Farhan, Ahmed Hilal (2016) Characterization of rubberized cement-stabilized roadbase mixtures. PhD thesis, University of Nottingham. Access from the University of Nottingham repository: http://eprints.nottingham.ac.uk/32840/1/Ahmed%20Hilal%20Farhan%27s%20PhD %20Thesis.pdf Copyright and reuse: The Nottingham ePrints service makes this work by researchers of the University of Nottingham available open access under the following conditions. This article is made available under the University of Nottingham End User licence and may be reused according to the conditions of the licence. For more details see: http://eprints.nottingham.ac.uk/end_user_agreement.pdf For more information, please contact [email protected] Facultyof Engineering–Civil EngineeringDepartment Characterization of Rubberized Cement-Stabilized Roadbase Mixtures By Ahmed Hilal Farhan B.Sc. Civil Eng., M.Sc. Highways and Airports Eng. Thesis submitted to the University of Nottingham for the degree of Doctor of Philosophy in Civil Engineering April2016 i Abstract Due to urbanization, industrialization and population increase, a substantial increase occurred in the number of vehicles and hence large numbers of end-of-use tires are being disposed every year. The vast majority of these tires are stockpiled or used as a fuel for combustion which, in both cases, affects the environment detrimentally. The use of tire rubber in cement-stabilized aggregate mixtures (CSAMs) will ensure beneficial use of large quantities of these waste materials, saving natural resources and may enhance the properties ofCSAMsespeciallytheserelatedtobrittlenessandsensitivitytofatiguefailure. Research was undertaken to investigate, at macro and mesoscale levels, the effect of both rubber and degree of stabilization and their combination on the behaviour of CSAMs in terms of the most influential pavement design properties under different static and dynamic modes of loading. These properties are strength, stiffness and fatigue. A range of testing equipment, methodologies and tools was developed, suggested and implemented to perform this investigation. Further investigation was also conducted to provide better understanding of the damage and failure mechanism through quantitative studying of the fractured surface, internalstructureandsurfacecrackingpatternsunderdifferenttestingmodes. The results of this study revealed that the addition of rubber has a negative effect on the compaction efficiency, compressive, flexural and tensile strengths while the stiffness, under different testing modes, was slightly reduced. In addition, a tougher mixture was produced after rubber-modification which means a change from a brittle to a more ductile behaviour. Thisbehaviourwasobservedthroughdifferentstiffnessmodulusevaluationmethods.Onthe other hand, increase in cementation level has resulted in an increase in both strength and stiffness for both reference and rubberized mixtures. However, the decrease in the mixtures’ strengthdue torubberizationwas more obvious inhighlycementedmixtures thanthe lightly cemented ones. On the other hand, a greater decline in the mixtures’ stiffness, due to rubber incorporation, was observed at low cement contents. This behaviour is related to the void- like behaviour which depends, to large extent, on the relative stiffness between rubber and surroundingmatrix. ii Quantification of the fractured surfaces and cracking pattern utilizing the photogrammatry and fractal dimension concepts, respectively, revealed that the addition of rubber resulted in rougher and more tortuous cracks and increases disperse-ability of these cracks. This means the rubber-modification changed the cracking pattern which implies better load transfer throughthecracksandlessriskofreflectioncracking. The investigation of the internal structure, at mesoscale level, showed that the cracks were propagated through the rubber particles at all investigated cementation levels. This contributed to a lengthening of the crack path and to the delaying of crack propagation by absorbing and relieving the stresses at the crack tip, especially at the microcrack level. The latter mechanisms are behind toughness and fatigue improvement. Evaluation of rubber distributionrevealeduniformdistributionandthisdecreaseasrubbercontentincreases. The results also indicated an improvement in the fatigue life for all rubber replacement levels. This was valid at all cementation levels. In terms of modulus degradability, rubberization of the cemented mixture has only a slight effect on this property while larger permanent deformation was accumulated after rubber inclusion. It was observed that the poorly cemented mixtures showed greater stiffness modulus degradation. Pavement analysis and design study showed that the decrease in the mixtures’ strength overshadowed any improvement due to both mitigation of mixtures’ stiffnesses or fatigue life enhancement. However, this is not the case for poor rubber mixtures where this mixture showed better behaviourthanthereferencemixtures. iii Dedication At the feet of my mother and my father iv Acknowledgement All thanks, glory, praise and adoration is due to God almighty, the most gracious the most merciful. O Allah you gave me the patience and strength to tackle with the hardships Ihave facedand guidedmetofinish this research. First of all I would like to express my deep thanks for my supervisors: Mr. Andrew Dawson and Dr. Nick Thom for their motivation, encouragement and guidance throughout this project. I can say that I still hear your encouragement statements which indeed were like a charger to continue in this project after many difficulties that I faced. Big thank is also due to Mr. Andrew (particularly) due to his effort in reviewing my thesis chapters. They really gave me an excellent experience. Mr. Andrew and Dr. Nick I would say I am sorry for the many virtual five minutes that I frequently took during my PhD program to discuss some issues which always becomehalf anhour. I appreciate the kind advices from Dr. Luis Neves, myinternal assessor, especiallyat thebeginningofthis project.Thanks Dr. Luis for yourkindness andencouragement. Sincere appreciation is due to the Higher Committee for Education Development in Iraq(HCED)forprovidingascholarshiptoconduct this PhDstudy. At this point, I can say that conducting such research with this type of mixture that share some properties of concrete (as cementitious material) and the others with the asphaltic mixtures (as a compacted material with relatively small stabilizer content) used in pavement structure is not an easy task. This is because this requires an understanding of both cement and asphalt concrete mixtures as well as cement- stabilized mixtures and their testing and most importantly higher level of independency in terms of sample manufacturing and testing. The independency in conducting this research was quit hard and useful at the same time. No doubt this comprehensive studyrequireddifferent tests andtools at different places. So, Iwould liketothankthefollowingpeoplewhohelpedme bydifferent means: v Mr. Nigel Rook (concrete laboratory) for his kindness by providing cement, moulds andsometechnical demonstration(at thestart ofmystudy). Balbir Loyla (structures laboratory) for helping during the development of fatigue testing machine, kind advices to start with instrumentation process and forstrain gauging. Mr. Richard Blackmore (Nottingham Transportation Engineering Centre- NTEC)forhis technical discussionanddemonstration. Mr. Jon Watson (NTEC) for his friendship, helping in X-raying some trials and scanningsomesamples andhis continuous encouragement andsupport. Mr. Steve Elesbrook (Servocone Company) for his technical advice (in spite of his extremelylimitedtime)duringmystrugglingwithcyclictestingfacility Mr.Andrew Cooper(CooperCompany)forhis cooperationanddiscussionwhen IstartedusingtheNAT machinetocharacterizemystiffmixtures. Mr. Tom Buss (senior technical manager at the Faculty of Engineering) for his technical discussionduringsometesting. Mr. Martyn Barret, Mr. Mathew Thomas and Miss. Laura (all from NTEC) for theirhelpinsamples trimming. Mr. Mark Dale (rock mechanics laboratory) for coring and testing my rock samples. Thanks must go toDr. MathewHall (theUniversityofNottingham)forprovidingme with the waste rubber and due to his discussion during my flexural program. Special thanks are also extended to Prof. Kypros Pilakoutas and Dr. Harris Angelakopoulos (both from Sheffield University) for providingme with some materials and their kind encouragement at the beginning of this project. Also, I am grateful to Dr. Martin Smith (Geospatial Institute at the University of Nottingham) and Dr. Sarhat Adam for their cooperation and involving me in scanning of myfractured surfaces samples. I must appreciate the help from Mr. Chris Fox (senior technician at Faculty of Engineering) for scanning some of samples. Special thanks to Dr. Alvaro Garcia for his friendship and support. I also appreciate the support from Dr. James Grenfell for helping in some ITS trials. Myappreciation also goes to Mrs. Kathryn Sanderson for her encouragement and support in my conference administrative work. I must give special thanks for the reviewers of my papers for providing me with a useful feedbackthat contributed toraisethequalityofthis PhDstudy. vi Thanks is also to my colleagues at the Nottingham Transportation Engineering Centre Dr. Ameer, Dr. Mahmood Al-Nasri, Dr. Chibuzor, Ahmed Nassar, Waleed, Ayad, Gustavo, Dr. Mahmoud, Rami, Bilal, Sydney, Venon, Hamed, Ahmed Ibrahim, Hasan, Abdulshafi, Yasameen, Haneen, Harith and Tariq. I am grateful to Dr.Ameerforhis helpwhen Ifirst cametotheUK. I would like also to thank Dr. Jamal A. Farhan, the Assistance Prof. at Al-Anbar University for his continuous support and encouragement during my academic and practical lives and for keepingintouchduringmyPhDstudy. Also, Iam grateful due Dr.Juma’ahAl-Sumaida’ai forhis encouragement. Now it is the time to thank my wife and my daughter: the tax payers of my success. Youreallystruggleda lot (especiallymydaughter Haya) duringmyPhDstudy. Haya I know that I was not a perfect father because of my busy time but I will be a father to be proud of. All thanks to my mother and my father for their prayers and encouragements during the whole of my life. I have also to give big thanks to my brothers and my sisters for their support during my study. Finally, I would say I am sorry for both my big and small families because I know that the three years of my studywithout anyvisit tomycountry,duetomycontinuous workinthis project,was hardandlongtimeforbothof you. vii Declaration This research described in this thesis was conducted at the Civil Engineering Department, the University of Nottingham between October 2012 and February 2016. I declare that the work is my own and has not been submitted for a degree at anotheruniversity. AhmedHilal Farhan TheUniversityofNottingham viii Table of Contents Abstract Dedication Acknowledgement Declaration Tableofcontents List offigures List oftables List ofabbreviations List ofnotations Chapter1................... Introduction …………………….……………...……… 1 1.1 Backgroundandproblem statement……………………………………..1 1.2 Aim andobjectives …………………………………...……….………...6 1.3 Noveltyofresearch…………………………………………………..….8 1.4 ResearchMethodologyandstructureofthesis …………………...……..9 1.5 Researchsignificanceandcontribution………………………....………13 1.6 Publications, Prizes andachievements...............................................…...16 1.7 References……………………………………………………….…….....18 ix
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