ES0000075 empresa national de residuos radiactivos, s.a. CATSIUS CLAY PROJECT CALCULATION AND TESTING OF BEHAVIOUR OF UNSATURATED CLAY AS BARRIER IN RADIOACTIVE WASTE REPOSITORIES STAGE 2: VALIDATION EXERCISES AT LABORATORY SCALE 7 PUBLICACION TECNICA NUM. 11/99 CATSIUS CLAY PROJECT CALCULATION AND TESTING OF BEHAVIOUR OF UNSATURATED CLAY AS BARRIER IN RADIOACTIVE WASTE REPOSITORIES STAGE 2: VALIDATION EXERCISES AT LABORATORY SCALE Compiled by E.E. Alonso and J. Alcoverro International Centre for Numerical Methods in Engineering (CIMNE, ES) Participating organisations: ANDRA (ER), ClAYT. (SE), ISMES (IT), SCK-CEN (BE), UPC (ES), ULg (BE), UWCC (GB) The CAJSIUS CLAY Project was performed under contract EI4WCJ950003 with the European Commission in the framework of its programme on Nuclear Eission Safety (1994-1998) m CATSIUS CLAY PROJECT CALCULATION AND TESTING OF BEHAVIOUR OF UNSATURATED CLAY AS BARRIER IN RADIOACTIVE WASTE REPOSITORIES STAGE 2: VALIDATION EXERCISES AT LABORATORY SCALE This report has been drawn up on behalf of ENRESA. It represents the opinion of the contractor wich need not necessarily coincide with that of ENRESA in every respect. Index RESUMEN 1 ABSTRACT 5 1. THE CATSIUS CLAY PROJECT 9 7.1 Objectives and scope 77 1.2 Project coordination and partners involved 77 7.5 Work programme 77 2. INTRODUCTION TO STAGE 2 OF THE CATSIUS CLAY PROJECT 13 3. BENCHMARK 2.1 "OEDOMETER SUCTION CONTROLLED TESTS ON SAMPLES OF COMPACTED BOOM CLAY" 17 3.1 Part A: "Volumetric deformations upon wetting-drying cycles". 19 3.1.1 Case definition 19 3.1.1.1 Introduction 19 3.1.1.2 Jest description 21 3.1.1.3 Required results 21 3.1.1.4 Finalremarks 21 3.1.2 Results 23 3.1.2.1 AHO (CLEO) 23 3.1.2.1.1 Mel description 23 3.1.2.1.2 Determination of model parameters 28 3.1.2.1.3 Computed results 28 3.1.2.2 CIA (ABAQUS) 31 3.1.2.2.1 Model description 37 3.1.2.2.2 determination of model parameters 32 3.1.2.2.3 Computed results 32 3.1.2.3 ISM (ABAQUS) 32 3.1.2.3.1 Model description 32 CATS IU S CLAY Project. Stage 2: Validation exercises at laboratory scale 3.1.2.3.2 Determination of model parameters 35 3.1.2.3.3 Computed results 35 3.1.2.4 UPC (CODE BRI6HI) 39 3.1.2.4.1 Model description 39 3.1.2.4.2 Determination of model parameters 40 3.1.2.4.3 Computed results 41 3.1.2.5 UOL (IAGAMINE) 41 3.1.2.5.1 Model description 41 3.1.2.5.2 Determination of model parameters 46 3.1.2.5.3 Computed results 49 3.1.2.6 UWC (COMPASS) 52 3.1.2.6.1 Model definition 52 3.1.2.6.2 Determination of model parameters 53 3.1.2.6.3 Computed results 54 3.1.3 Discussion 58 3.2 PartB: "Swellingpressure test" 65 3.2.1 Case definition 65 3.2.1.1 Introduction 65 3.2.1.2 Jest description 66 3.2.1.2.1 Sample preparation 66 3.2.1.2.2 Jest description 68 3.2.1.3 Required results 68 3.2.2 Results 72 3.2.2.1 AND (CLEO) 72 3.2.2.2 CIA (ABAQUS) 73 3.2.2.3 ISM (ABAQUS) 73 3.2.2.4 UPC (CODEBRIGHJ) 73 3.2.2.5 UOL (IAGAMIHE) 74 3.2.2.6 UWC (COMPASS) 76 3.2.3 Discussion 76 4. BENCHMARK 2.2 "SMALL SCALE WETTING-HEATING TEST ON COMPACTED BENTONITE" 79 4.1 Case definition 81 4.1.1 Introduction 81 4.1.2 Jest description 81 4.1.2.1 The thermohydraulic cell 81 Index 4.1.2.2 Sample preparation : 81 4.1.2.3 Jest description 81 4.1.3 Data obtained during and after the experience 82 4.1.3.1 Data obtained during the experience 82 4.1.3.2 Data obtained after the experience 82 4.1.4 Characteristics of the s2 bentonite 83 4.1.4.1 Waterflow 83 4.1.4.2 Heat transport 83 4.1.4.3 Mechanical properties 83 4.1.5 Required results 84 4.2 Results 84 4.2.1 AND (CLEO) 86 4.2.1.1 Model description 86 4.2.1.2 Determination of model parameters 87 4.2.1.3 Computed results 87 4.2.2 CIA (ABAQUS) 88 4.2.2.1 Model description 88 4.2.2.2 Determination of model parameters 90 4.2.2.3 Computed results 94 4.2.3 ISM (ABAQUS) 94 4.2.3.1 Model description 94 4.2.3.2 Determination of model parameters 95 4.2.3.3 Computed results 98 4.2.4 UPC (CODE BRIGHT) 98 4.2.4.1 Model description 98 4.2.4.2 Determination of model parameters 101 4.2.4.3 Computed results 707 4.2.5 ML (IAGAMINE) 104 4.2.5.1 Model description 104 4.2.5.2 Determination of model parameters 108 4.2.5.3 Computed results 7/3 4.2.6 UWC (COMPASS) 114 4.2.6.1 Model description 114 4.2.6.2 Determination of model parameters 119 4.2.6.3 Computed results 120 4.3 Discussion 139 V CATS!US CLAY Project. Stage 2: Validation exercises at laboratory scale 5. CONCLUSIONS 143 6. REFERENCES 147 APPENDIX 1. FIGURES AND TABLES FOR BENCHMARK 2.1 151 All Suction Controlled Jests Under Constant Vertical Stress 153 A1.2 Retention Curves For Boom Clay (Wetting-drying paths) 157 A1.3 Net stress path during sample preparation for the blind swelling pressure test 159 A1.4 Assembly used to perform the blind swelling pressure test 161 APPENDIX 2. FIGURES AND TABLES FOR BENCHMARK 2.2 163 A2.1 Scheme of the thermohydraulic cell (CIEMAJ) 165 A2.2 Water intake during the experience (CIEMAJ) 166 A2.3 Pressure evolution during the experience (CIEMAJ) 167 A2.4 Temperatures measured during the experience (CIEMAJ) 168 A2.5 Final physical properties of the clay (CIEMAJ) 169 A2.6 Hydraulic saturated conductivity (CIEMAJ) 170 A2.7 Water retention curves (CIEMAJ) 171 A2.8 Water retention curves (UPC) 175 A2.9 Thermal conductivity (CIEMAJ) 178 A2.10 Thermal expansion (UPC) 179 A2.11 Suction controlled oedometric tests (CIEMAJ) 180 APPENDIX 3. DESCRIPTION OF THE PROGRAMS USED BY PARTNERS 189 A3.1 CLEO(ANO) 191 A3.2 ABAQUS (CIA, ISM) 191 A3.3 CODE BRIGHT (UK) 192 A3.4 IA6AMINE (UOU 193 A3.5 COMPASS (UWO 193 VI Index INDEX OF FIGURES Figure 3-1 a) Sample before testing b) Wetted sample 19 Figure 3-2 Microphotographs of Compacted Boom clay. 20 Figure 3-3 Jesting pah for sample of Benchmark 2.1. Dots indicate suction values actually applied to samples 22 Figure 3-4 Results of oedometer suction controlled tests on samples of compacted Boom Clay 22 Figure 3-5 Activation of the yield surfaces for a higblyoverconsolidated material 26 Figure 3-6 Activation of the yield surfaces for a normally consolidated material 27 Figure 3-7 Activation of the yield surface for a slightly overconsolidated material 28 Figure 3-8 Oedometer Suction Controlled Jests on Samples of Compacted Boom Cloy. Case A 29 Figure 3-9 Oedometer Suction Controlled Jests on Samples of Compacted Boom Clay. CaseB 29 Figure 3-10 Oedometer Suction Controlled Jests on Samples of Compacted Boom Clay. CaseC 30 Figure 3-11 Oedometer Suction Controlled Jests on Samples of Compacted Boom Clay. Cased 30 Figure 3-12 Oedometer Suction Controlled Jests on Samples of Compacted Boom Clay. Cose E 31 Figure 3-13 Oedometer Suction Controlled Jests on Samples of Compacted Boom Clay. Case A 32 Figure 3-14 Oedometer Suction Controlled Jests on Samples of Compacted Boom Clay. Case B 33 Figure 3-15 Oedometer Suction Controlled Jests on Samples of Compacted Boom Clay. Cose C 33 Figure 3-16 Oedometer Suction Controlled Jests on Samples of Compacted Boom Clay. Case D 34 Figure 3-17 Oedometer Suction Controlled Jests on Samples of Compacted Boom Clay. Cose E 34 Figure 3-18 Oedometer Suction Controlled Jests on Samples of Compacted Boom Clay. Case A 36 Figure 3-19 Oedometer Suction Controlled Jests on Samples of Compacted Boom Clay. Case B 37 Figure 3-20 Oedometer Suction Controlled Jests on Samples of Compacted Boom Clay. Case C 37 Figure 3-21 Oedometer Suction Controlled Jests on Samples of Compacted Boom Clay. Case D 38 Figure 3-22 Oedometer Suction Controlled Jests on Samples of Compacted Boom Clay. CaseE 38 Figure 3-23 Oedometer Suction Controlled Jests on Samples of Compacted Boom Clay. Case A 42 Figure 3-24 Oedometer Suction Controlled Jests on Samples of Compacted Boom Clay. CaseB 42 Figure 3-25 Oedometer Suction Controlled Jests on Samples of Compacted Boom Clay. Case C 43 Figure 3-26 Oedometer Suction Controlled Jests on Samples of Compacted Boom Clay. Case D 43 Figure 3-27 Oedometer Suction Controlled Jests on Samples of Compacted Boom Clay. Case E 44 Figure 3-28 Calibration of the elastic index upon suction os a function of the net mean stress 47 Figure 3-29 Oedometer Suction Controlled Jests on Samples of Compacted Boom Clay. Case A 49 Figure 3-30 Oedometer Suction Controlled Jests on Samples of Compacted Boom Clay. Case B 50 Figure 3-31 Oedometer Suction Controlled Jests on Samples of Compacted Boom Cloy. Case C 50 Figure 3-32 Oedometer Suction Controlled Jests on Samples of Compacted Boom Clay. Cased 5/ Figure 3-33 Oedometer Suction Controlled Jests on Samples of Compacted Boom Clay. CaseE 5/ CATSIUS CLAY Project. Stage 2: Validation exercises at laboratory scale Figure 3-34 Oedometer Suction Controlled Jests on Samples ofCompacted Boom Clay. Case A 55 Figure 3-35 Oedometer Suction Controlled Tests on Samples of Compacted Boom Clay. Case B 56 Figure 3-36 Oedometer Suction Controlled Tests on Samples of Compacted Boom Clay. CaseC 56 Figure 3-37 Oedometer Suction Controlled Tests on Samples of Compacted Boom Clay. Case D 57 Figure 3-38 Oedometer Suction Controlled Tests on Samples of Compacted Boom Clay. Case F 57 Figure 3-39 Oedometer Suction Controlled Tests on Samples of Compacted Boom Clay. Case A 62 Figure 3-40 Oedometer Suction Controlled Tests on Samples of Compacted Boom Clay. Case B 62 Figure 3-41 Oedometer Suction Controlled Tests on Samples of Compacted Boom Clay. Case C 63 Figure 3-42 Oedometer Suction Controlled Tests on Samples of Compacted Boom Clay. Case D 63 Figure 3-43 Oedometer Suction Controlled Tests on Samples of Compacted Boom Clay. Case F 64 Figure 3-44 LC curves plotted in the In (p) - In (s) space 64 Figure 3-45 LC curves plotted in the p - In (s) space 65 Figure 3-46 Swelling pressure (qualitative) plotted in the (a - Pa, s) plane. Also indicated are the wetting drying paths at constant vertical v stress considered in Benchmark 2.1, Part A 66 Figure 3-47 Water retention curves for compacted Boom Clay powder at y</ = 13.7 kN/m 67 Figure 3-48 Vertical and horizontal stresses measured during the swelling pressure test 67 Figure 3-49 Suction controlled oedometer cell 69 Figure 3-50 Suction controlled oedometric cell. Whole setup 70 Figure3-51 Results ofswelling pressure test for benchmark 2.1, Part B 71 Figure 3-52 Results of an additional swelling pressure test carried out in Boom clay powder in connection with Benchmark 2.1, Part B 71 Figure 3-53 Blind Suction Controlled Swelling Pressure Test on a Sample of Compacted Boom Clay 72 Figure 3-54 Blind Suction Controlled Swelling Pressure Test on a Sample of Compacted Boom Clay 73 Figure 3-55 Blind Suction Controlled Swelling Pressure Test on a Sample of Compacted Boom Clay 74 Figure 3-56 Blind Suction Controlled Swelling Pressure Test on a Sample of Compacted Boom Clay 75 Figure 3-57 Blind Suction Controlled Swelling Pressure Test on a Sample of Compacted Boom Clay (first calibration) 75 Figure 3-58 Blind Suction Controlled Swelling Pressure Test on a Sample of Compacted Boom Clay (second calibration) 76 Figure 3-59 Blind Suction Controlled Swelling Pressure Test on a Sample of Compacted Boom Clay 77 Figure 4-1 Swelling volumetric strain as a function of the degree of saturation 96 Figure 4-2 Retention curve considered in the analysis 102 Figure 4-3 Saturated hydraulic conductivity considered in the analysis 102 Figure 4-4 Comparison between measured thermal conductivity and thermal conductivity computed by geometric mean for various degrees of saturation 703 Figure 4-5 Comparison between experimental and backanalised results of swelling tests 703 Figure 4-6 Thermal expansion coefficient consiedered in the analysis 705 Figure4-7 Elastic stiffness parameter for changes in net mean stresses in function of suction 70? Figure 4-8 Plastic stiffness parameters for changes in net mean stresses in function of suction 110
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