IS 13097: Fluvalinate, Technical

9 Pages·1991·1.1 MB·English

by  Bureau of Indian Standards

इंटरनेट मानक
Disclosure to Promote the Right To Information
Whereas the Parliament of India has set out to provide a practical regime of right to
information for citizens to secure access to information under the control of public authorities,
in order to promote transparency and accountability in the working of every public authority,
and whereas the attached publication of the Bureau of Indian Standards is of particular interest
to the public, particularly disadvantaged communities and those engaged in the pursuit of
education and knowledge, the attached public safety standard is made available to promote the
timely dissemination of this information in an accurate manner to the public.
“जान1 का अ+धकार, जी1 का अ+धकार” “प0रा1 को छोड न’ 5 तरफ”
Mazdoor Kisan Shakti Sangathan Jawaharlal Nehru
“The Right to Information, The Right to Live” “Step Out From the Old to the New”
IS 13097 (1991): Fluvalinate, Technical [FAD 1: Pesticides
and Pesticides Residue Analysis]
“!ान $ एक न’ भारत का +नम-ण”
Satyanarayan Gangaram Pitroda
““IInnvveenntt aa NNeeww IInnddiiaa UUssiinngg KKnnoowwlleeddggee””
“!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता हहहहै””ै”
Bhartṛhari—Nītiśatakam
“Knowledge is such a treasure which cannot be stolen”

SI 13087 : lam

Indian Standard
FLUVALINATE,TECHNICAL
UDC 632’951 FLU 006’354

@ BIS 1991
BUREAU OF INDIAN STANDARDS
MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG
NEW DELHl 110002

July 1991 Price Grq 1
sedicitseP lanoitceS ,eettimmoC FADC 1
FOREWORD
sihT naidrI dradnatS was detpoda yb eht uaeruB fo naidnI Standards, retfa eht tfard dezilanif
sedicitseP lanoitceS eettimmoC had neeb devorppa yb eht dooF and erutlucirgA noisiviD
by the
.licnuoC
,etanilavulE lacinhcet is deyolpme ni eht noitaraperp fo ladicitcesni .snoitalumrof
etan’lavulF is eht nommoc eman rof ( RS lyznebyxonehp-3-onayc-a-) ( R [-2-) -4-orolhc-2
( lyhtemoroulfirt ) lyhtem-3-onilina etaonatub 1. ehT laciripme and larutcurts ealumrof and eht
rslucclom mass fo etanilavulf era nevig :woleb
Empirical Formula Structural Formula Molecular Mass
CzcH&lFsNdh 502'92
nI eht noitaraperp fo this standard eud noitaredisnoc has neeb nevig ot eht snoisivorp fo eht
Insecticides act, 1968 and eht seluR demarf .rednuereht ,revewoH this standard is tcejbus ot eht
snoitcirtser desopmi rednu ,eseht reverehw .elbacilppa
roF eht esoprup fo gnidiced rehtehw a ralucitrap tnemeriuqer fo this standard is deilpmoc .htiw
eht lanif ,eulav devresbo ro ,detaluclac gnisserpxe eht tluser fo a tset ro ,sisylana shall eb dednuor
ffo ni ecnadrocca htiw SI 2 : 1960 seluR‘ rof gnidnuor ffo laciremun seulav ( revised )‘. ehT rebmun
secalp deniater ni eht dednuor ffo eulav dluohs eb eht emas as that fo eht deificeps
of significant
eulav ni this standard.
SI 7903I : 1991
hdiart Standard
FLUVALINATEJECHNICAL
1 EPOCS ehT sreniatnoc shall osla ylpmoc htiw eht
lareneg stnemeriuqer as deificeps ni 2 fo SI 8190
sihT standard sebircserp ehtr stnemeriuqer and ( traP 2 ) : 1988.
sdohtem fo sampling and tset rof ,etanilavulf
.lacinhcet 5 GNIKRAM
2 SECNEREFER P.5 ehT reniatnoc shall raeb ylbigel and ylbiledni
eht gniwollof noitamrofni ni noitidda ot yna
ehT naidnI Standards detsil ni xennA A era rehto noitamrofni as is yrassecen rednu eht
yrassecen stcnujda ot this standard. Insecticides Act, 1968 and eht seluR demarf
:rednuereht
3 STNEMERIUQER
a) emaN fo eht ;lairetam
3.1 noitpircseD b) noitacidnI fo eht ecruos fo -unam
;erutcaf
ehT lairetam shall eb ni eht mrof fo a ,suocsiv
wolley ot nworb ,diuqil eerf morf elbisiv 4 hctaB ;rebmun
suoenartxe seitirupmi ro dedda gniyfidom
.stnega 4 etaD fo ;erutcafunam .
3.2 ehT lairetam shall osla ylpmoc htiw eht 4 etaD fo ;yripxe
stnemeriuqer deificeps ni elbaT 1.
>f etanilavulF ,tnetnoc tnecrep ( m/m ;)
Table 1 Reqniremeotlb for Flavalinate, Technical 9 teN mass fo ;stnetnoc and
( Clauses 3.2 and 7.1 ) h) ehT yranoituac eciton dedrow as ni eht
sedicitcesnI ,tcA 1968 and its .seluR
Chara;~r- Reqoire- Method of Test, Ref to
El. meat r-------~ 5.2 ehT reniatnoc yam osla eb dekram htiw eht
xennA esualC
dradnatS Mark.
fo sihT .oN fo
dradnatS J’;W90 :
6 GNILPMAS
(1) (2) (3) (4) (5)
)i etanilavulF -noc 88.0 B - evitatneserpeR samples fo eht lairetam shall eb
,tnet tnecrep yb drawn as debircserp ni SI 10946 : 1984.
,ssam Min
ii) erutsioM ,tnetnoc W5 - 4 7 STSET
tnecrep yb ,ssam
xaM 7.1 stseT shall eb deirrac yb eht etairporppa
)iii lairetaM elbulosni @5 - 9 sdohtem derrefer ot ni 1oc 4 and 5 fo elbaT 1.
ni ,enoteca tnecrep
yb ,ssam Max
7.2 ytilaoQ fo stnegaeR
iv) ytidicA ( sa ,OS,H .) 0.5 - 11.3.2
tnecrep yb ,ssam Unless deificeps ,esiwrehto erup slacimehc and
Max dellitsid retaw ( ees SI 1070 : 1977 ) shall eb
deyolpme ni .stset
4 PACKING
NOTE - eruP‘ ’slacimehc llahs naem slacimehc
ehT lairetam shall eb dekcap ni dlim leets drums
taht od ton niatnoc seitirupmi hcihw tceffa eht
ylbatius aiid ylreporb dereuqcal morf .edisni StlUser fo .sisylana
ANNEX A
( Clause 2 )
TSIL OF REFERRED INDIAN STANDARDS
SI .oN Title IS No. Title
1070 : 1977 retaW rof lareneg yrotiirobal 8190 tnemeriuqeR rof gnikcap fo
esu ( dnoces revision ) ( traP 2 ) : 1988 sedicitsep : traP 2 diuqiL
sedicitsep (
6940 : 1982 sdohteM fo tset rof sedicitsep second revision )
and rieht snoitalumrof (first 10946 : 1984 sdohteM fo sampling rof
lacinhcet edarg sedicitsep
revision )
1
IS 13097: 1991
ANNEX B
[ Table 1, SZ. NO. )i( ]
DETERMINATION OF FLUVALINATE CONTENT
tnelaviuqe ot 50 gm etanilavulf otni a lm-05
B-l GENERAL
cirtemulov .ksalf .4dd 10 lm lanretni standard
etanilavulF tnetnoc is denimreted using an noitulos and etulid eht kram htiw 3 : 1 ( v/v )
lanretni standard no a gas diuqil -otamorhc eneulot-enaxel .noitulos ekahS ylsuorogiv ot
,hparg deppiuqe htiw a emalf noitazinoi .evlossid
.rotceted
3.4-B noitaraperP fo elpmaS noituloS
2-B SUTARAPPA
hgieW yletarucca a ytitnauq fo elpmas -niatnoc
1.2-B saG diuqiL bpargotamorhC
gni tnelaviuqe ot gm-05 fo etanilavulf otni a
A gas diuqil ,hpargotnmorhc deppiuqe htiw a lm-05 cirtemulov .ksalf Add 10 lm lanretni
emalf noitazinoi rotceted and delpuoc ot a standard and etulid ot eht kram htiw 3 : I ( v/v )
retnirp rettolp muc rotargetni is detarepo rednu eneulot-enaxeh .noitulos ekahS ylsuorogiv ot
eht gniwollof detseggus gnitarepo .sretemarap .evlossid
esehT sretemarap yam eb deirav as rep elbaliava
,seitilicaf dedivorp noitazidradnats is .enod 4.4-B Analysis of the Sample
nmuloC Glass, 5’0 m htgnel and B-4.4.1 tcejnI 2 ~1 fo ecnerefer standard noitulos
2’0 mm ,DI dekcap htiw 3 and fi ,yrassecen adjust eht CLG sretemrarap ot
tnecrep 0 !OI-V brosomorhc evig a etelpmoc noitarapes nihtiw a elbanosaer
001-og )hsem emit and kaep thgieh flah ot htruof-eerht lluf
W-AW-DMCS (
.elacs taepeR eht snoitcejni llit eht esnopser
reirraC gas and ;negortiN 30 nim/lm
rotcaf stabilises nihtiw f I .tnecrep tcejnI
wolf etar
elpmas noitulos and deecorp htiw noitanimreted
erutarepmeT
fo etanilavulf tnetnoc gnirusne that at tsael eno
nmuloC 220°C ecnerefer standard noitcejni is decalp retfa yreve
rotcejnI 240°C htruof fo htfif elpmas ,noitcejni dewolloF yb eno
rotceteD 270°C at eht dne fo eht .nur
2.4.4-B erusaeM eht kaep saera fo etanilavulf
2.2-B Micro-Syringe - 1p-OI .yticapac ecnerefer standard, lanretni standard and
.elpmas enimreteD eht esnopser srotcaf and
3-B STNEGAER
etaluclac eht evitca tneidergni tnetnoc ni eht
.elpmas
1.3-B etaoilhvolF ecnerefeR dradnatS fo
nwonk .ytirup
5-B NOlTALUCLAC

2.3-B lanretnI dradnatS ( enatnocairtod-n ) 99

etanilavulF ,tnetnoc tnecrep yb mass=
tnecrep plus .ytirup
MI .-._ x zR x P
3.3-B Hexaae - lacitylana tnegaer .edarg
2M x lX
4.3-B eneuloT - lacitylana tnegaer .edarg erehw
IIh = mass, ni g, fo etanilavult ecnerefer
4-B PROCEDURE standard;
kaep aera fo elpmas
B-4.1 Preparation of Internal Standard Solution
R2 = kaep aera fo lanretni staudard ’
hgieW yletarucca tuoba 500 gm enatnocairtod-n
otni a lm-001 cirtemulov ,ksalf evlossid ni 3 : 1 P = tnecrep ytirup fo ff etanilavu ecnerefer
( v/v ) eneulot-enaxeh noitulos and ekam up eht standard;
emulov ot eht kram htiw eht emas .noitulos
sihT noitulos lliw niatnoc 5 lm/gm fo lanretni Mz = mass, ni g, fo eht elpmas nekat rof
standard. ;tset and
2.4-B Preparation of Reference Standard kaep aera fo etanilavulf ecnerefer
standard
Solution RI = -____- kaep-- aera fo lanretni standard
hgieW yletarucca a ytitnauq fo ecnerefer standard,
2
Standard Mark

I
ehT esu fo eht dradnatS Mark is denrevog yb eht snoisivorp fo eht Bureau of Indian
Standards Act, 1986 and eht seluR and snoitalugeR edam .rednuereht ehT dradnatS Mark no
stcudorp derevoc yb an naidnI dradnatS syevnoc eht ecnarussa that yeht evah neeb decudorp
ot ylpmoc htiw eht stnemeriuqer fo that standard rednu a llew denifed metsys fo ,noitcepsni
gnitset and ytilauq lortnoc hcihw is desived and desivrepus yb SlB and detarepo yb eht -orp
.recud dradnatS dekram stcudorp era osla ylsuounitnoc dekcehc yb SIB rof ytimrofnoc ot
that standard as a rehtruf .draugefas sliateD fo snoitidnoc rednu hcihw a ecnecil rof eht esu
~ fo eht dradnatS Mark yam be detnarg ot srerutcafunam ro srecudorp yam eb deniatbo morf
, eht uaeruB fo naidnI Standards.
Boreao of Indian Standards
BIS is a yrotutats noitutitsni dehsilbatse rednu eht uaeruB ofhdiun Stundurdr Act, 1986 ot etomorp
suoinomrah tnempoleved fo eht seitivitca fo ,noitazidradnats gnikram and ytilauq noitacifitrec fo
sdoog and gnidnetta ot detcennoc srettam ni eht .yrtnuoc
Copyright
SIB has eht thgirypoc fo all its .snoitacilbup oN trap fo eseht snoitacilbup yam eb decudorper ni
yna mrof tuohtiw eht roirp noissimrep ni gnitirw fo .SIB sihT seod ton edulcerp eht eerf ,esu ni
eht esruoc fo gnitnemelpmi eht standard, fo yrassecen ,sliated hcus as slobmys and ,sezis epyt ro
edarg .snoitangised seiriuqnE gnitaler ot thgirypoc eb desserdda ot eht rotceriD ( noitacilbuP ,) .SIB
Revision of Indian Standards
naidnI Standards era deweiver yllacidoirep and ,desiver nehw yrassecen and ,stnemdnema fi ,yna
era issued morf emit ot .emit sresU fo naidnI Standards dluohs niatrecsa that yeht era ni
noissessop fo eht tsetal stnemdnema ro .noitide stnemmoC no this naidnI dradnatS yam eb tnes
ot SIB gnivig eht gniwollof ecnerefer :
toD : .oN FADC 3814(I )
Amendments Issued Since Publication
dnemA .oN etaD fo eussI txeT Affected
UAERUB FO NAIDNI S
*c .f
c,
sretrauqdaeH : . ‘s
Manak ,navahB 9 rudahaB Shah rafaZ Marg, 2OOOll_ihleD~weN
:senohpeleT 331 01 31, 331 13 75 smargeleT : Manaksanetha
( nommoC ot all sec50 )

lanoigeR seciffO : ” onohpeleT
.
lartneC : Manak ,navahB 9 rudahaB Shah 4 ._ 3tra t 331 01 31
WEN IHLED 110002 .# 331 13 75
nretsaE : 41/l .T.I.C emehcS IIV M, .P.I.V ,daoR alotkinaM
ATTUCLAC 700054 37 86 62
nrehtroN : SC0 ,644-544 rotceS 35-C, HRAGIDNAHC 160036 53 38 43
nrehtuoS : .T.I.C Campus, VI ssorC ,daoR MADRAS 600113 2350216
nretseW : ,ayalakanaM 9E MlDC, ,loraM irehdnA ( East )
-._
YABMOB 400093 6 32 92 95
sehcnarB : .DABADAMHA .EROLAGNAB .LAPOHB .RAWHSENABUHB
.EROTABMIOC .DABADIRAF .DABAIZAHG .ITAHAWUG
.DABAREDYH JAIPUR. .RUPNAK .ANTAP .MARUPAHTNANAVURIHT

Printed at Swatantra Bharat Press, Delhi. lndla
__