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IS 10461-1: Resistance to Inter-Granular Corrosion of Austenitic Stainless Steels - Method for Determination, Part 1: Corrosion Test in Nitric Acid Medium by Measurement of Loss in Mass (Huey Test) PDF

9 Pages·1994·1.2 MB·English
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Preview IS 10461-1: Resistance to Inter-Granular Corrosion of Austenitic Stainless Steels - Method for Determination, Part 1: Corrosion Test in Nitric Acid Medium by Measurement of Loss in Mass (Huey Test)

इंटरनेट मानक Disclosure to Promote the Right To Information Whereas the Parliament of India has set out to provide a practical regime of right to information for citizens to secure access to information under the control of public authorities, in order to promote transparency and accountability in the working of every public authority, and whereas the attached publication of the Bureau of Indian Standards is of particular interest to the public, particularly disadvantaged communities and those engaged in the pursuit of education and knowledge, the attached public safety standard is made available to promote the timely dissemination of this information in an accurate manner to the public. “जान1 का अ+धकार, जी1 का अ+धकार” “प0रा1 को छोड न’ 5 तरफ” Mazdoor Kisan Shakti Sangathan Jawaharlal Nehru “The Right to Information, The Right to Live” “Step Out From the Old to the New” IS 10461-1 (1994): Resistance to Inter-Granular Corrosion of Austenitic Stainless Steels - Method for Determination, Part 1: Corrosion Test in Nitric Acid Medium by Measurement of Loss in Mass (Huey Test) [MTD 24: Corrosion Protection] “!ान $ एक न’ भारत का +नम-ण” Satyanarayan Gangaram Pitroda ““IInnvveenntt aa NNeeww IInnddiiaa UUssiinngg KKnnoowwlleeddggee”” “!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता हहहहै””ै” Bhartṛhari—Nītiśatakam “Knowledge is such a treasure which cannot be stolen” IS10461 (Part1 ):1994 Indian Standard RESISTANCE TO INTER-GRANULAR CORROSION OF AUSTENITIC STAINLESS STEELS - METHOD FOR DETERMINATION PART 1 CORROSlON TEST IN NITRIC ACID MEDIUM BY MEASUREMENT OF LOSS IN MASS (HUEY TEST ) First Revision ) ( UDC 65’491-8’810’41’966 : 391’026 @ SIB 1994 BUREAU OF INDIAN STANDARDS KANAM ,NAVAHB 9 RUDAHAB HAHS RAFAZ MARG WEN IHLED 110002 Muy 1994 Price Group 2 noisorroC noitcetorP lanoitceS ,eettimmoC DTM 24 DROWEKOF sihT naidnI dradnatS ( traP 1 ) ( tsriF noisiveR ) was detpoda yb uaeruB fo naidnI Standards, retfa eht tfard dezilanif yb eht noisorroC noitcetorP lanoitceS eettimmoC had neeb devorppa yb lacigrullateM gnireenignE noisiviD .licnuoC sihT standard was tsrif dehsilbup ni 1983 desab no 0SI 6791-l/1553 )E( citinetsuA sselniatS -sleetS noitanimreteD fo ecnatsiser ot ralunargretni :noisorroc traP 1 noisorroC tset ni cirtin dica muidem yb tnemerusaem fo ssol ni mass ( yeuH tseT ,) issued yb eht lanoitanretnI noitazinagrO rof .noitazidradnatS elihW gniweiver this standard ni eht thgil fo ecneirepxe deniag gnirud eseht ,sraey eht eettimmoc dediced ot esiver this standard gnignirb ti ni enil htiw tneserp secitcarp gnieb dewollof ni eht .yrtnuoc nI this noisiver erugiF rof Apparatus has neeb .dedda ralunargretnI noisorroc setoned noitaroireted fo slatem yb snaem fo laitnereferp gnikcatta fo eht niarg .seirdnuob roF citinetsua stainless ,sleets hcihw yam eb tcejbus ot hcus as kcatta nehw yeht era- tpek at a erutarepmet neewteb tuoba 430 ot 82O”C, ti is detaicossa htiw eht noitatipicerp fo muimorhc hcir sedibrac ro cillaemretni ,sdnuopmoc hcus as sigma esahp at niarg .seirdnuob ehT taeh ,elcyc hcihw yam ekovorp noitazitisnes ot ralunargretni ,noisorroc yam rucco gnirud -toh gnimrof ssecorp ekil gnigrof and ,gnillor as eht tluser fo tcerrocni noitulos tnemtaert ro gnirud a gnidlew .noitarepo sihT standard ( traP 1 ) has neeb deraperp ot edivorp a mrofinu and dezilanoitar dohtem fo gninimreted eht ytilibitpecsus fo citinetsua stainless sleets ot ralunargretni .noisorroc sihT standard is issued ni owt parts, traP 2 fo this standard slaed htiw noisorroc tset ni a ciruhplus reppoc/dica etahplus muidem ni eht ecneserp fo reppoc sgninrut ( ynnepynoM Strauss tseT .) nI gnitroper eht tluser fo a tset edam ni ecnadrocca htiw this standard, fi eht lanif ,eulav devresbo ro ,detaluclac is ot eb dednuor ,ffo ti shall eb enod ni ecnadrocca htiw SI 2 : 1960 seluR‘ rof gnidnuor ffo laciremun seulav ( revised )‘. IS 10461( Part 1 ) : 1994 Indian Standard RESISTANCETO INTER-GRANULAR CORROSIONOFAUSTENITICSTAINLESS STEELS-METHODFORDETERMINATION PART 1 CORROSION TEST IN NITRIC ACID MEDIUM BY MEASUREMENT OF LOSS IN MASS ( HUEY TEST ) ( First Revision ) gnitsiser ralunargretni ,noisorroc ti is yrassecen lr SCOBE ot yrrac tuo a taeh tnemtaert rof .noitazitisnes I.1 sihT standard sebircsed a erudecorp rof sihT tnemtaert is yllausu deniatbo yb -niatniam noitanimreted fo eht ecnatsiser ot ralunargretni gni a tset seceip rof 1 ruoh at a erutarepmet fo noisorroc+ fo citinetsua stainless sleets ni a cirtin 650-675°C dewollof yb dipar gnilooc ot moor dica. muidem yb tnemerusaem fo eht ssol ni mass erutarepmet ni ria ro retaw unless rehto cificeps (, yeuH tseT .) gnitaeh ro gnilooc setar era .detalupits roF wol nobrac yteirav fo stainless ,sleets eht tsom 1.2 sihT dohtem is elbacilppa ot citinetsua ylnommoc desu taeh tnemtaert is gnitaeh at stainless sleets deilppus ni eht mrof fo castings, 675°C rof eno ruoh dewollof yb dipar gnilooc dellor ro degrof stcudorp and sebut gnidulcni ni ria ro .retaw sihT taeh tnemtaert stluser otni dlew slatem and dednetni ot eb desu ni an ylbaicerppa hgih noitatipicerp fo sedibrac and gnisidixo aidem ( rof~ ,elpmaxe ylevitaler -necnoc osla setalumis ot a niatrec tnetxe erutcurtsorcim detart cirtin dica .) hcihw is deniatbo retfa .gnidlew 1.2.1 ehT ecneserp ro ecnesba fo ralunargretni 4 CORROSION TSET noisorroc ni eseht stset is ton ylirassecen a erusaem fo eht ecnamrofrep fo eht lairetam ni 4.1 elpicnirP rehto, evisorroc .aidem ehT stset od ton edivorp a basis rof gnitciderp eht ecnatsiser ot rehto A tset ,eceip deraperp as deificeps ni 4.4.2, is smrof fo noisorroc hcus as lareneg ,noisorroc ;dehgiew neht desremmi ni a gniliob noitulos fo gnittip ro stress noisorroc .gnikcarc cirtin dica rof 5 ,sdoirep hcae fo 48 ruoh using hserf snoitulos rof hcae .doirep ehT noiretirc .2 ESOPRUP FO EHT TSET rof gnitaulave eht tset is ssol ni mass denimreted yb gnihgiew retfa hcae .doirep 2.1 ehT tset setacidni ytilibitpecsus ot -unargretni ral kcatta detaicossa htiw eht noitatipicerp fo 4.2 evisorroC noituloS muimorhc, hcir sedibrac ro cillatemretni sdnuopmoc hcus as sigma esahp at eht niarg ehT evisorroc noitulos is an suoeuqa noitulos fo .yradnuob emoS epyt fo snoisulcni ( evitca 6.5 & 2 tnecrep ( m/m ) tnegaer edarg cirtin dica snoisulcni ) era osla elbitpecsus ot kcatta ni this ( .d.r 1.40 .) .tsetj NOTE - ehT cirtin dica mrofnoc ot eht -acificeps 2.2 sihT tset yam eb desu ot etaulave yna fo eht snoit rof lacitylana tnegaer lacimehc dna llahs evah gniwollof eerht :srotcaf eht gniwollof laudiser :stnetnoc )a eht ssenevitceffe fo eht lanif tnemtaert dexiF eudiser < 50 gk/gm nehw eht lairetam is detset ni eht as bP K- 5 gk/gm dereviled noitidnoc tuohtiw rehtruf tset eF i 2 gk/gm taeh tnemtaert ;noitazitisnes nM evitageN tset sA ( 0.05 gk/gm )b eht ssenevitceffe fo eht dedda gnizilibats -lC < 1 gk/gm ,stnemele- ro wol nobrac tnetnoc nehw eht *-”OS < 10 gk/gm lairetam is detset ni eht noitulos taeh detaert and yltneuqesbus dezitisnes -noc PO’-8 < 2 mg/kg ;noitid and F- < 1 w/kg )c eht ecneulfni fo gnidlew and detaicossa 4.3 Apparatus tsop tsop/noitacirbaf dlew taeh .stnemtaert 4.3.1 Conical ;lask TAEH TNEMTAERT FOR NOITAZITISNES 3 fO yticapac at tsael 1 ,ertil dettif htiw a dloc“ nI redro ot yfirev eht ssenevitceffe fo eht dedda ”regnif noisremmi .resnednoc rehtO sepyt fo gnizilibats stnemele ro wol nobrac tnetnoc ot ,resnednoc hcus as nhillA resnednoc htiw at tsael 1 IS 10461 ( Part 1 ) : 1994 ruof balbs yam eb .desu ehT noisorroc setar redro ot eht ,yrartnoc eht dohtem fo ,noitaraperp sdneped no eht epyt fo resnednoc desu ( ees shall eb tfel ot eht noitercsid fo eht -,-cafunam .giF 1 .) yB snaem fo a repap ,rotacidni ti shall .rerut eb dekcehc that on dica semuf nevig~era ffo gnirud eht .tset roF evitarapmoc ,stnemerusaem 4.4.2.1 Mechanical preparation eht apparatus shall niamer lacitnedi rof all eht .stset ehT tset eceip shall eb delacsed yllacinahcem ’yb gnihsilop no all ,secafrus gnidulcni eht ,segde htiw edarg 120 evisarba repap ro ,htolc 4.4.2.2 Chemical preparation ehT tset eceip shall eb ,delacsed tuohtiw ’yna suoiverp lacinahcem ,tnemtaert ni a .noitulos gnitsisnoc fo 50 semulov fo cirolhcordyh dica -F?- ( d.r ,!91.1 5 semulov fo cirtin dica ( d.r 04.1 ,) and 50 semulov fo retaw at 50 ot 60°C. I 9cm 4.4.2.3 Degreasing ehT tset eceip shall neht eb ,desaerged erofeb gnieb decalp ni eht evisorroc ,noitulos and deird using gnitanirolhcnon stnegaer hcus as paos and c ) .enoteca COLD REGNIF NHILLA NOTE - ehT noitaraperp tnemtaert debircsed ni (WIDEMOUTH6cm) 05/54 JOINT 4.4.2.1, yam eb detnemelppus yb gnisremmi eht nemiceps ni cirtin dica rof elpmaxe 20 tnecrep ONE ERTIL REYEMNELRE SKSALF ( thgiew ) at C°06-05 rof 20 setunim dewollof .yb gnisaerged dna .gniyrd nI esac fo llams retemaid FIG. 1 TYPES OF CDNDENSERS sebut hcihw tonnac eb yltneinevnoc yllacinahcem dehsilop no ,edisni ti si detseggus ot esremmi eht nemicens ni gniliob cirtin dica ( 65 tnecreo ) rof 4.3.2 Support for the Test Piece $4 sruoh gnisu iht emas ’sutaiappa sa iof eht actual .stset sihT tnemtaert sevomer yna ecafrus yllareneG edam fo glass noitanimatnoc taht yam ton eb elbissop yb raluger gninaelc dna dluow esiwrehto tluser ni esaercni ni eht tnerappa thgiew ssol fo eht nemiceps .gnirud 4.3.3 gnitaeH Device ylrae trap fo eht .tset oT peek eht noitulos .gniliob 4.5 Procedure 4.4 Test Piece esJI a emulov fo evisorroc noitulos ( ees 4.2 > fo at tsael 20 lm rep erauqs ertemitnec fo ecafrus 4.4.1 Dimensions aera fo eht tset .eceip nI ,lareneg ylno eno tset eceip shall eb decalp ni hcae lacinoc .ksalf ehT tset eceip nekat morf eht tcudorp shall evah ,revewoH ti is elbissop ot tset lareves tset seceip its tsegral noisnemid detacol ni eht noitcerid fo at eht emas ,emit no noitidnoc that yeht all .gnikrow ehT tset eceip noisnemid shall eb emoc mcrf eht emas edarg fo leets and era denimreted as a noitcnuf fo eht elbaliava detalosi morf eno rehtona at a ecnatsid fo at gnihgiew seitilicaf and eht emulov fo noitulos ot tsael 5 .mm eb .desu ehT tset eceip htgnel shall, ,revewoh eb at tsael lauqe ot eciwt its ,htdiw and eht 4.5.1 enimreteD eht mass fo eht tset eceip ot an latot ecafrus aera fo eht ,noitces ralucidneprep ycarucca fo IOC’O g as llew as its ecafrus aera ot ot eht noitcerid fo gnikrow ro eht ,serbif shall an ycarucca fo 5 .tnecrep nehT esremmi eht eb less than 50 tnecrep fo eht latot ecafrus aera tset eceip ni eht evisorroc noitulos and gnirb eht fo eht tset .eceip nI evitarapmoc ,stset eht oitar noitulos ot eht .liob lioB rof 5 sdoirep fo 48 h fo eht latot ecafrus aera ot eht latot ecafrus aera ,hcse using a hserf noitulos rof hcte .doirep fo eht snoitces shall eb tpek .tnatsnoc ehT dedlew retfA hcae ,doirep wash eht tset eceip ni ,retaw snemiceps dluohs eb tuc ni hcus a yaw that erom yrd and .hgiew than 13 mm htdiw fo esab latem is dedulcni ni rehtie edis fo eht .dlew NOTE - yB laiceps tnemeerga neewteb eht -retni detse ,seitrap eht tset yam eb detimil ot 3 sdoirep fo 48 h .hcae 4.4.2 Preparation gnidnepeD no eht esoprup fo eht tset ( ees 2.2 ,) 4.5.2 nl eht esac fo lareves txet seceip gnieb eht tset ,eceip rehtie htiw ro tuohtiw -azitisnes detset ni eht emas ,ksalf eht tset shall eb -moc noit ,tnemtaert shall eb deraperp as deificeps ni yletelp dellecnac ,fi retfa a doirep fo ,emit an rehtie 4.4.2.1 ro 4.4.2.2. Unless detats no eht detareggaxe ssol ni mass fo eno fo eht tset eceip 2 1 ) : 4991 IS 10461 ( Part is .deton ehT tset shall eb detaeper yletelpmoc s = ecafrus aera fo eht tset ,eceip ni no eht emas tset eceip hcihw shall eb detset erauqs ;sertemitnec yletarapes retfa gnivah enogrednu a hserf ecafrus nr = naem ssol ni mass rep ,doirep ,ni .noitaraperp grams; and 4.6 Expression of Results d = ytisned fo eht tset eceip ( 1 8mc/g >. 4.6.1 ehT tceffe fo eht kcatta yb eht cirtin noitulos is derusaem yb eht naem ssol ni mass rep .doirep 4.6.3 Sample Results 4.6.2 ehT noisorroc etar is nevig rehtie ni sselniatS sleets ( epyT 304 and 304 L ) era netfo sertemillim rep raey ( mm l-y ) yb alumrof ( 1 ) desu ni detartnecnoc cirtin dica stnemnorivne ro ni grams rep erauqs ertem rep ruoh ( )I-hem/g as ni eht esac fo eht gnissecorp fo raelcun ,sleuf by alumrof :)2( wastes, .cte nI hcus ,sesac mass ssol ni eht yeuH tset shall ton deecxe 0.46 mm 1-a ( -aviuqe 87 600 m tnel ot 18 sllim l-a .e.i 18 ypm .) sihT yam eb fXdXS . . . . . . , . . . . , . . . . . . . . . . . . . . . OI deredisnoc as a lareneg .ecnadiug fI eht IOOOOm noisorroc etar rof hcae doirep sesaercni revo xs t . . . . . l ...,.. s . . . . . . ...n ...L (2) that fo eht suoiverp ,doirep eht lairetam nac eb deredisnoc ot eb elbitpecsus ot ralunargretni t = doirep fo ,kcatta ni ;sruoh .noisorroc Bureau of Indian Standards BIS is a yrotutats noitutitsni dehsilbatse rednu eht Bureau of Indian Standards Act, 1986 ot etomorp& suoinomrah tnempoleved fo eht seitivitca fo ,noitazidradnats gnikram and ytilauq noitacifitrec fo sdoog and gnidnetta ot detcennoc srettam ni eht .yrtnuoc Copyright SIB has eht thgirypoc fo all its .snoitacilbup oN trap fo eseht snoitacilbup yam eb decudorper ni yna mrof tuohtiw eht roirp noissimrep ni gnitirw fo BIS. sihT seod ton edulcerp eht eerf ,esu ni ehit esruoc fo gnitnemelpmi eht standard, fo yrassecen ,sliated hcus as slobmys and ,sezis epyt ro edarg .snoitangised seiriuqnE gnitaler ot thgirypoc eb desserdda ot eht rotceriD ( snoitacilbuP ,) .SIB Review of Indian Standards stnemdnemA# era issued ot standards as eht deen sesira no eht basis fo .stnemmoc Standards era osla deweiver ;yllacidoirep a standard gnola htiw stnemdnema is demriffaer nehw hcus weiver setacidni that on segnahc era ;dedeen fi eht weiver setacidni that segnahc era ,dedeen ti is nekat up rof .noisiver sresU fo naidnI Standards dluohs niatrecsa that yeht era ni noissessop fo eht tsetal stnemdnema ro noitide yb gnirrefer ot eht tsetal issue fo SIB‘ ’koobdnaH and sdradnatS‘ ylhtnoM- .’snoitiddA sihT. naidnI dradnatS has neeb depoleved morf toD .oN : DTM 24 ( 3917 ) Amendments Issued Since Publication dnemA .oN etaD fo eussI txeT detceffA UAERUB FO NAIDNI SDRADNATS :sretrauqdaeH Manak ,navahB 9 rudahaB Shah rafaZ Marg, weN ihleD 110002 :senohpeleT 331 01 31, 331 57:31 smargeleT : Manaksanstha ( nommoC ot all seciffO ) lanoigeR :seciffO senohpeleT lartneC : Manak ,navahB 9 rudahaB Shah rafaZ Marg 331 01 31 WEN IHLED 110002 331 13 75 nretsaE : 41/l .T.I.C emehcS IIV M, .P.I.V ,daoR alotkinaM 37 84 99, 37 85 61 ATTUCLAC 700054 37 86 26, 37 86 62 nrehtroN : SC0 ,644-544 rotceS 35-C, HRAGIDNAHC 160036 53 38 43, 53 16 40 i 53 23 84 nrehtuoS : .T.I.C Campus, VI ssorC ,daoR MADR-AS 600113 235 02 16, 235 04 42 235 15 19, 235 23 15 nretseW : ,ayalakanaM 9E ,loraM,CDIM irehdnA ( East ) C 632 92 95, 632 78 58 YABMOB 430093 632 78 91, 632 78 92 sehcnarB : .DABADAMHA .EROLAGNAB .LAPOHB .RAWHSENABUHB .EROTABMIOC .DABADIRAF .DABAIZAHG .ITAHAWUG .DABAREDYH JAIPUR. .RUPNAK .WONKCUL .ANTAP .MARUPAHTNANAVURIHT detnirP at nogaraP ,sesirpretnE ,ihleD aidnI

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