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Editedby Gu¨nterGauglitzandDavidS.Moore HandbookofSpectroscopy RelatedTitles Gu¨nther,H. Berger,S.,Sicker,D. NMR Spectroscopy ClassicsinSpectroscopy BasicPrinciples,Conceptsand IsolationandStructureElucidationof ApplicationsinChemistry NaturalProducts Third,CompletelyRevisedandUpdated Edition 2009 ISBN:978-3-527-32617-4 2013 ISBN:978-3-527-33004-1 Andrews,D.L.(ed.) EncyclopediaofApplied Zerbe,O.,Jurt,S. Spectroscopy AppliedNMRSpectroscopyfor Series:EncyclopediaofAppliedPhysics ChemistsandLifeScientists 2009 2013 ISBN:978-3-527-40773-6 ISBN:978-3-527-32774-4 Friebolin,H. BasicOne-and Two-Dimensional NMR Spectroscopy Fifth,CompletelyRevisedandEnlarged Edition 2010 ISBN:978-3-527-32782-9 Edited by Gu¨nter Gauglitz and David S. Moore Handbook of Spectroscopy Second, Enlarged Edition Volume 1 Edited by Gu¨nter Gauglitz and David S. Moore Handbook of Spectroscopy Second, Enlarged Edition Volume 2 Edited by Gu¨nter Gauglitz and David S. Moore Handbook of Spectroscopy Second, Enlarged Edition Volume 3 Edited by Gu¨nter Gauglitz and David S. Moore Handbook of Spectroscopy Second, Enlarged Edition Volume 4 TheEditors AllbookspublishedbyWiley-VCHare carefullyproduced.Nevertheless,authors, editors,andpublisherdonotwarrantthe Prof.Dr.Gu¨nterGauglitz informationcontainedinthesebooks, UniversityofTu¨bingen includingthisbook,tobefreeoferrors. InstituteforPhysicalandTheoretical Readersareadvisedtokeepinmindthat Chemistry statements,data,illustrations,procedural AufderMorgenstelle18 detailsorotheritemsmayinadvertentlybe 72076Tu¨bingen inaccurate. Germany Dr.DavidS.Moore LibraryofCongressCardNo.:appliedfor ShockandDetonationPhysics LosAlamosNationalLaboratory BritishLibraryCataloguing-in-Publication MS-P952,LosAlamos,NM87545 Data USA Acataloguerecordforthisbookisavailable fromtheBritishLibrary. Bibliographicinformationpublishedbythe DeutscheNationalbibliothek TheDeutscheNationalbibliothek liststhispublicationintheDeutsche Nationalbibliografie;detailedbibliographic dataareavailableontheInternetat <http://dnb.d-nb.de>. ©2014Wiley-VCHVerlag&Co.KGaA, Boschstr.12,69469Weinheim,Germany Allrightsreserved(includingthoseof translationintootherlanguages).Nopart ofthisbookmaybereproducedinany form–byphotoprinting,microfilm,orany othermeans–nortransmittedortranslated intoamachinelanguagewithoutwritten permissionfromthepublishers.Registered names,trademarks,etc.usedinthisbook, evenwhennotspecificallymarkedassuch, arenottobeconsideredunprotectedbylaw. PrintISBN:978-3-527-32150-6 ePDFISBN:978-3-527-65473-4 ePubISBN:978-3-527-65472-7 mobiISBN:978-3-527-65471-0 oBookISBN:978-3-527-65470-3 Cover-Design BerndAdamDesign, Weinheim,Germany Typesetting LaserwordsPrivateLimited, Chennai,India PrintingandBinding MarkonoPrintMedia PteLtd,Singapore Printedonacid-freepaper V Contents ListofContributors XVII Preface XXIX Volume1 SectionI SamplePreparationandSamplePretreatment 1 1 PreparationofLiquidandSolidSamples 3 BrianM.CullumandTuanVo-Dinh 1.1 Introduction 3 1.2 PreparationofSamplesforAnalysis 3 1.2.1 MeasurementProcess 3 1.2.2 PreparationofSamplesforAnalysis 4 1.2.3 SolidSamples 5 1.2.4 LiquidSamples 10 References 13 2 LiquidandSolidSampleCollection 15 PaolodeZorzi 2.1 Introduction 15 2.2 SamplingProcess 16 2.3 SamplingStrategyandCollection 18 2.3.1 LiquidSampling 20 2.3.2 SolidSampling 22 2.4 QA/QCinSampling 23 References 26 SectionII Methods1:OpticalSpectroscopy 27 Introduction 29 References 30