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Handbook Of Instrumental Techniques For Analytical Chemistry PDF

728 Pages·1997·12.79 MB·English
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Preview Handbook Of Instrumental Techniques For Analytical Chemistry

am © TECHNIQUES ANALYTICAL CHEMISTRY FRANK SETTLE, evitor Handbook ofInstrumental Techniques f for Analytical Chemistry Frank A. Settle, Editor 'o Join a Peeatioe Hall Interns pulling il, poine to: rips/4rssesprenhall. comma fists Preotice ial, Lppee Saddle River, NJ F458, leoRarerrakaitareney annem Sere Medes Mins. Mb ee ag Dvr oe gt oF Intra ank ally me i pb dec al Sani Lael ane Us Lil ane Pla latnpaat fil Scr Protected ens Dealt avon Un Ne Des te esd atipaine Sum Satu Te Spon ivvatnn nF Ie ll a col Ny pt uth bergen a oy, Dedication hie bk ctictel che nuaeies ufc gereralag wnaale oajeeuriatio he slevelaainen fe eine Feel etry al ad pre influence om thea sell senna prucinioners ut anaticdl chery. De Sid Sa, profewor ofchersy xr che Ukiersiy uf Machi, i ering incr asl alee cea hy Aevelopel de anal! ioe procera ata or, Dr, Lucaet Baa Rees, artes Felis Gir Crivenity of Georgia, Pune Uivershy ane che Masons Inet Ter fel. ne an onewandg einige kya ha worked nro ny arm Faunjical heme. De, Jahn KE, Tagor, a scents for over Sears he rin nine Standards and Technolgy he old Nieional areas of Salers ses mation reasune oF rare lavwcedge Fo addin tu thee professional vontlrdons altace were gentlerse™ “rho alee sce rach posorteny chu thei elaronlops with Fin, cleats, and sade Then ala deicrced 9 the memuny of Tle Baker che ahr of the shaper ur capillary lowtropharess rhu completed eas chope beforohis death Contents Section? ite tH ee es Chapter Howto Use the Handbook ........ weed Front Ste Eltor Puupase and Senge : a Oxganivanon : mila Summary : wn 3 Shapter2_ Sample Preparation in Analytical Chemisty (Organic Analysis) vere Amd E Moors Inuraduetint Types of Suuples Encountered «1. : ne Sauiple Preparation for Solid and Seudsold Samples ern s Exuneuon af Solid Spee...» peer 28 ‘Sample Heeparation Methods for Liquid Stmples. «0. nas Degiewisalon in Chranatvgraphy se as Chapter 3 Sample Preparation in Analytical Chemistry Unorganic Analysis). : Jaf Moody and Chole te Becki Classical Clu Analysis bee . 56 Seupling : ne se Sommple Drying see : aoa 38 Souple Weighing... TINIE : 0 Sample Dissolution ane eERIEEE Exraction, Preconcenteation, and Separations nl 6s Dilution spd Matrix Matching. : on 66 “ Hanabookl istamentlTeniquesfor Analyt here reparation vf Standard Solutions « 66 Aiton of Soop Preps “ Conclusions. seve eRe RnSRILOIDTEEET) Chapter 4 Quantitative Measurements. . BB EariVieey Limie of Desuton, Lint uf Quansiiacon, and Sensitivity Calilnaton, Ibterferences, Coutsorination, al Low uf Analy. Sunpting Vertis of Accuracy Chapter 5 Managing Laboratory inform: 81 Pobert Megargle Laboratories as Information Producers fi Properties of Gond {nformasicn. 8 Laboratory bniormation Managemint Sytem. Liss Conclusions 09 Chapter 6 Laboratory Automation . 101 Joe iicous Whar is Laboratory Autontation? 104 Approaches 19 Laboratory Antomacon 108 Allahevarory Aneomation Trl us Plaaning fr Faboracory Aueomaton it6 Validation ut Chapter 7 introduction Mary tane Van Sant Chapter 8 Gas Chromatography ... ‘ary dane Var Sant Summary Ls Tnnradaetion 128 How Te Works 128 What Ir Does 0 Analytical Information 0 Apnlicetions: Nits and Boles, Chapter9 High-Performance Liquid Chromatography Phyl Brown and kathayn DeAntonis Tatracerion How fy Wists Whar Fr nee Spplicaione Nis and Toi. Chapter 10 Capillary Electrophoresis. Dole R Boker Sanmaty Treeeductian Tow Works, What Doss Analyte lnforeaution Applicatioas Nis and Bolrs Chapter 11 Supercritical Flue Chromatography and Extraction. . amy Toytor Suuuenesy Auzeduetion “Haw le Works What le Does Applications ‘Nas aud Bolts, Chapter 12 lon Chromatography . dob Satter Summary lauredaction + How Lt Worle What I Dass Aculpeal Informatio ‘Appliations ‘Nous and Bolts Handhnck ners Tachraes for Anite Chemin Chapter 13 Thin-Layer (Planar) Chromatography Dieter Joenehen Summary Tnerosucron Vion Te Werks Wha F Does. Anahsica Tnformarion Appheaions Ninn and Boies Chapter 14. Introduction, Poul Bovis Chapter 15 Infrared Spectroscopy . 9. Sherman Hey, PAP Sunematy trreduction How 1, Works What ht Does, Asay uel Aufornution Applications, Nins and Bolts Chapter 16 Raman Spectroscopy ...- Dennis? Stromien Sumniey Javon How As Works What ie Does, Analyt Loformnation Applistivas. Nuls Axl Bolts Chapter 17 Nuclear Magnetic Resonance Spectroscopy Michael McGregor Sumuary Introduction Mow Tr Works. m What le Does aF Aniltiod Lnforeastion 320 ‘Applications : mn 329 Nuts zna Bul mn t 34 Chapter 18 X-Ray Diffraction .. Joseph Formica Susmuary Intradaction Howe Ir Works. What Ie Des Analytical lnforntion Applivaions Rus nl Bois See Chapter 19 Introduction. Ear Wehvy Capsule Pesuripcions of the Techniques Diseased in This Seerion 362 Chapter 20 Atomic Absorption Spectrometry 373 Joseph Sredeon Tnrodaction Tow Ir Work Whar les Applications Nis and Pits Chapter 21__ Inductively Coupled Plasma Atomic Emission Spectroscopy .... Arthur W. arnes Snmmary 395 Tonroduesinn 198 Hone Te Worke aa, Whar It nes an Herabook fnsvurant!Tecwavester alc Chery Analytical Tnfnemarion Applicauons Nurgand Bolts Chapter 22 inductively Coupled Plasma Mass Spectrometry Arthur Varnes Summary Toevodnetion Hons Works Whar foes Analytical Soanation Applionions Wins and Bes Chapter 23 Atomic Fluorescence Spectrometry Davi Bucher Suoiaey uducus Blow h Works ‘What ft Does. Analyial Yorn Applies Nab aad Belts Chapter 24 X-Ray Fluorescence Spectrometry George 5 Haveito Swaunary Intruduction Low FeWorks What le Does Analytical Infomation Applications Netyand Bolt Chapter 25. Ultraviolet and Visible Molecular Absorption Spectrometry .. James A Howe Summary Sncrstuction low feWorks 41 283

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