Analytical Instrumentation: Practical Guides for Measurement and Control

748 Pages·1996·59.58 MB·English

by  R. E. Sherman

Analytical
Instrumentation

R. E. Sherman, Editor
L. Rhodes, Associate Editor
Analytical
Instrumentation

R. E. Sherman, Editor
L. Rhodes, Associate Editor

Practical Guides
for Measurement and Control
cepyran 1996, lnaumen: Society at America
sib served

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a
Table of Contents

ABOUT THIS SERIES ¥

(GALL FOR PARTICIPATION YU

PREFACE X¥11 i
ABOUT THE EDITORS 0%

CONTRIBUTOR X11 -
INTRODUGTION XXIN

Part)” IMPLEMENTATION OF
PROGESS ANALYZER SYSTEMS 1

Chapter TYPICAL PROCESS ANALYZER
APPLICATION JUSTIFICATIONS 3
Coppliace wh Gorerautent Repsations, 9
Stee Constiratoms 6
Boone intent 8
eeu Regusemes 1,
Hier Gay eutng
Ralsenes, "

Chapter2 INTERFACING WITH PROCESS ANALYZER SYSTEMS 33
[Commvaiesion Tecrigues, 34
Sbplomentop Anas Commtnicaon, 48
Tab Use of Aowiyet Servos, 32

CChaptor’ PROCESS SAMPLE CONDITIONING SYSTEMS 59
Process Chnzaterulcs. 39
Soa Cheraretcs. 6L
Sinole Inaster nets
Ente yes a Futon, TE

Suuple Ceters. 7
Sindee Reto 65

Sendazsnte Eaforn Protection, 86
Sipe eps, Heer aed, 9
‘Edgple Coadidonng 4 Sym, 97
Referee, 10

Chapter 4 PRINCIPLES OF PROGESS:
ANALYZER CALIBRATION 103

Refueoses, 112 a
Table of Contents

Chaptor5 SPC/SGCFOA PROCESS ANALYZER SYSTEMS 135
General Panciptes, 115
Bese eaiscn Tid

Seeeaceas
Applicaton g Pinca Andie, 14

Chapter6 VALIDATION OF PROCESS ANALYZERS 161
Veli Paseens, 16
eee Reuben, 162
Rebnnitgnent, 169
Reeronse

Chapter? SPECIFICATION AND PURCHASE
(OF PROCESS ANALYZER SYSTEMS 171
‘Use of Spetfiation and Data Steet, 171
Staple Shrcine Verses Ope Bidding Techniques, 181
ey Resumen eae SA

er Concept Yesus tidal Analyze

Rooeepent, 18)
pie Solace Speccutions, 12

Ghapler@ PROCESS ANALYZER SYSTEM
TRAINING CONSIDERATIONS 163
{opsfving Analyser Personae Repcnen, 182
SGiRane avs of Aba Haase
een Socrss or payzer ican, 167
‘Thang Programs, 18

Ghoptor3 PROCESS ANALYZER SYSTEM MAINTENANCE:
PERSONNEL AND CHGANIZATIONAL ISSUES 191
Peronnel sss, 192
Grpeurtona sces, 201
Relrvaces, He

Perttt PROCESS ANALYZER APPLICATION
FUNDAMENTALS 217
‘pie Menssremene Principle, 217

PHYSICAL PROPERTY PROCESS ANALYZER SYSTEMS 219

Sie Soe Fon AULD a
pee
sere,

Eemiatee fio. 2
Bikey ee
fino Sion Reyemgay, 250
vad calrn Reguimat, 2
fetbooung and Maucnsres, 29

Chapt 1 e200 PONT AKO FOUR OWT AKALYZENS 244
Soreren ange Se
oc
Sareea
Seats

w eplag denne a8

Seager
‘Table of Contents

Chapter 12

(Chapter 15

Chapter 14

Chapter 15

Chapter 16

(Chapter 17

FLASH POINT ANALYZERS 251
Gocne races Ananzery, 252
Srnec Applicezene. 259.
Rang of Wapbles, 260
Spits an Aeeesceies, 260,
Clniatine, 260
frsalisign Hine, 260
the eaeryWeaes, 260
regu Saumpiog Sepia Requiemenss, 260
‘ype Culbrces Regirenmas, 200
‘PBablekaoestg and Maeeance, 261

FREEZE POINT ANALYZERS 243
Betsey amy 3

roe eae

Hepat Walon 20

ence See

Prat te, 206

eae 2 es

i Satglat Sc boqranene, .
Fd Saas von amen

ienLSurea aes

REFRACTIVE INDEX ANALYZERS 260
pseu pte ner Reto
Vegan Catone, 271

Heated Ayan, 379

isigrae ae

‘THERUAL CONDUCTIVITY ANALYZERS. 268
Messner cepts, 253

Tracey 84

‘Avsivear estrone, 285

‘Siprel Replies, 297

MScecen,

rouble, 208

COMBUSTIBLE GAS ANALYZERS 291
eserent Prog, 292
Gomer Appreicny 250
Sagoo tienen BP
Unt, 9
Jewel ine, 300
Ske ae 20 sco
Figue Sm Stirs Reqiemens, 5
wpa Callraota Repuwens 301
rbeshootae sod Seancoanee, 35
Referees ‘9
Blige, 907

ViscosiTY ANALYZERS (NON-ASTM) 309

Ce es ee paene.

‘Tootleootng ead Qfamsenenes, 321
‘ibogayey, 2
Table of Contents

Chapter 18

Chapter 19

Chapter 20

Chapter 21

Chapter 22

Chapter 23

MOISTURE/DEW POINT ANALYZERS 225
Meccuenee Pincgle, 325

Dio Points roe Bit Carvers, 327
(ese ewig. 8

Ter Comsteaatogs For Making Moietare
omen Guts Udi oR 3,354
oping System Desig

Nortel Co Am
ise Orsnni Tigaide [REF O35
elernese, 3H

HYPROGEN SULFIDE ANALYZERS 243

eetncaan
Bibogeply. 352

TOTAL SULFUR ANALYZERS 259
Bit Anahi Syria, 300,
is, 3

Stegdard Moat ant Certicetioné, 35
Bibbopaply. Sat

‘OCTANE AND CETANE ANALYZERS 967

= Lbrangey Tea Mets, 368

(Gears Ritlyary 363

Ganson Aerfctons of Octane Anazers, 384
Ranger of Vepuhles, Mit

Spt tnt evcces 384

Elastane, 380

Fenalistign Hints, 4

Siete Thea 3 see

yet ras Reverenres 368

(blesioting and Mactcaanes, SSF

YAPOR PRESSURE ANALYZERS a7
Geto ren Ama, 38
Rapes of Miata, 303
Spencer 398
ee

Specie Sy Wace 305

rs Snag een 30

‘PERiasovg see Means, 3

\VAPOR-TO-LIQWD RATIO (VfL) ANALYZERS 401
Terese Anlyzer
Gintnon fo hetiong, 403
Ranges of Wahlen, 408
pts: and Acresiies, 403
tons, aos
Tesaliie tins, 408
St a
yp crates Reuueotens
Yubleshoonag and Mamtoanoe, 273

x
‘Table of Contents

ELECTROCHEMICAL PROCESS ANALYZER SYSTEMS 407

chapter 2a

haptor 25,

Chapter 26

Chapter 27

eseumr ANALG «>
Theta Copan 118

HERE amg. on
‘alti nd aga, ok *
‘etionees a8

manaLraee oo
case
TEA <2
Acaoinledeieats, $86

denier

ob (REDOX) ANALYZERS 457
Seaodbnen Shes a
teary cana
Spats ae
Se aoe as, 6
Sepa cence tg
pre arm aera 2
cone
eboeen

‘HACE OXYGEN ANALYZERS 469
Frosple Operation, 185,
‘Ropieaions, 28

mg. an
é er
ete, 32

SPECTROPHOTOMETRIC PROCESS ANALYZER SYSTEMS 485

Chapter 2a

INFRARED QF AND NOW)
ABSORPTION ANALYZERS 497
‘Mestacren’ Principe, 497
eomoa Aprheiony” $05

anges of Cable 300

Borie and Asgrsincs, 508
Elniens, 38

Inulin Hoes, $09

Spee Bian 8
Pru Sampliog Sper Requiem

equirenas, 508
Type eaenon Keene
eatrbootig ond Susoisanse, 10
Eefovmt 3h

Bpoirerenbye B11