Characterization of Minerals, Metals, and Materials 2015

773 Pages·2016·63.526 MB·English

by  John S. Carpenter, Chenguang Bai, Juan Pablo Escobedo, Jiann-Yang Hwang, Shadia Ikhmayies B.Sc. from the physics department, Bowen Li, Jian Li, Sergio Neves Monteiro, Zhiwei Peng, Mingming Zhang (eds.)

Characterization
of Minerals, Metals,
and Materials 2015
Cover Images: Scanning electron microscopy images of voids in DC04 steel
prepared by ion slope cutting (Front) and of the fracture surface of a DC04 tensile
test specimen (Back). For further information please refer to the article entitled
‘Comparison of the Mechanisms of Void Formation by Plastic Deformation in
Single and Dual Phase BCC Steels’ by G. Gerstein, H.-B. Besserer, F. Nürnberger,
and H. J. Maier of the Leibniz Universität Hannover.
MS
144th Annual Meeting & Exhibition
March 15-19, 2015 • Wall Disney World· Orlando, Florida, USA
Characterization
of Minerals, Metals,
and Materials 2015
Proceedings of a symposium sponsored by
the Materials Characterization Committee of
the Extraction and Processing Division of
The Minerals, Metals & Materials Society (TMS)
held during
March 15-19, 2015
Walt Disney World • Orlando, Florida, USA
Edited by
John S. Carpenter
Chenguang Bai
Juan Pablo Escobedo
Jiann-Yang Hwang
Shadia Ikhmayies
Bowen Li
Jian Li
Sergio Neves Monteiro
Zhiwei Peng
Mingming Zhang
Editors
John S. Carpenter Bowen Li
Chenguang Bai JianLi
Juan Pablo Escobedo Sergio Neves Monteiro
Jiann-Yang Hwang Zhiwci Pcng
Shadia Ikhmayies Mingming Zhang

ISBN 978-3-319-48601-7 ISBN 978-3-319-48191-3 (eBook)
DOI 10.1007/978-3-319-48191-3
Chcmistry and l'vlaterials Science: Professional
Copyright © 2016 by The Minerals. Metals & Materials Society
Published by Springer International Publishers, Switzerland, 2016
Reprint of the original edition published by John Wiley & Sons, Inc., 2015, 978-1-119-08246-0
This work is subject to copyright. All rights are reserved by the Publisher, whether the whole or
part of the material is concerned, specifically the rights of translation, reprinting, reuse of
illustrations, recitation, broadcasting, reproduction on microfilms or in any other physical way,
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or by similar or dissimilar methodology now known or hereafter developed.
The use of general descriptive names, registered names, trademarks, service marks, etc. in this
publication does not imply, even in the absence of a specific statement, that such names are
exempt from the relevant protective laws and regulations and therefore free for general use.
The pnblisher, the authors and the editors are safe to assume that the advice and information in
this book are believed to be true and accurate at the date ofpublication. Neither the publisher nor
the authors or the editors give a warranty, express or implied, with respect to the material
contained herein or for any errors or omissions that may have been made.
Printed 011 acid-free paper
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TABLE OF CONTENTS
Characterization of Minerals, Metals,
and Materials 2015

Preface ................................................................................................................xv
About the Editors ............................................................................................. xvii
Session Chairs ................................................................................................... xxv
Characterization of Ferrous Metals
Study of Age Hardening Behavior in a 350 Grade Maraging Steel .....................3
L. de Carvalho, R. Plaut, M. Martorano, and A. Padilha

Characterization of Welding and Solidification
Laser Welding between TWIP Steels and Automotive High-Strength Steels ...13
P. Spena, M. Rossini, L. Cortese, P. Matteis, G. Scavino, and D. Firrao
Undercooling of Rapidly Solidified Droplets and Spray Formed
Strips of Al-Cu (Sc) ...........................................................................................21
A. Bogno, P. Natzke, S. Yin, and H. Henein
Selective Laser Melting: Characteristics of IN718 Powder and
Microstructures of Fabricated IN718 Sample ....................................................29
X. Sun, S. Liu, J. Bao, and K. Kang

Method Development in Characterization

Advanced FIB Applications in Materials Research at CanmetMATERIALS ...41
J. Li, P. Liu, R. Zhang, and J. Lo
Cyclic Hardness Test PHYBAL : A New Short-Time Procedure to
CHT
Estimate Fatigue Properties of Metallic Materials .............................................49
H. Kramer, M. Klein, and D. Eifler
Innovative Procedure for the Characterisation of Thermo-Mechanical
Properties of Carbon Base Materials Using the Gleeble® 3800 System ............57
D. Racine, D. Lukovnikov, D. Marceau, and D. Laroche
Solid Solution Characterization in Metal by Original Tomographic
Scanning Microwave Microscopy Technique ....................................................65
E. Bourillot, P. Vitry, V. Optasanu, C. Plassard, Y. Lacroute, T. Montessin,
and E. Lesniewska

v

v
Characterization of Material Processing and
Corrosion
Comparsion of the Mechanisms of Void Formation by Plastic
Deformation in Single- and Dual-Phase BCC-Steels .........................................75
G. Gerstein, H. Besserer, F. Nürnberger, and H. Maier
Characterization of Sintering Dust, Blast Furnace Dust and Carbon Steel
Electric Arc Furnace Dust ..................................................................................83
F. Chang, S. Wu, F. Zhang, H. Lu, and K. Du
Influence of Mineralogical Characteristics of Iron Ore on Formation and
Flow of Liquid Phase .........................................................................................91
B. Su, S. Wu, and G. Zhang
Effect of Pressure on the Corrosion of Materials in High Temperature Water ..99
W. Li, O. Woo, D. Guzonas, J. Li, X. Huang, R. Sanchez, and C. Bibby
The Effect of Strain Reversal during High Pressure Torsion on the
Microstructure Evolution and Texture of Aluminum Alloys ...........................107
K. Chadha, P. Bhattacharjee, and M. Jahazi

Characterization of Composites
Bending Mechanical Behavior of Polyester Matrix Reinforced with
Fique Fiber .......................................................................................................117
G. Altoé, P. Netto, M. Barcelos, A. Gomes, F. Margem, and S. Monteiro
Weibull Analysis of the Behavior on Tensile Strength of Hemp Fibers for
Different Intervals of Fiber Diameters .............................................................123
L. Rohen, F. Margem, A. Neves, M. Gomes, S. Monteiro , C. Vieira,
R. de Castro, and G. Borges
Preparation and Characterization of Natural Rubber/Organophilic
Clay Nanocomposites ......................................................................................131
M. Gonzales-Fernandes, F. Esper, M. Silva-Valenzuela, G. Martín-Cortés,
F. Valenzuela-Diaz, and H. Wiebeck
Tensile Properties of Epoxy Composites Reinforced with Continuous
PALF Fibers ....................................................................................................139
G. Glória, G. Altoé, Y. Moraes, R. Loyola, F. Margem , andS. Monteiro
vi

vi
Replacement of Carbon Black on Natural Rubber Composites and
Nanocomposites – Part 1 .................................................................................145
G. Martín-Cortés, F. Esper, A. de Araujo, W. Hennies, M. Valenzuela,
and F. Valenzuela-Díaz
Flexural Mechanical Characterization of Epoxy Composites
Reinforced with Continuous Banana Fibers ....................................................153
F.de Assis, P. Netto, F. Margem, R. Loiola, and S. Monteiro
Influence of the Nanoclay Cloisite 20A Incorporation on Properties of
Acrylonitrile Butadiene Styrene (ABS) ...........................................................159
J. Sales, A. Silva, F. Valenzuela-Diaz, and E. Moura
Characterization of Non-Ferrous Metals
Characterization of Closed-Cell Aluminium Foams Subjected to
Compressive Loading ......................................................................................167
M. Islam, J. Escobedo, P. Hazell, G. Appleby-Thomas, and M. Quadir
Characterization of Materials Extraction
Improvement on Performance of Mg-C Refractories as Lining of
Vanadium-Extraction Converters ....................................................................177
W. Huang, L. Xu, S. Zhang , and M. Chen
Analysis on Deep Treatment Effect of Coking Wastewater Using 3D
Electrode Combined with Fenton Reagent ......................................................185
L. Zhang, L. Wang, P. Liu, B. Fu, J. Hwang, and S. Chen
Characterization of Steelmaking Desulfurization Slag ....................................193
M. Bogala, M. Zhang, and R. Reddy
Development and Characterization of Nanomaterials for Zinc
Vapor Capture ..................................................................................................201
P. Korinko and S. Murph
Separation of Roasted Coating and Core in Double-Layered Pellet Roasting
for Pretreatment of Sulfur and Arsenic-Bearing Gold Concentrate .................209
T. Jiang, X. Li, Y. Yang, Q. Li, and J. Ge
Prediction for the Surface Tension of FeO-TiO(cid:909)-Ti(cid:909)O(cid:910)-X(SiO(cid:909),CaO, MgO)
Slag Systems ....................................................................................................217
Y. Liu, X. Lv, and C. Bai
vii

vii
Characterization of Soft Materials
Constitutive Modeling of a Glass Fiber-Reinforced PTFE Gasketed-Joint
Under a Re-Torque ..........................................................................................227
J. Williams and A. Gordon
Microwave Absorption Characteristics of Tire ................................................235
Y. Zhang, J. Hwang, Z. Peng, M. Andriese, B. Li, X. Huang, and X. Wang
Optical Evaluation for Biomimetic Microlens Array on PDMS Sheet ............245
K. Monden
Behavior of Linear Low Density Polyethylene Films Under UV Ageing for
Agricultural Application ..................................................................................253
P. Poveda, H. Viana, and L. Silva
Photoacoustic Thermal Characterization of Malva Fibers ...............................259
J. Margem, V. Gomes, R. Faria, F. Margem, T. Cordeiro, M. Margem,
and S. Monteiro
Mechanical, Morphological and Thermal Properties of Açaí Fibers
Reinforced Biodegradable Polymer Composites .............................................265
C. Wataya, R. Lima, R. Oliveira, and E. Moura
Influence of Clay Exfoliation on the Properties of EVOH/Clay Flexible
Films ................................................................................................................273
M. Machado, R. Godoy, A. Silva, R. Lima, R. Oliveira, F. Valenzuela-Díaz,
and E. Moura
Characterization of Minerals
Chemical Resistance of Ornamental Compound Stone Produced with
Marble Waste and Unsaturated Polyester ........................................................283
C. Ribeiro, R. Rodriguez, and C. Vieira
Characterization of Feldspar by Instrumental Analytical Techniques .............291
Z. Aliyu, A. Garkida, E. Ali, and M. Dauda
Microwave Power Absorption Characteristics of Iron Oxides ........................299
Z. Peng, J. Hwang, M. Andriese, Y. Zhang, G. Li, and T. Jiang
viii

viii
Qualitative and Mineralogical Characterization of Lead Deposit in Ishiagu,
Ebonyi State, Nigeria .......................................................................................307
G. Onyedika, K. Onwukamike, C. Onyenehide, and M. Ogwuegbu
Sintering Characteristics of Iron Ores with Addition of Laterite Nickel
Ores ..................................................................................................................317
X. Li, J. Zhang, C. Yao, Y. Zhang, Z. Shi, and F. Wang
Characterization of Clays and Ceramics
Alumina Superfines Based Geopolymeres: Developments and
Characterization ...............................................................................................327
N. Nagem, M. Costa, V. Silva, A. Henriques, A. Mansur, A. Peres,
and H. Mansur
Densification and Mechanical Properties of Reaction Sintered
Al(cid:909)O(cid:910)-MgO-CaO Refractory ...........................................................................337
L. Xu, L. Jin, X. Yin, and M. Chen
Influence of Sintering Temperature on Microstructure and Properties of
Magnesia Partially Stabilized Zirconia Ceramics ............................................345
L. Jiang, S. Guo, Y. Liu, Y. Bian, S. Chen, X. Zhang, G. Yang, and W. Ding
Evaluation of Structural Clay Brick Masonry Units by Weibull
Analysis and Brazilian Code and Specifications .............................................353
N. Azeredo, J. Alexandre, A. Azevedo, C. Xavier, S. Monteiro, E. Zanelato,
and R. Oliveira
Brazilian Bentonite Submitted to Mild Acid Treatment Under
Moderated Conditions ......................................................................................361
C. Andrade, V. Justo, D. Fermino, M. Valenzuela, C. Volzone,
and F. Valenzuela-Diaz
Increase of Flexural Strength of Red Ceramic Pieces Incorporated with
Ornamental Rock Waste: Application of Weibull Statistic for Determination
of Best Firing Temperature ..............................................................................369
C. Piazzarollo, G. Xavier, J. Alexandre, A. Azevedo, and S. Monteiro
ix

ix