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IS 1353: Methods of test for coal carbonization - caking index, swelling and Grey-King assay (L.T) coke types PDF

24 Pages·1993·2.4 MB·English
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Preview IS 1353: Methods of test for coal carbonization - caking index, swelling and Grey-King assay (L.T) coke types

इंटरनेट मानक Disclosure to Promote the Right To Information Whereas the Parliament of India has set out to provide a practical regime of right to information for citizens to secure access to information under the control of public authorities, in order to promote transparency and accountability in the working of every public authority, and whereas the attached publication of the Bureau of Indian Standards is of particular interest to the public, particularly disadvantaged communities and those engaged in the pursuit of education and knowledge, the attached public safety standard is made available to promote the timely dissemination of this information in an accurate manner to the public. “जान1 का अ+धकार, जी1 का अ+धकार” “प0रा1 को छोड न’ 5 तरफ” Mazdoor Kisan Shakti Sangathan Jawaharlal Nehru “The Right to Information, The Right to Live” “Step Out From the Old to the New” IS 1353 (1993): Methods of test for coal carbonization - caking index, swelling and Grey-King assay (L.T) coke types [PCD 7: Solid Mineral Fuels] “!ान $ एक न’ भारत का +नम-ण” Satyanarayan Gangaram Pitroda ““IInnvveenntt aa NNeeww IInnddiiaa UUssiinngg KKnnoowwlleeddggee”” “!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता हहहहै””ै” Bhartṛhari—Nītiśatakam “Knowledge is such a treasure which cannot be stolen” ( lJw??t=jr ) TgT Indian Standard METHODS OF TEST FOR COAL CARBONIZATION -CAKING INDEX, SWELLING NUMBER AND (LT) GRAY-KING ASSAY ( First Revision J UDC 662’66 : 662’8’057_‘1 Q BIS 1993 BUREAU OF INDIAN STANDARDS MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG NEW DELHI 110002 May 1993 PriceGroap 8 diloS lareniM sleuF lanoitceS ,eettimmoC DCP 7 DROWEROF sihT naidnT dradnatS ( tsriF noisiveR ) was adopted yb the uaeruB of naidnI ,sdradnatS after the draft dezilanif yb the diloS lareniM sleuF lanoitceS eettimmoC had neeb devorppa yb the ,muelorteP laoC dna detaleR stcudorP noisiviD .licnuoC sihT dradnats was tsrif deussi ni the raey 1959 nehw ti was prepared no the sisab of detimil lanoitagitsevni data elbaliava htiw lartneC leuF Research ,etutitsnI lanoigeR laoC yevruS snoitatS dna other sertnec of noitagitsevni dna research ni those .syad ehT eettimmoC at that emit dluoc evired tifeneb of gniyduts suoirav stnemucod detalucric yb lanoitanretnI noitazinagrO for noitazidradnatS ( 0SI ) hcihw were osla ni the evitamrof stages. ehT ,eettimmoC elbisnopser for the noitaraperp of siht dradnats had, therefore, degasivne ot etadpu the emas as dna nehw erom data are edam .elbaliava nI the tneserp noisrev esu of tnerapsnart etacilisorob ssalg retorts ni noitidda ot those of acilis retorts has neeb debircserp no the sisab of lanoitagitsevni work enod dna data edam .elbaliava ,sediseB a deifilpmis tey elbailer dohtem for noitanimreted of klub ytisned of ylenif dehsurc edortcele ekoc/nobrac ezeerb has neeb detaroprocni ni ecalp of the remrof emosrebmuc .dohtem ehT sliated of suoirav test sdohtem evah osla neeb ylbatius .detadpu nI the noitaraperp of siht dradnats elbaredisnoc ecnatsissa has neeb nward morf the gniwollof stnemucod deussi yb the lacinhceT ,eettimmoC ,yleman CT/OSI 27 - diloS lareniM sleuF of -retnI lanoitan noitazinagrO for noitazidradnatS ( 0SI :) )i 0SI 501 : 1981 laoC - noitanimreteD of the elbicurc gnillews ,rebmun dna )ii 0SI 502 : 1982 laoC - noitanimreteD of gnikac reyap gniK-yarG coke test. gniwO ot the gniyrav scitsiretcarahc of ,laoc tests debircserp ni siht dradnats are laciripme dna dilav ylno ”ii the snoitidnoc of test are yldigir .devresbo roF the esoprup of gnidiced whether test stluser ylpmoc htiw the srnemeriuqer of tnereffid sdradnats of ,ytilauq the lanif ,eulav devresbo or ,detaluclac gnisserpxe the tluser of a test, llahs eb dednuor off ni ecnadrocca htiw SI 2 : 1960 seluR‘ for gnidnuor off laciremun seulav ( revised )'. rebmuN of tnacifingis secalp deniater ni the dednuor off eulav dluohs eb the emas as that of the deificeps eulav ni the etairporppa .dradnats IS 1353 : 1993 Indian Standard METHODS OF TEST FOR COAL CARBONIZATION - CAKING INDEX, SWELLING NUMBER AND (LT) GRAY-KING ASSAY (F irst Revision ) 1 SCOPE 4 GNILPMAS - sihT dradnats sebircserp the sdohtem of test for laoc 4.1 Methods of Sampling ,noitazinobrac ,yleman gnitanitulgga or gnikac ,xedni Methods of gnilpmas llahs eb as debircserp ni gnillews rebmun dna wol erutarepmet )TL( -yarG SI 436 (Pa.rt teS/l 1) : 1964. gniK .yassa 5 GNIKAC DNA GNILLEWS SEITREPORP FO LAOC 2 REFERENCES 5.1 ehT gnikac power of laoc si the ytreporp or gniwolloF naidnI sdradnatS are yrassecen stcnujda ytiliba of laoc ot mrof a tnerehoc ssam nehw the ot siht :dradnats ylenif powdered laoc si heated rednu deificeps snoitidnoc ni the .yrotarobal A rebmun of sdohtem IS No. Title evah neeb devlove for the tnemerusaem of siht ,ytreporp tub the noitaulave of the stluser of those 436 (Part 11 Methods of gnilpmas of laoc dna has dereffid esuaceb the ytreporp derusaem had ton Set 1) : 1964 :ekoc Part 1 gnilpmaS of ,laoc syawla neeb yltcaxe the .emas tI si a rettam of noitceS 1 launaM gnilpmas tsri/( ecneirepxe that for yrotarobal ,sesoprup the revision) tnemerusaem of eno or other of these seitreporp sevig 1350 (Part /4 Methods of test for laoc dna a ylriaf elbailer noitacidni of the gnikoc ssalc otni Set 2) : 1975 coke : Part 4 etamitlU ,sisylana hcihw a nevig laoc .sllaf eerhT sdohtem are ni ,esu noitceS 2 noitanimreteD of :yleman negortin tsrif( revision) a) dnaS Method for gninimreted noitanitulggA ,xednI )b elbicurC gnillewS rebmuN ,tseT dna 3 TERMINOLOGY c) gniK-yarG yassA )TL( Coke .epyT roF the esoprup of siht dradnats the gniwollof ehT dnas dohtem for gninimreted ssenikcits or snoitinifed llahs .ylppa gnitanitulgga power has deniag lareneg ecnatpecca ni aidnI tub there are ynam sevitanretla for the 3.1 gnitanitulggA xednI gnikaC( )xednI noitanimreted of gnikac power rehtie ylevitatitnauq mumixaM elohw rebmun oitar of dnas ot laoc ni or .ylevitatilauq a erutxim of dradnats dnas dna laoc ,hcihw after 6 GNITANITULGGA XEDNI OR GNIKAC gnitaeh rednu deificeps ,snoitidnoc sevig a tnerehoc XEDNI ,ssam elbapac of gnitroppus a 500 g ssam dna gnitareneg ssel naht 5 tnecrep of esool powder. tI 6.1 eniltuO of the Method si yrassecen that yllaiceps prepared ralugna dnas of morF a seires of tests, the mumixam oitar of dnas cificeps graded ezis dna ytilauq dluohs eb .desu ot laoc si deniatbo ni a laoc dnas erutxim ,hcihw after noitazinobrac rednu deificeps ,snoitidnoc sevig 3.2 elbicurC gnillewS rebmuN a tnerehoc ssam elbapac of gnitroppus a 500 g ,ssam eziS xedni of the coke nottub decudorp nehw 1 g at the emas emit the noitroporp of esool powder of laoc si heated rednu deificeps ,snoitidnoc as gnieb ssel naht 5 tnecrep of the ssam of dnas dna derapmoc htiw a set of dradnats .seliforp .laoc sihT si the gnitanitulgga xedni or gnikac .xedni tI si dootsrednu that siht dohtem sedivorp ylno na 3.3 Low Temperature (LT) Gray-King Assay etamixorppa erusaem of the ycnednet of a laoc ot etanitulgga or ot ecudorp a pmul morf powder. oT eziS dna erutan of coke eudiser dna osla the sdleiy erusne elbailer ,nosirapmoc ti si yrassecen that of coke dna suoirav stcudorpyb ,yleman tar, ,rouqil evitarapmoc tests neewteb tnereffid operators dluohs ainomma dna gas decudorp yb gnizinobrac 20 g of eb deirrac tuo htiw seilppus morf the emas hctab laoc at C°006 ni a tnerapsnart etacilisorob ssalg or of .dnas nI lla cases the hctab rebmun dluohs eb acilis retort rednu deificeps .snoitidnoc stated. 1 IS 1353 : 1993 6.2 Apparatus 6.3 dnaS )a Weighing bottle - stoppered, ,lacirdnilyc tI si ylemertxe tnatropmi that the dnas desu ni siht yletamixorppa 75 mm ni thgieh dna 2.5 mm test dluohs eb of mrofinu ytilauq htiw regard ot ,ezis ni .retemaid ,ytirup ,ssenprahs etc. ehT dradnats acilis dnas si ton elbulos ni hot etulid cirolhcordyh dica ot a b) Silica crucible - ,tneculsnart htiw ,dil of greater tnetxe naht 0.5 .tnecrep tI stsisnoc ylniam neve taper, the relmi ecafrus gnieb free morf of ralugna selcitrap of erup ,acilis dna si free morf .ssenhguor ehT elbicurc llahs mrofnoc ot the ,seitirupmi hcus as ,yalc ,klahc or nori .etanobrac gniwollof :snoisnemid tI si graded ot pass SI eveiS 30 (296 )snorcim dna lanretnI retemaid at the 38 ? 1 mm ot eb deniater no SI eveiS 20 (211 )snorcim gniniatnoc top of elbicurc ton erom naht 5 tnecrep of ezisrevo dna ton erom naht 10 tnecrep of ,ezisrednu the ezisrevo dna lanretxE retemaid at 26 2 1 mm ezisrednu lairetam gnieb ton ylbaicerppa tnereffid mottob morf the deificeps neercs .sezis ehT dnas llahs ton kaerb nwod no gnitaeh for three sruoh at C°029 ot ssenkcihT of :sllaw hcus na tnetxe that the egatnecrep of ezisrednu tA top of elbicurc 2.25 ? 0.50 mm lairetam si desaercni yb 2.5. dnaS of siht ytilauq tA mottob 1.25 ot 1.5 si elbaniatbo morf the lartneC leuF Research etutitsnI 111111 ,.I.R.F ,rahiB .aidnI thgieH of elbicurc 42 t 0.75 mm suidaR of ,erutavruc 3.5 mm 6.4 erudecorP dednuor edge of elbicurc 4 yrd-riA the laoc dna dnirg ti so that the mottob lairetam tsuj passes hguorht SI eveiS 20 (211 muminiM htdiw of dil 46 mm .)norcim nI gniraperp the laoc ot siht ,ezis ti si laitnesse that yrev enif gnidnirg dluohs mumixaM ,htdiw -dulcni 60 ot 62.5 mm eb dediova ecnis the stluser deniatbo are ot gni noisnetxe ot etatilicaf emos tnetxe tnedneped nopu the tnuoma of gnildnah yrev enif lairetam ni the .elpmas ssenkcihT of dil tuobA 1.5 mm b) hgieW otni the gnihgiew ,elttob the etisiuqer retemaiD of recessed 36 mm stnuoma of the laoc dna the dradnats dnas part of dil ot evig 25 g of the ,erutxim gniniatnoc the two stneidergni ni the derised .snoitroporp Depth of recessed 3 ot 4 mm xiM the dnas dna laoc yb gnitator the ebut part of dil neewteb the regnif dna ,bmuht litnu the lc Spat&z - edam morf sheet latem 0.7 mm erutxim si of mrofinu ecnaraeppa ot the .eye ruoP the erutxim otni the acilis ,elbicurc the (or 22 )GWS renni ecafrus of hcihw gnivah neeb derevoc 4 Silica triangle support - of hcus snoisnemid htiw a reyal of citihparg nobrac inorf a that the elbicurc [see 6.2 ])b( si dleh thgirpu suoiverp test. htiw the esab 10 mm evoba the level of the lC sA emos noitagerges of the stneidergni yam .hcneb rucco gnirud the refsnart ot the elbicurc )e Glazed paper etelpmoc the gnixim yb gnitator the ,elbicurc gnitser no sti ,esab htiw the tfel dnah ni a )f MuJfle furnace - gas or yllacirtcele heated, esiwkcolc-retnuoc .noitcerid tA the emas ,emit elbapac of gniniatniam a ydaets erutarepmet dloh the alutaps htiw the reworran dne ni of 900 + 15OC, dedivorp htiw a ylesolc gnittif the thgir dnah ylthgils denilcni ot the lacitrev door. ehT heat evreser of siht ecanruf dluohs yawa morf the operator htiw the edalb of eb hcus that the erutarepmet si deniager the alutaps gnicaf the noitcerid of noitator erofeb the dne of the neves setunim gnitaeh of the ,elbicurc dna htiw sti redaorb dne doirep of the test. ehT erutarepmet dluohs desremmi ni the .erutxim yldetaepeR esiar eb denimreted yb snaem of a elbatius detalusni dna rewol the alutaps elihw the elbicurc si elpuocomreht dna ,retemtlovillim the hot rotated, eunitnoc the gnixim for two ,setunim noitcnuj of the remrof gnieb decalp yawa dna wardhtiw the .alutaps leveL the ecafrus morf the roolf or sedis of the ecanruf tub of the erutxim yb gnisserp yltneg htiw the ni the noitisop ot eb deipucco yltneuqesbus reworran dne of the rebbur ,gnub care gnieb yb the .elbicurc nekat gnirud siht noitarepo that the elbicurc f4 Rubber bung - ,dilos gnimrofnoc ot the si ton derraj or the stnetnoc .depmat gniwollof :snoisnemid 4 revoC the elbicurc htiw sti dil dna refsnart :retemaiD ot the acilis elgnairt .troppus ecalP the elbicurc Narrow dne 35 mm dna the ,troppus ni na cirtcele or derif-sag ediW dne 41 mm ,elffum ylsuoiverp desiar ot a ydaets thgieH 32 mm erutarepmet of C°009 r? 15OC dna dedivorp 2 IS 1353 : 1993 htiw a ylesolc gnittif door. ecalpeR the 7.2 Gas Heating Method elffum door. tA the dne of neves setunim wardhtiw the elbicurc dna the troppus 7.2.1 Apparatus morf the ecanruf dna wolla ot looc ylwols ehT ylbmessa of the sutarappa si nwohs ni .giF 1. ot moor erutarepmet elihw gnidnats no tI stsisnoc of the gniwollof .stnenopmoc na sotsebsa .draob tA the dne of 30 ot 40 setunim evomer the elbicurc ,dil -htiw draw the elbicurc morf the troppus dna ecalp ti no sti esab no a sheet of dezalg paper. d ecalP the rebbur gnub htiw the reworran dne gnitser no the ecafrus of the stnetnoc of the .elbicurc trevnI the elbicurc dna rebbur gnub yb gnidloh the mir of the elbicurc dna the rebbur ,gnub no etisoppo ,sedis neewteb the bmuht dna dnoces regnif of eno .dnah yrraC tuo siht noitarepo revo the sheet of dezalg paper so that yna selcitrap gnillaf morf the elbicurc dna gnirehda ot the regnif dna bmuht yam eb .detcelloc esiaR the elbicurc yllacitrev yawa morf the dezinobrac eudiser of dnas dna .laoc tfiL the laudiser cake morf the ,gnub gnidloh ti yltneg neewteb the regnif dna bmuht (care gnieb nekat ot tcudorp on powder) dna ecalp ti htiw sti daorb dne no a nialecrop .elit yltneG rewol a 500 g ssam 0 litnu sti esab rests nopu the dezinobrac eudiser dna ton whether the ssam si detroppus SOTSEBf* TNfM?,C tuohtiw .gnilbmurc hgieW the esool powder t CIEL.UTn mB)U RNER (WALL SSENKKYT PIPING ),mnS no the dezalg paper, together htiw that morf the top of the .gnub )f retfA the test, the relmi edis of the elbicurc lliw eb dnuof ot eb derevoc htiw a thgirb reyal of .nobrac sihT dluohs eb deniater morf test ot test dna dluohs ton eb tnrub off. g) Repeat the test htiw gnisaercni soitar of dnas ot ,laoc the ssam of the latot erutxim syawla being 25 g and repor t as agglutinating All dimensions in millimetres. xedni the mumixam oitar hcihw stroppus a FIG. 1 APPARATUSF ORn o CRWBIE SWELLING ssam of 500 g htiw the noitroporp of esool NUMBERT EST powder gnieb ssel naht 5 tnecrep of the ssam of the .erutxim 7.2.1.1 Silicn ,tneculsnarT tauqs shape, gnivah a acilis dil htiw 7 CRUCIBLE SWELLING NUMBER gnir eldnah gnihgiew ton erom naht 12.75 g or ssel naht 11 g htiw yticapac yletamixorppa 17 lm dna 7.1 General htiw the snoimemid nevig ni .giF 2. ehT gnillews rebmun of ,laoc as denimreted yb the elbicurc gnillews rebmun test, debircsed ,woleb si dednetni ylelos ot evig emos evitarapmoc erusaem of the gnillews seitreporp of .slaoc morF a noitaredisnoc of the egareva error, ti has neeb deniatrecsa that the naem tluser of ruof tests no the emas laoc elpmas si correct ot nihtiw 2 1 tinu ni 99 tuo of 100 cases dna nihtiw C- 0.5 tinu ni SO’ tuo of 100 cases, there si suht emos ecnarussa that tnereffid srotagitsevni nac ylesolc ecudorper stluser no the emas .laoc ehT ecruos of heat desu ni the test si a gas renrub or yllacirtcele heated .ecanruf ehT lanoitanretnI noitazinagrO for All dimensions in millimelres. noitazidradnatS )OSI( has dednemmocer htob the FIG. 2 CRVJBLE AND LID FORC RUCIBLES WELLING gnitaeh .sdohtem NUMBER 3 IS 1353 : 1993 nI case where the rewol ecafrus of the elbicurc dil 7.2.3 Grinding the Coal si ton ,talf ytluciffid yam eb decneirepxe ni gnissessa yrd-riA the laoc ot eb tested dna dnirg ti so that the gnillews fo~rebmun the .laoc oT emocrevo ,siht ti passes SI eveiS 20 (211 )snorcim [see 6.4 (a)]. ti si detseggus that a llams acim etalp dluohs eb ehT gnidnirg dluohs eb enod ton erom naht two sruoh detresni neewteb the dil dua the elbicurc erofeb erofeb gnitset laoc of weak gnillews scitsiretcarahc gnitaeh the .laoc ot tneverp error eud ot .noitadixo 7.2.1.2 Silica triangle 7.2.4 Procedure gnitsisnoC of tneculsnart acilis ,gnibut 6 ot 6.5 mm hgieW 1.00 ot 1.01 g of the ylhserf dnuorg laoc lanretxe ,retemaid detnuom no lekcin-emorhc eriw otni a elbicurc dna ylthgil tap the elbicurc 12 semit the htgnel of the edis gnieb 63 ot 64 ,mm the retemaid no the hcneb ot level the ecafrus of the .laoc revoC of the debircsni elcric gnieb yletamixorppa 32 .mm the elbicurc htiw the dil dna ecalp ti thgirpu ni the acilis elgnairt detroppus ni the thguard .dleihs thgiL 7.2.1.3 Teclu burner the gas dna heat for hcus emit as si deriuqer for 12.7 mm .erob ynA other elbatius epyt of renrub the emalf of the gninrub elitalov rettam ot eid ,tuo yam osla eb used. dna ni yna case for ton ssel naht 2.5 .setunim wollA the elbicurc ot looc dna ylluferac evomer the coke 7.2.1.4 Draught shield .nottub Repeat the test litnu ruof snottub evah neeb .deniatbo nI emos cases ti yam eb yrassecen ot Made morf sotsebsa tnemec ,gnipip yletamixorppa prepare 5 .snottub retfA each test evomer the nobrac 150 mm gnol htiw 100 mm lanretni dna 110 mm eudiser ni the elbicurc dna epiw the roiretni of the lanretxe .sretemaid ehT gnipip has three stols at eno elbicurc .naelc ,dne 25 mm deep, ni hcihw the eriw snoitrop of the acilis elgnairt rest (see .giF 1). 7.2.5 Examination 7.2.2 Conditions of Heating erapmoC the coke nottub htiw the dradnats derebmun seniltuo ni .giF 3. roF the ,nosirapmoc rotate the The gas erusserp dna the gas dna ria seilppus for nottub tuoba sti sixa so that the tsegral eliforp si the renrub llahs eb detsujda yb gnigralne the ezis detneserp ot .weiv A dohtem of gniweiv hcihw of the gas tej so that the emalf si yletamixorppa sedulcxe the effect of xallarap si nwohs ni .giF 4. 300 mm .gnol htiW the renrub so ,detsujda the noitisop eht-ecalP gniward htiw hcihw the nottub si ot eb of the ,elbicurc gnitser ni the acilis elgnairt dna derapmoc yltcaxe ni the ertnec of the dleif of noisiv detroppus ni the thguard ,dleihs llahs eb so degnarra morf the top of the .ebut egnarrA the nottub so that that the emalf spolevne the elbicurc dna the the mumixam cross noitces si ni enil htiw the gniward erutarepmet of the renni ecafrus of the mottob of nehw deweiv htiw eno eye decalp yletaidemmi revo the elbicurc reaches C°008 2 C°01 ni 1.5 setunim the top of the .ebut dna 82OOC + 5OC ni 2.5 setunim morf the emit the gas si detingi .tsrif htiW these ,snoitidnoc ti lliw 7.2.6 Report yllareneg eb dnuof that the esab of the elbicurc si tsuj evoba the pit of the eulb .enoc esehT snoitidnoc The gnillews xedni of a nottub si the rebmun debircsni ylppa ylralucitrap ot laoc gas of tuoba 4 500 -K ni the eniltuo that sti tsegral eliforp tsom ylraen .3mn/laC roF gas of hcum rehgih or hcum rewol .sehctam Report the naem gnillews rebmun of the cifirolac eulav a tnereffid htgnel of emalf yam eb ,seires expressed ot the tseraen flah .rebmun .deriuqer ehT esu of ruof selbicurc so that the test nac eb deirrac tuo ni dipar ,ecneuqes gniwollof a 7.2.7 roF nellows-non ,nottub the rebmun ‘0’ si desu knalb test ot mraw the thguard ,dleihs si lufpleh nehw ot ebircsed slaoc hcihw evig a powder .eudiser ehT ytluciffid si dnuof ni gniniatta the dradnats rate of rebmun ’%l‘ sebircsed slaoc hcihw evig a tnerehoc .gnitaeh esehT snoitidnoc of gnitaeh llahs eb eudiser that lliw ton raeb a 500 g .ssam ehT rebmun checked at tneuqerf slavretni yb snaem of a enif ‘1’ sebircsed slaoc hcihw evig a tnerehoc eudiser eriw elpuocomreht detresni hguorht a decreip ,dil that cracks otni two or three hard eceip nehw the dna gnivah sti detcetorpnu noitcnuj ni tcatnoc htiw 500 g ssam si .deilppa the ertnec of the esab of the ytpme .elbicurc sihT elpuoc dluohs eb edam of seriw ton reivaeh naht 7.3 Electrical Heating Method 0.22 mm munitalp or 0.45 mm esab ,latem dna the dne of the elpuoc dluohs eb ni the mrof of denettalf 7.3.1 Apparatus pool so that the noitcnuj dna a noitrop of each eriw rest no the mottob of the elbicurc gnirud a 7.3.1.1 Furnace erutarepmet .tnemerusaem ehT snoitidnoc for gniniatta A elbatius epyt of yllacirtcele heated ecanruf si the correct gnitaeh gnivah neeb ,deniatrecsa the nwohs ni .giF 5, hguohtla other sepyt of secanruf sutarappa yam yltneinevnoc niamer yltnenamrep yam osla eb ,desu dedivorp that the stluser deniatbo errected yb gnixif the thguard dleihs no a elbatius are the emas nihtiw( % )tinu as those deniatbo htiw ,troppus the renrub gniniamer dertnec dna gnieb the gas gnitaeh .dohtem detsujda in situ. 4 .GIF 3 STANDARD PROFILESA ND CORRESPONDINCGR UCIBLES WELLING SREBMUN ehT ecanruf detartsulli stsisnoc of a evoorg yrotcarfer etalp yletamixorppa 100 mm ni retemaid dna 20 mm ,kciht gniyrrac the gnitaeh ,tnemele hcihw nac eb dellarips cillatem .lioc nA detrevni acilis hsid of 1 mm llaw ,ssenkciht 10 nun hgih dna yletamixorppa 85 nun lanretxe ,retemaid si decalp revo the sgnidniw dna acts as a troppus for the .elbicurc ehT setalp are dednuorrus yb a yrotcarfer rednilyc of yletamixorppa 225 mm ,retemaid derob ot a depth of tuoba 50 mm htiw a 100 mm retemaid .eloh ehT rednilyc si dettif htiw a yrotcarfer dil 75 mm ,kciht a eloh 50 mm ni retemaid si derob ni the ertnec of the yrotcarfer dil ot wolla for noitresni of the .elbicurc ehT elohw ecanruf si decalp ni na muinimula or dlim leets case. A eloh derob hguorht the esab of the ecanruf selbane a elpuocomreht ot eb decalp ni tcatnoc htiw the edisrednu of the acilis .hsid ehT ecanruf llahs eb deppiuqe htiw a elbatius -otua remrofsnart retem dna elbatius erutarepmet gnirusaem .ecived 7.3.1.2 Crucible and lid emaS as debircsed rednu 7.2.1.1. 7.3.1.3 Pierced silica lid L BUTTON ralimiS ot that debircsed ni 7.2.1.1 tub htiw a All dimensionsi n millimetres. 6 mm eloh ot etadommocca the elpuocomreht .giF( 6). .GIF 4 APPARATUFSO RV IEWINGT HEB LJITON

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