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Handbook of superconducting materials. Volume 2, Processing and cryogenics PDF

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Handbook of Superconductivity Handbook of Superconductivity Processing and Cryogenics, Volume Two Second Edition Edited by David A. Cardwell David C. Larbalestier Aleksander I. Braginski MATLAB® is a trademark of The MathWorks, Inc. and is used with permission. The MathWorks does not warrant the accuracy of the text or exer- cises in this book. This book's use or discussion of MATLAB® software or related products does not constitute endorsement or sponsorship by The MathWorks of a particular pedagogical approach or particular use of the MATLAB® software. Second edition published 2023 by CRC Press 6000 Broken Sound Parkway NW, Suite 300, Boca Raton, FL 33487-2742 and by CRC Press 2 Park Square, Milton Park, Abingdon, Oxon, OX14 4RN © 2023 Taylor & Francis Group, LLC First edition published by IOP Publishing 2003 CRC Press is an imprint of Taylor & Francis Group, LLC Reasonable efforts have been made to publish reliable data and information, but the author and publisher cannot assume responsibility for the validity of all materials or the consequences of their use. The authors and publishers have attempted to trace the copyright holders of all material reproduced in this publication and apologize to copyright holders if permission to publish in this form has not been obtained. If any copyright material has not been acknowledged please write and let us know so we may rectify in any future reprint. Except as permitted under U.S. Copyright Law, no part of this book may be reprinted, reproduced, transmitted, or utilized in any form by any elec- tronic, mechanical, or other means, now known or hereafter invented, including photocopying, microfilming, and recording, or in any information storage or retrieval system, without written permission from the publishers. For permission to photocopy or use material electronically from this work, access www.copyright.com or contact the Copyright Clearance Center, Inc. (CCC), 222 Rosewood Drive, Danvers, MA 01923, 978-750-8400. For works that are not available on CCC please contact mpkbookspermissions@ tandf.co.uk Trademark notice: Product or corporate names may be trademarks or registered trademarks and are used only for identification and explanation without intent to infringe. ISBN: 978-1-4398-1734-6 (hbk) ISBN: 978-0-3676-8908-7 (pbk) ISBN: 978-0-4291-8302-7 (ebk) DOI: 10.1201/9780429183027 Typeset in Minion Pro by KnowledgeWorks Global Ltd. Contents Foreword ................................................................................................................................................. ix Preface..................................................................................................................................................... xi Acknowledgements ...............................................................................................................................xiii Editors-in-Chief .....................................................................................................................................xv Contributors ........................................................................................................................................xvii PART E Processing E1 Introduction to Processing Methods .......................................................................................3 Kazumasa Iida E2 Introduction to Section E2: Bulk Materials ............................................................................7 Kazumasa Iida E2.1 Introduction to Bulk Firing Techniques .................................................................................8 Mark O. Rikel and Frank N. Werfel E2.2 (RE)BCO Melt Processing Techniques: Fundamentals of the Melt Process ........................28 Yunhua Shi and David A. Cardwell E2.3 Melt Processing Techniques: Melt Processing for BSCCO ...................................................52 Jun-ichi Shimoyama E2.4 Growth of Superconducting Single Crystals .........................................................................58 Debra L. Kaiser and Lynn F. Schneemeyer E2.5 Growth of A15 Type Single Crystals and Polycrystals and Their Physical Properties ........86 René Flükiger E2.6 Irradiation ..............................................................................................................................97 Harald W. Weber E2.7 Superconductors in Future Accelerators: Irradiation Problems ..........................................114 René Flükiger, Tiziana Spina, Francesco Cerutti, Amalia Ballarino, and Luca Bottura E3 Introduction to Section E3: Processing of Wires and Tapes ..............................................123 Jianyi Jiang E3.1 Processing of High T Conductors: The Compound Bi-2212 ..............................................125 c Jianyi Jiang and Eric E. Hellstrom E3.2 Processing of High T Conductors: The Compound Bi,Pb(2223) .......................................144 c Kenichi Sato v vi Contents E3.3 Highlights on Tl(1223) ......................................................................................................... 153 Athena Safa Sefat E3.4 Processing of High T Conductors: The Compound YBCO ............................................... 162 c Judith L. MacManus-Driscoll E3.5 Processing of High T Conductors: The Compound Hg(1223) ........................................... 170 c Ayako Yamamoto E3.6 Overview of High Field LTS Materials (Without Nb Sn) ....................................................174 3 René Flükiger E3.7 Processing of Low T Conductors: The Alloy Nb–Ti .......................................................... 187 c Lance D. Cooley, Peter J. Lee, and David C. Larbalestier E3.8 Processing of Low T Conductors: The Compound Nb Sn .................................................213 c 3 Ian Pong E3.9 Processing of Low T Conductors: The Compound Nb Al .................................................276 c 3 Takao Takeuchi, Akihiro Kikuchi, Nobuya Banno, and Yasuo Iijima E3.10 Processing of Low T Conductors: The Compounds PbMo S and SnMo S .....................291 c 6 8 6 8 Bernd Seeber E3.11 Processing of Low T Conductors: The Compound MgB ..................................................308 c 2 Akiyasu Yamamoto and René Flükiger E3.12 Processing Pnictide Superconductors .................................................................................324 Jeremy D. Weiss and Eric E. Hellstrom E4 Introduction to Section E4: Thick and Thin Films ............................................................332 François Weiss and Michael Lorenz E4.1 Substrates and Functional Buffer Layers .............................................................................334 Bernhard Holzapfel and Jörg Wiesmann E4.2 Physical Vapor Thin-Film Deposition Techniques .............................................................348 Roger Wördenweber E4.3 Chemical Deposition Processes for REBa Cu O Coated Conductors ...............................365 2 3 7 François Weiss and Carmen Jimenez E4.4 High Temperature Superconductor Films: Processing Techniques ....................................382 Paul Seidel and Volker Tympel E4.5 Processing and Manufacture of Josephson Junctions: Low-T ............................................403 c Sergey K. Tolpygo, Thomas Schurig, and Johannes Kohlmann E4.6 Processing and Manufacture of Josephson Junctions: High-T ..........................................425 c Aleksander I. Braginski and Brian H. Moeckly E5 Introduction to Section E5: Superconductor Contacts .......................................................447 Kazumasa Iida E5.1 Superconductor to Normal-Metal Contacts ........................................................................448 Jack W. Ekin E5.2 Resistive High Current Splices ............................................................................................467 Christian Scheuerlein E5.3 Persistent Mode Joints .........................................................................................................480 Susie Speller, Timothy Davies, and Chris Grovenor Contents vii PART F Refrigeration Methods F1 Introduction to Part F: Refrigeration Methods ...................................................................499 Ray Radebaugh F1.1 Review of Refrigeration Methods ........................................................................................501 Ray Radebaugh F1.2 Pulse Tube Cryocoolers........................................................................................................519 John M. Pfotenhauer and Xiaoqin Zhi F1.3 Gifford–McMahon Cryocoolers ..........................................................................................535 Mingyao Xu and Ralph Longsworth F1.4 Microcooling ........................................................................................................................547 Marcel ter Brake and Haishan Cao F1.5 Cooling with Liquid Helium ................................................................................................562 John M. Pfotenhauer Glossary ................................................................................................................................................573 Index ..................................................................................................................................................... 591 Foreword It is a pleasure to introduce the second edition of the the tables are turned – a range of applications are now nudg- Handbook of Superconductivity, now with the subtitle Theory, ing their way onto the market even though we do not really Materials, Processing, Characterization and Applications. In understand them. combination, the enlarged title expresses the very broad scope That, of course, overstates the matter. We know that the of this publication. It is a mark of the ongoing vigour of the supercarriers in HTS are Cooper pairs and their symmetry in field of superconductivity that, in the 15 years or so since the reciprocal space is predominantly d-wave. We quantitatively first edition, tremendous progress has been made in theory, understand many properties of HTS materials such as the materials discovery and applications. Completely new topics effect of impurities in suppressing superconductivity and the have emerged, including topological superconductors, single- temperature dependence of the specific heat, thermal expan- atomic-layer superconductivity and twistronics. New super- sion and superfluid density. However, this description is pri- conductors have been predicted and demonstrated, most marily based on thermodynamics and the observed d-wave notably the clathrate superhydride LaH , which supercon- symmetry. What we lack is a clear understanding of the mech- 10 ducts close to room temperature (though at several megabars). anism that binds the pairs in the first place and a relation- New applied technologies, such as flux pumps, have been ship between the magnitude of this interaction and the energy demonstrated in motors, generators and MRI. This new edi- scale of the superconductivity set by the maximum d-wave tion is therefore timely in presenting the broad vista of our gap amplitude. The difficulty here is the strongly interacting current knowledge in basic and applied superconductivity. electronic system and HTS cuprates, which, in this sense, are Superconductivity is one of the most remarkable physi- just part of a much wider problem of strongly correlated tran- cal states yet discovered. More than any other known effect, sition metal oxides that incorporate manganites, ruthenates, superconductivity brings quantum mechanics to the scale of cuprates, vanadates and tungstates to name just a few, not to the everyday world where a single, coherent quantum state mention hybrid materials, such as the ruthenocuprates, in may extend over a distance of metres – or even kilometres – which magnetism and superconductivity coexist. depending on the size of a coil or length of superconducting Such materials not only formally defy a suitable pertur- wire. And perhaps less well known, the underlying physics bation treatment, but they exhibit many different types of extends in scale to the very size of the universe, for the Higgs ground-state correlation that compete with each other. Thus, mechanism, by which all matter particles acquire their mass, in the HTS cuprates, we currently struggle with the issues has the same symmetry-breaking origins as superconductivity. of charge ordering, spin ordering, nematicity and supercon- There is something in this mysterious state that never fails ductivity and the question as to whether these are intimately to enchant its beholders: researcher, student or lay-person linked or, in fact, compete. What if we could methodically alike. The allure is to be found not only in the demonstrations remove each of these competing states one by one? Would of infinite conductivity and levitation, not only in the ongo- superconductivity remain at all as the ground state? Would ing intellectual puzzle of its root physics, but also in the bold it fade away along with its supporters? Or might it even be technologies that superconductivity enables. enhanced? What is the importance of fluctuations or of short- The puzzle of superconductivity resisted explanation for a range versus long-range correlations? A current challenge to very long time. The eventual breakthrough with the Bardeen– the community is to develop the tools to do precisely these Cooper–Schrieffer theory, 46 years after their discovery, kinds of elucidating experiments. actually preceded, by about a decade, any significant practi- The central approach then to these issues is systematic cal and commercial development of these remarkable mate- measurement in high-quality materials. With the combined rials. Today, half a century later still, the progress of science improvement in quality of single crystals as well as resolution and technology is greatly accelerated. And yet a theory of the in low-energy experimental techniques, much progress has cuprate high temperature superconductors (HTS), discov- been made in the last several decades leading to many surpris- ered 33 years ago, still remains elusive. For these materials ing new results. By “systematic” I mean variation in properties ix

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