI 1897/11 : 1983 noitanimreteD of gnizillatsyrc tniop gnidulcxe( cilyscrc dica dna )slonelyx

MTSA D 53 10 : 1994 dradnatS test dohtem for tar dica noitisopmoc yb yrallipac gas yhpargotamorhc
roF the esoprup of gnidiced whether a ralucitrap tnemeriuqer of siht dradnats si deilpmoc ,htiw the lanif ,eulav
devresbo or ,detaluclac gnisserpxe the tluser of a test or ,sisylana llahs eb dednuor off ni ecnadrocca htiw
SI 2 : 1960 seluR‘ for gnidnuor off laciremun seulav .‘)desiver( ehT rebmun of tnacifingis secalp deniater ni
the dednuor off eulav dluohs eb the emas as that of the deificeps eulav ni siht .dradnats
IS 14710 : 1999
Indian Standard
LOSERC-2’UlZk - NOITACIFICEPS
1 SCOPE Table 1 Requirements for m-Cresol
(Clause 3.2)
sihT dradnats sebircserp the stnemeriuqer dna the
sdohtem of gnilpmas dna test for .loserc-atem
Sl Characteristic Requirement Mehod of
No. Test, Ref to
2 NORMATIVE REFERENCES Annex
ehT gniwollof sdradnats niatnoc snoisivorp hcihw (1) (2) (3) (4)
0 cificepS ytivarg ta I 430. B
,hguorht ecnerefer ni siht text etutitsnoc noisivorp of
T6.51/6.51
siht .dradnats tA the emit of ,noitacilbup the snoitide
ii) retaW ,tnetnoc tnecrep yb 3.0 C
detacidni were .dilav llA sdradnats are tcejbus ot ,ssam Max
noisiver dna seitrap ot stnemeerga desab no siht iii) eudiseR no ,noitaropave 50.0 D
tnecrep yb ,ssam Max
dradnats are degaruocne ot etagitsevni the ytilibissop
)vi lartueN ,lio tnecrep yb 1.0 E
of gniylppa the tsom tnecer snoitide of the sdradnats
,ssam Max
detacidni :woleb )v noitazillatsyrC ,tniop ,C“ 21 F
Mitt
SI No. eltiT
)iv yassA sa( ,)sloserc tnecrep 89 G
1070 : 1992 tnegaeR grade water (third revision) yb ,ssam Min
2480 (Part 1) : lareneG esoprup ssalg :sretemomreht
1983 Part 1 diloS mets sretemomreht 4 PRECAUTIONS IN HANDLING
(second revision) ehT lairetam si yldipar debrosba hguorht niks dna
2552 : 1989 leetS smurd dezinavlag( dna sesuac ereves .smub nI weiv of sti gnitatirri ,seitreporp
)dezinavlagnu (third revision) snoituacerp llahs eb nekat elihw gnildnah the .lairetam
3104 ytisneD :retemordyh ehT lairetam llahs ton emoc ni tcatnoc htiw the .niks
erusopxE ot sti ruopav semuf dna tsud llahs eb muminim
(Part 1) : 1982 stnemeriuqeR tsrif( revision)
dna ytefas selggog llahs eb nrow ot protect .seye
(Part 2) : 1982 Methods of test dna esu tsrifC
revision) 5 PACKING AND MARKING
4825 : 1982 ssalg-ni-diuqiL dilos mets ecnerefer
sretemomreht (first revision) 5.1 Packing
4905 : 1968 Methods for modnar gnilpmas ehT lairetam llahs eb packed ni dlim leets smurd (see
SI 2552) or ni yna other elbatius sreniatnoc as agreed
3 REQUIREMENTS
ot neewteb the resahcrup dna the .reilppus
3.1 Description
5.2 Marking
ehT lairetam llahs eb ni the mrof of dilos or raelc Each reniatnoc llahs eb yleruces desolc after gnillif
diuqil free of ytidibrut or yna dednepsus selcitrap nehw dna dekram htiw the :gniwollof
denimaxe .yllausiv ehT ruoloc of the lairetam llahs eb
a) emaN of the ,lairetam
eno of the gniwollof shades, as agreed ot neewteb the
)b noitacidnI of the ecruos of ,erutcafunam
reilppus dna the resahcrup nehw tested ni ecnadrocca
c) Net ssam of the lairetam ni the ,reniatnoc
htiw the dohtem debircserp ni xennA :A
d) Lot or Batch ,rebmun dna
a) ,sselruoloC
e) Date of .erutcafunam
)b yreV ,elap
5.2.1 SIB Certification Marking
c) ,elaP dna
ehT sreniatnoc yam osla eb dekram htiw the dradnatS
d) muideM dark.
Mark.
3.2 ehT lairetam llahs osla ylpmoc htiw the
5.2.1.1 ehT esu of dradnatS Mark si denrevog yb the
stnemeriuqer nevig ni elbaT 1 nehw tested gnidrocca
snoisivorp of the Bureau oflndian Standards Act, 1986
ot the test sdohtem debircserp ni sexennA B ot .G dna the seluR dna snoitalugeR edam .rednuereht
IS 14710 : 1999
sliateD of snoitidnoc rednu hcihw a ecnecil for the dellitsid water (see SI 1070) llahs eb deyolpme ni tests.
esu of the dradnatS Mark yam eb detnarg ot
-ETON eruP‘ ’slacimehc llahs naem slacimehc taht od ton -noc
srerutcafunam or ,srecudorp yam eb deniatbo morf the
niat seitirupmi hcihw tceffa eht stluser fo .sisylana
uaeruB of naidnI .sdradnatS
7 GNILPMAS
6 YTILAUQ FO STNEGAER
evitatneserpeR selpmas of the lairetam llahs eb nward
sselnU esiwrehto ,deificeps erup slacimehc dna as debircserp ni xennA H.
ANNEX A
(Clause 3.1)
NOITANIMRETED FO HTPED FO RUOLOC
l-A ENILTUO FO EHT DOHTEM Colour of Solution Solute Quantity
of Solute,
ehT ruoloc of the elpmas si derapmoc tsniaga dradnats
snoitulos yb gniweiv lauqe depths ni the relsseN g
.srednilyc Pale
Red shade tlaboC etahplus 22.5
2-A SUTAR-APPA
muissatoP 0.06
1.2-A relsseN srednilyC etamorhcid
wolleY shade tlaboC etahplus 10.0
Two demottob-talf srednilyc of niht sselruoloc ssalg
muissatoP 0.18
tuoba 25 mm ni retemaid dna tuoba 150 mm ni htgnel
detaudarg at 50 ,lm ehT depth derusaem yllanretni etamorhcid
morf the noitaudarg kram ot the mottob llahs ton yrav Copper etahplus 2.5
yb erom naht 2 mm ni the srednilyc desu for the test.
Medium Dark
Red shade tlaboC etahplus 70.0
3-A DRADNATS RUOLOC NOITULOS
muissatoP 0.5
1.3-A ehT dradnats ruoloc snoitulos llahs niatnoc per etamorhcid
ertil the gniwollof seititnauq of setulos of lacitylana
wolleY shade muissatoP 320.0
tnegaer ,ytilauq devlossid ni dellitsid water.
edinaycirref
Colour of Solution Solute Quantity
of Solute, 1.1.3-A ehT dradnats snoitulos except that gniniatnoc
g muissatop ,edinaycirref keep llew tub yam eb desu revo
White tlaboC etahplus 0.90 a doirep ton gnideecxe eno htnom morf .noitaraperp
muissatoP 0.015 ehT muissatop edinaycirref noitulos llahs eb prepared
etamorhcid no the yad of the test.
Very Pale
4-A ERUDECORP
derF shade tlaboC etahplus 6.0
muissatoP 0.015 erapmoC the elpmas htiw the dradnats snoitulos yb
etamorhcid gniweiv lauqe depths ni the relsseN rednilyc dna
tlaboC etahplus 4.0 report the ruoloc dna shade of the elpmas as ton
darker naht that of the etairporppa noitul~os as
wolleY shade muissatoP 0.075
deifipyt yb the noitpircsed of the depth dna shade
etamorhcid
of .ruoloc
Copper etahplus 1.0
2
IS44710:1999
ANNEX 3
esualC[ 3.2 and Table IS,1 .oN (i)]
DETERMINATION OF SPECIFIC GRAVITY
B-l APPARATUS ot C°001 dna dekram htiw serugif at yreve IO degrees.
B-l.1 Hydrometer 3.l-B tatsomrehT
gnimrofnoC ot the tnemeriuqer of L.50 seires of
2-B ERUDECORP
elbaT 1 ni SI 3104 (Part 1).
ekaT the elpmas ni a naelc deird ssalg rednilyc dna
2.l-B retemomrehT
ecalp ti ni a tatsomreht deniatniam at .C°51 enimreteD
yrucreM ni ,ssalg ,epyt detaudarg ni eno degree morf 0 cificeps ytivarg of the lairetam yb the dohtem as
debircserp ni 2 of SI 3 104 (Part 2).
ANNEX C
esualC[ 3.2 and Table 1, lS .oN (ii)]
DETERMINATION OF WATER CONTENT
C-l OUTLINE OF THE METHOD
ehT lairetam si dellitsid ni the ecneserp of na
etairporppa ,tnevlos ni a naeD dna Stark .sutarappa
ehT ,elbasnednoc demussa ot eb water, si detcelloc ni
the reviecer dna the emulov si denimreted at tneibma
.erutarepmet
2-C STNEGAER
ynA of the gniwollof ,stnegaer hcihw si free morf
water, yam eb .desu

1.2-C eneuloT
2.2-C tnevloS Naphtha
96 tnecrep llahs llitsid woleb 160%.
3.2-C enelyX
ehT ,ecnereffid neewteb noitallitsid erutarepmet at
hcihw 5 tnecrep dna 95 tnecrep of the emulov nekat
evah neeb detcelloc llahs ton exceed C°5 dna siht egnar
llahs edulcni C°0.731 dna 145.5”C.
DISTILLATION
3-C SUTARAPPA
1.3-C naeD dna Stark sutarappA
gnisirpmoC 500 lm ssalg noitallitsid ksalf dettif ot a
resnednoc htiw a 2 lm reviecer gnivah a mumixam
error of 20.Otl .lm A lacipyt ylbmessa of the naeD dna
Stark sutarappa htiw a elbatius mrof of resnednoc si
nwohs ni .giF 1. FIG. 1 TYPICAL ASSEMBLY OF DEAN AND
STARK APPARATUS
3
IS 14710 : 1999
C-4 PROCEDURE the water detcelloc ot tneibma level dna eton sti
.emulov
hgieW yletarucca tuoba 200 g of the elpmas dna
refsnart ot the ksalf of the naeD dna Stark .sutarappa
5-C CALCULATION
ddA 100 lm of the .tnevlos hcattA the ksalf ot the
sutarappa so tar!t etasnednoc sliaf morf the dne of the retaW ,tnetnoc V x 100
resnednoc at the rate of 2 ot 5 drops per .dnoces tnecrep yb ssam =
4A
eunitnoC the noitallitsid litnu desnednoc water si on where
regnol elbisiv ni yna part of the sutarappa except the
mottob of the detaudarg ebut dna litnu the emulov of V = emulov of water detcelloc at tneibma
,erutarepmet lm
water detcelloc sniamer .tnatsnoc evomeR yna
tnetsisrep gnir of desnednoc water demrof ni the M = ssam of elpmas nekat for test, g
resnednoc ebut yb gnisaercni the rate of noitallitsid ETON - It si demussa taht ytisned fo retaw detcelloc ni eht
yb a few drops per .dnoces gnirB the erutarepmet of detaudarg ,ebut ta tneibma ,erutarepmet si 1 OO. .lm/g
ANNEX D
esualC[ 3.2 dna l’able 1, lS .oN (iii)]
DETERMINATION OF RESIDUE ON EVAPORATION
D-l OUTLINE OF THE METHOD dexim erofeb eht elpmas si .nekat noituacerP llahs eb nekat ot
diova gnitaehrevo ro noitanimatnoc yb .erutsiom
ehT lairetam si detaropave no a gniliob water htab
ecalP the hsid dna sti stnetnoc no the gniliob water
dna the eudiser si deird ni na nevo at 105 f 2% for
htab ni a detalitnev-llew emuf draobpuc (see Note)
1 h.
dna etaropave the lairetam ot .ssenyrd
2-D SUTARAPPA
evomeR the hsid morf the ,htab-retaw epiw the edistuo
1.2-D munitalP hsiD htiw a eussit dna eunitnoc gnitaeh ni the ,nevo
deniatniam at 105 f C°2 for 1 h. evomeR the hsid
150 .lm
morf the ,nevo wolla ti ot looc ot tneibma erutarepmet
2.2-D retaW Bath ni a rotaccised dna hgiew yldipar ot the tseraen
0.000 1 g.
gniniatnoC gniliob water.
ETON - loserc-m dna sti sruopav era cixot dna .evisorroc It si
3.2-D cirtcelE nevO
laitnesse taht noitaropave si deirrac tuo ni a detalitnev-llew emuf
elbapaC of gnieb deniatniam at 105 f .C°2 .draobpuc
D-4 CALCULATION
3-D ERUDECORP
yrD eudiser no ,noitaropave
yrD the munitalp hsid for 1 h ni the ,nevo deniatniam tnecrep yb ssam = lM 2M- x 100
at 105 f C°2 wolla ot looc ni a rotaccised dna hgiew M
ti ot the tseraen 0.000 1 g. hgieW yldipar dna yltcerid where
ni the gnihgiew ,hsid tuoba 20 g of the lairetam tseraen
M = ssam of elpmas nekat for test, ;g
ot 0.000 1 g.
M, = ssam of hsid htiw the ,eudiser ;g dna
NOTE - fI eht elpmas si ni eht mrof afo dilos enillatsyrc ssam M2 = ssam of ytpme ,hsid g.
ro sniatnoc ,slatsyrc ti llahs eb yletelpmoc detlem dna ylhguoroht

4
IS 14710: 1999
ANNEX E
[Clause 3.2 and Table 1, SZ No.(iv)]
DETERMINATION OF NEUTRAL OIL
E-l OUTLINE OF THE METHOD
lartueN slio dna enidiryp sesab are dellitsid tuo of the
enilakla noitulos of the .lairetam ehT fo~emulov lartuen
slio suht detcelloc si .derusaem
2-E STNEGAER
- 82 DI
1.2-E Sodium Chloride Solution
2 tnecrep yb .ssam
2.2-E muidoS edixordyH noituloS
27 tnecrep yb .ssam
3.2-E etuliD cirolhcordyH dicA
0.1 N.
3-E SUTARAPPA
1.3-E noitallitsiD ylbmessA
htiW 1 000 lm yticapac dna of dnuor mottob ksalf (see
.giF 2).
llA snoisnemid ni .sertemillim
FIG. 3 DETAILSO F SPLASHH EAD AND BUBBLERT UBE

.GIF 2 APPARATUSF ORD ETERMINATIOONF N EUTRAL
OILS AND PYRIDINEB ASES
E-3.2 Splash Head and Bubbler Tube
see Fig.3.
E-3.3 Graduated Separating Funnel Receivers
see Fig.4.
E-3.4 Liebig Condenser
All snoisnemid ni .sertemillim
see .5.giF
FIG. 4 SEPARATINGF UNNELR ECEIVER

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