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From nanopowders to functional materials : proceedings of Symposium G, European Materials Research Society Fall Meeting, Warsaw University of Technology, 6th-10th September, 2004 PDF

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From Nanopowders to Functional Materials From Nanopowders to Functional Materials Proceedings of Symposium G European Materials Research Society Fall Meeting Warsaw University of Technology th th 6 -10 September, 2004 Edited by Radu Robert Piticescu, Witold Łojkowski and John R. Blizzard TRANS TECH PUBLICATIONS LTD Switzerland • Germany • UK • USA Copyright © 2005 Trans Tech Publications Ltd, Switzerland All rights reserved. No part of the contents of this book may be reproduced or transmitted in any form or by any means without the written permission of the publisher. Trans Tech Publications Ltd Brandrain 6 CH-8707 Uetikon-Zuerich Switzerland http://www.ttp.net Volume 106 of Solid State Phenomena ISSN 1012-0394 (Pt. B of Diffusion and Defect Data - Solid State Data (ISSN 0377-6883)) Covered by Science Citation Index Full text available online at http://www.scientific.net Distributed worldwide by and in the Americas by Trans Tech Publications Ltd Trans Tech Publications Inc Brandrain 6 PO Box 699, May Street CH-8707 Uetikon-Zuerich Enfield, NH 03748 Switzerland USA Phone: +1 (603) 632-737 Fax: +41 (44) 922 10 33 Fax: +1 (603) 632-5611 e-mail: [email protected] e-mail: [email protected] THE EUROPEAN MATERIALS RESEARCH SOCIETY The European Materials Research Society (E-MRS) is a non-profit making scientific society founded in 1983 with its Headquarters in Strasbourg, France. The Society focuses its activities on creating synergy from the interaction between interdisciplinary, innovative fields of materials research. Great attention is given to spreading and exchanging information and promoting technology transfer from public institutions to industry. The primary objective of E-MRS is to promote and enhance the efficiency of research in Europe in the field of Advanced Materials. E-MRS seeks to quickly inform researchers about the scientific and technological developments in their fields of interest, taking advantage of the Society’s links with other Materials Research Societies belonging to the International Union (IUMRS). Since 2002, in parallel with the Spring Meeting held in Strasbourg which attracts over 1500 participants, Fall Meetings have been held in Warsaw. The 2004 Fall Meeting consisted of 9 symposia running concurrently, Plenary Sessions, a joint session with other symposia and included an exhibition of relevant products and services as well as training activities for young researchers and scientists. E-MRS General Secretary P. Siffert E-MRS BP 20 67037 Strasbourg Cedex 2 France Telephone: +33 3 88 10 65 43 +33 3 88 10 62 55 Fax: +33 3 88 10 62 93 e-mail: [email protected] THE E-MRS FALL MEETING CHAIRMEN Krzysztof J. Kurzydłowski Warsaw University of Technology, Warsaw Witold Łojkowski Institute of High Pressure Physics, Polish Academy of Sciences, Warsaw Andrzej Mycielski Institute of Physics, Polish Academy of Sciences, Warsaw Paul Siffert European Materials Research Society, Strasbourg, France E-MRS FALL MEETING 2004 CONFERENCE ORGANISERS Polish Materials Society Polskie Towarzystwo Materialoznawcze ul. Wołoska 141 Telephone: +48 (0)22 660 84 41 02-507 Warsaw Fax: +48 (0)22 848 4947 Poland e-mail: [email protected] Institute of High Pressure Physics, Polish Academy of Sciences ul. Sokołowska 29/37 Telephone: +48 (0)22 632 50 10 01-142 Warsaw Fax: +48 (0)22 632 42 18 Poland e-mail: [email protected] Institute of Physics, Polish Academy of Sciences Al. Lotników 32/46 Telephone: +48 (0)22 843 66 01 02-668 Warsaw Fax: +48 (0)22 843 09 26 Poland e-mail: [email protected] Faculty of Materials Science and Engineering Warsaw University of Technology ul. Wołoska 141 Telephone: +48 (0)22 849 99 29 02-507 Warsaw Fax: +48 (0)22 660 85 14 Poland e-mail: [email protected] E-MRS General Secretary P. Siffert E-MRS Telephone: +33 3 88 10 65 43 BP 20 +33 3 88 10 62 55 67037 Strasbourg Cedex 2 Fax: +33 3 88 10 62 93 France e-mail: [email protected] Local Organising Committee K.J. Kurzydłowski A. Mycielski W. Łojkowski A.Szadkowski H. Garbacz M. Lewandowska R. Pielaszek M. Ryszkowska L. Ciupiński J.R. Blizzard ACKNOWLEDGEMENTS The organisers of Symposium G of the E-MRS Fall Meeting 2004 acknowledge the support given by: Polish Ministry of Science and Information Technology Romanian Ministry of Education and Research Directorate for European Integration The Polish Materials Society Faculty of Materials Science and Engineering Warsaw University of Technology Institute of High Pressure Physics “UNIPRESS” Polish Academy of Sciences SPUB-MSN, SPUB-PRENABIO "Network Namic "Nano and Microtechnology" The European Commission Center of Excellence Project PRENABIO, Contract: No GIMA-CT-2002-04055 Nanostructured materials Network, Contract: No ICAI-CT_2002-60028 EUROPEAN MATERIALS RESEARCH SOCIETY Network Namic "Nano and Microtechnology" E-MRS FALL MEETING 2004 – SYMPOSIUM G FROM NANOPOWDERS TO FUNCTIONAL MATERIALS Introduction Research and development in the whole area of nanomaterials including – thin films, nanowires, nanocrystals, nano-composites and nanostructured bulk materials – is continuing to increase year by year. More and more attention is being focused on research to enable greater control of the structure at nanometer level in order to ensure that the desired functional properties can be obtained. The symposium aim was to enable those working at the leading edge of research to present and debate the progress being made in the theory and applications of functionalised nanoparticles within a multidisciplinary topic. Applications of functional materials based on their mechanical, catalytic, electronic, optical and photonic properties, atomic and transport properties, electrical, magnetic and ferroelectric properties as well as biocompatibility presented in this symposium are expected to innovate the nanotechnologies of tomorrow. As part of the symposium a Joint Session was held with Symposium I – Metal Based Nanomaterials, Thin Films and Surfaces. This volume includes the abstracts of this Joint Session as well as the abstracts of the Plenary Session. Radu Robert Piticescu Witold Łojkowski John R. Blizzard The Symposium Organisers Radu Robert Piticescu, Institute for Non-Ferrous and Rare Metals, Bucharest, Romania e-mail: [email protected] Witold Lojkowski, Institute for High Pressure Physics, Polish Academy of Sciences, Warsaw, Poland e-mail: [email protected] Claude Monty, Procédés, Matériaux et Energie Solaire (PROMES), Font Romeu, France e-mail: [email protected] Table of Contents Luminescence Properties of Neodymium-Doped Yttrium Aluminium Garnet Obtained by the Co-Precipitation Method Combined with the Mechanical Process E. Caponetti, M.L. Saladino, D. Chillura Martino, L. Pedone, S. Enzo, S. Russu, M. Bettinelli and A. Speghini 7 High-Pressure Induced Structural Decomposition of RE-Doped YAG Nanoceramics D. Hreniak, S. Gierlotka, W. Łojkowski, W. Stręk, P. Mazur and R. Fedyk 17 Formation of Core-Shell Nanoparticles by Laser Ablation of Copper and Brass in Liquids P.V. Kazakevich, A.V. Simakin, V.V. Voronov, G.A. Shafeev, D. Starikov and A. Bensaoula 23 Laser-Induced Size and Shape Transformation of Silver Colloidal Nanoparticles N. Tarasenko, A. Butsen, G. Shevchenko and I. Yakutik 27 Direct Electrochemical Activity and Stability of Capped Platinum Nanoparticles S. Cavaliere, F. Raynal, A. Etcheberry, M. Herlem and H. Perez 31 Precipitation of Nickel Hydroxides from Nickel Dodecylsulphate C. Coudun and J. Hochepied 35 Microstructural Characterization of BaTiO Ceramic Nanoparticles Synthesized by the 3 Hydrothermal Technique X.H. Zhu, J.M. Zhu, S.H. Zhou, Z.G. Liu, N.B. Ming and D. Hesse 41 Hybrid HAp-Maleic Anhydride Copolymer Nanocomposites Obtained by In Situ Functionalisation R.M. Piticescu, G.C. Chitanu, M. Albulescu, M. Giurginca, M.L. Popescu and W. Łojkowski 47 Review on the Production and Synthesis of Nanosized SnO 2 S. Papargyri, D.N. Tsipas, D.A. Papargyris, A.I. Botis and A.D. Papargyris 57 Phase Stability in Nanocrystalline Zirconia G. Baldinozzi, D. Simeone, D. Gosset and M. Dutheil 63 Natural Opal as a Model System for Studying the Process of Biomineralization L. Pramatarova, E. Pecheva, R. Presker, U. Schwarz and R. Kniep 75 New Nano-Sized Sensing Drug and Its Clinical Application R. Ion and D. Brezoi 79 Nanostructure, Nanochemistry and Grain Boundary Conductivity of Yttria-Doped Zirconia A. Rizea, J.M. Raulot, C. Petot, G. Petot-Ervas and G. Baldinozzi 83 Wavelength Tunable Random Laser E. Tikhonov, V.P. Yashchuk, O. Prygodjuk and V. Bezrodny 87 Potential of Nano-Sized Rare Earth Fluorides in Optical Applications U.H. Kynast, M.M. Lezhnina and H. Kätker 93 Luminescence of ZrO Nanocrystals 2 D. Millers, L. Grigorjeva, W. Łojkowski and A. Opalińska 103 Additional Absorption in the Multiply Scattering Absorbing Media V.P. Yashchuk, E. Tikhonov, O. Prygodjuk, O. Levandovska and M. Zhuravsky 109 Lateral Size of Self-Patterned Nanostructures Controlled by Multi-Step Deposition I. Szafraniak, D. Hesse and M. Alexe 117 Hydroxyapatite Growth on Glass/CdSe/SiO Nanostructures x L. Pramatarova, E. Pecheva, D. Nesheva, Z. Aneva, A.L. Tóth, E. Horváth and F. Riesz 123 Spectroscopic Ellipsometry and Raman Studies on Sputtered TiO Thin Films 2 B. Karunagaran, Y.K. Kim, K.H. Kim, S.K. Dhungel, J.S. Yoo, D. Mangalaraj and J. Yi 127 Formation of Thallium Sulphide Layers on Polyethylene (PE) Sulphurised in a Solution of Higher Polythionic Acid I. Bružaitė, V. Janickis, I. Ancutienė and V. Snitka 133 Polymer Matrix Composites with Particles of TiC Obtained by a Sol-Gel Method K. Konopka, A. Biedunkiewicz, A. Boczkowska, Z. Rosłaniec and K.J. Kurzydłowski 141 Self-Organization and Dynamic Characteristics Study of Nanostructured Liquid Crystal Compounds N.V. Kamanina, Y.A. Zubtsova, V.A. Shulev, M.M. Mikhailova, A.I. Denisyuk, S.V. Butyanov, S.V. Murashov and I.Y. Sapurina 145 b From Nanopowders to Functional Materials CBN Composites with a Nanosized Binding Phase W. Gorczyńska-Zawiślan, E. Benko and P. Klimczyk 149 Microstructure and Mechanical Properties of Spark Plasma Sintered ZrO -Al O -TiC N 2 2 3 0.5 0.5 Nanocomposites K. Vanmeensel, K.Y. Sastry, J. Hennicke, G. Anné, D. Jiang, A.I. Laptev, J. Vleugels and O. Van der Biest 153 Effect of Sintering Temperature on Structure and Properties of Al O /Ni-P Composites 2 3 with Interpenetrating Phases J. Michalski, M.J. Woźniak, K. Konopka, J. Bieliński, S. Gierlotka and K.J. Kurzydłowski 161 Plenary Session Abstracts 167 Joint Session Abstracts 173

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