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ADVANCES IN POWDER AND CERAMIC MATERIALS SCIENCE 2023 EDITED BY Bowen Li Dipankar Ghosh Eugene A. Olevsky Kathy Lu Faqin Dong Jinhong Li Ruigang Wang Alexander D. Dupuy Elisa Torresani The Minerals, Metals & Materials Series · · · Bowen Li Dipankar Ghosh Eugene A. Olevsky · · · Kathy Lu Faqin Dong Jinhong Li · · Ruigang Wang Alexander D. Dupuy Elisa Torresani Editors Advances in Powder and Ceramic Materials Science 2023 Editors BowenLi DipankarGhosh MichiganTechnologicalUniversity OldDominionUniversity Houghton,MI,USA Norfolk,VA,USA EugeneA.Olevsky KathyLu SanDiegoStateUniversity VirginiaPolytechnicInstituteandState SanDiego,CA,USA University Blacksburg,VA,USA FaqinDong SouthwestUniversityofScience JinhongLi andTechnology ChinaUniversityofGeosciences Mianyang,China Beijing,China RuigangWang AlexanderD.Dupuy TheUniversityofAlabama UniversityofCalifornia,Irvine Tuscaloosa,AL,USA Irvine,CA,USA ElisaTorresani SanDiegoStateUniversity SanDiego,CA,USA ISSN 2367-1181 ISSN 2367-1696 (electronic) TheMinerals,Metals&MaterialsSeries ISBN 978-3-031-22621-2 ISBN 978-3-031-22622-9 (eBook) https://doi.org/10.1007/978-3-031-22622-9 ©TheMinerals,Metals&MaterialsSociety2023 Thisworkissubjecttocopyright.AllrightsaresolelyandexclusivelylicensedbythePublisher,whether thewholeorpartofthematerialisconcerned,specificallytherightsoftranslation,reprinting,reuse ofillustrations,recitation,broadcasting,reproductiononmicrofilmsorinanyotherphysicalway,and transmissionorinformationstorageandretrieval,electronicadaptation,computersoftware,orbysimilar ordissimilarmethodologynowknownorhereafterdeveloped. Theuseofgeneraldescriptivenames,registerednames,trademarks,servicemarks,etc.inthispublication doesnotimply,evenintheabsenceofaspecificstatement,thatsuchnamesareexemptfromtherelevant protectivelawsandregulationsandthereforefreeforgeneraluse. Thepublisher,theauthors,andtheeditorsaresafetoassumethattheadviceandinformationinthisbook arebelievedtobetrueandaccurateatthedateofpublication.Neitherthepublishernortheauthorsor theeditorsgiveawarranty,expressedorimplied,withrespecttothematerialcontainedhereinorforany errorsoromissionsthatmayhavebeenmade.Thepublisherremainsneutralwithregardtojurisdictional claimsinpublishedmapsandinstitutionalaffiliations. Coverillustration:FromChapter“FabricationofUltra-LightweightandHighlyPorousAluminaScaffolds byaNovelSol–Gel/FreezeCastingHybridMethod”,Pei-ChiehHoetal.,Figure3:SEMmicrographs ofaluminascaffoldsinaintransversesectionwith10vol%solidcontentbinlongitudinalplanewith 10vol%solidcontentcsmoothlamellaesurfaceofaluminascaffoldswithnanoscaleporeswith10vol% solidcontentdtransversesectionwith5vol%solidcontentelongitudinalplanewith5vol%solidcontent fdiscontinuouslamellaesurfaceofaluminascaffoldswith10vol%solidcontent.https://doi.org/10.1007/ 978-3-031-22622-9_4. ThisSpringerimprintispublishedbytheregisteredcompanySpringerNatureSwitzerlandAG Theregisteredcompanyaddressis:Gewerbestrasse11,6330Cham,Switzerland Preface Ceramic materials science covers the science and technology of creating objects frominorganic,non-metallicmaterials,andincludesdesign,synthesis,andfabrica- tionofceramics,glasses,advancedconcretes,andceramic-metalcomposites.Powder metallurgyandceramicsalwayssharesimilartechnicalprincipalsandmethodologies instudyingprocessesandstructuresofdiversematerialsfrompowderpreparation, forming, sintering, until product finishing. In recent years, the hybrids of ceramic materials and metallic materials have received plenty of interdisciplinary inspira- tionsandachievementsinmaterialprocessesandfunctionalapplicationsincluding ionicbatteries,catalysis,energystorage,superconductors,semiconductor,filtrations, additivemanufacturing,etc. Topromoteinterdisciplinarystudies,TheMinerals,Metals&MaterialsSociety (TMS)MaterialsCharacterizationCommitteeandPowderMaterialsCommitteehave co-sponsoredasymposium“AdvancesinPowderandCeramicMaterialsScience” duringtheTMSAnnualMeetingannuallysince2020.Thissymposiumisfocused ontheadvancesofpowderandceramicmaterialsinthefundamentalresearch,tech- nology development, and industrial applications. The subjects of the symposium includesynthesis,characterization,modeling,andsimulationofpowderandceramic materials; design and control of ceramic microstructure and properties; ceramic powders and processing; surface treatment and thin films, membranes, and coat- ings of ceramics; hybrid systems of ceramic, metal, and/or polymer composites; andmetallurgicalbyproductsforceramicmanufacturing.Aspecialtopicof“high- entropyceramics”hasbeenaddedtothe2023symposiumduetothesuperiorprop- ertiesofhigh-entropyceramicswithnovelconceptsthathaveattractedresearchers to explore various potential structural and functional applications, while a number ofmaterialsarebeingre-acquaintedanddeveloped. Thisvolumeofproceedingsincludes16reviewedmanuscriptsoforiginalresearch fromthesymposia“AdvancesinPowderandCeramicMaterialScience”and“Powder MaterialsProcessingandFundamentalUnderstanding”(SponsoredbyTMSMate- rials Processing & Manufacturing Division Powder Materials Committee). The manuscriptswereinvitedorcontributedbytheresearchersfromthefieldsofpowder processing,materialsscience,engineering,metallurgy,physics,manufacturing,and v vi Preface applications. This book provides authors’ up-to-date achievements in powder and ceramicmaterials.Itwouldbeausefulreferenceforacademicandindustryreaders. Theeditorsofthisbookwouldliketothanktheauthorsfortheircontributionof manuscripts,theTMSMaterialsCharacterizationCommitteeandPowderMaterials Committee for their support, and the TMS Program Committee and Springer for publishingthisstand-alonevolume. BowenLi LeadOrganizer Contents PartI AdvancesinPowderandCeramicMaterialsScience DesignofHigh-EntropyCeramicswithIGZO-BasedCompounds forElectroceramicsApplications .................................... 3 ZaidAlejandroLuzanillaMeléndrez, AlejandroDurán, FranciscoBrown, OfeliaHernándezNegrete, JavierHernándezParedes,andVictorEmmanuelAlvarezMontano DevelopmentofHighVoltageMultilayerCeramicCapacitor .......... 11 HyungsukK.D.Kim DevelopmentofanExperimentallyDerivedModelforMolybdenum Carbide(Mo C)SynthesisinaFluidized-BedReactor ................ 17 2 MaureenP.Chorney,JeromeP.Downey,andK.V.Sudhakar FabricationofUltra-LightweightandHighlyPorousAlumina ScaffoldsbyaNovelSol–Gel/FreezeCastingHybridMethod .......... 27 Pei-ChiehHo,Haw-KaiChang,andPo-YuChen EffectofThree-DimensionallyConnectedPorousHydroxyapatite CeramicsonEnhancingHeatStorageofLithiumNitratePhase TransformationMaterials .......................................... 39 RuifanZhou,ShuangSong,JinhongLi,LuJiang,andYixiuXin WaterGradationsStoichiometricallyResolveCuprous-Chloride TetrahedralStampsinaHydrochloric-AcidSmelter .................. 51 Kai-WeiLiuandJia-LinHsu Phase Equilibria of SiO -Ce O -CaO-25wt.% Al O System 2 2 3 2 3 at1773K ......................................................... 63 RenshengLi,MengchuanLi,TongshengZhang,andWanlinWang Printed Carbon Nanotube and Graphene Heaters for Drying Ceramics ......................................................... 77 ZiyadSherif,JohnPatsavellas,andKonstantinosSalonitis vii viii Contents EnhancingReinforcingEfficiencyofSiCParticlesinAluminum MatrixCompositeswithIntercalatedOxygenAtoms .................. 89 M.R.JooandD.H.Bae Weathering Resistance of Post-consumer Glass and Sawdust ReinforcedPolyesterComposites .................................... 99 KatorJeffJomboh, MohammedKabirYakubu, WilsonUzochukwuEze, AdeleDzikwiGarkida, andEmmanuelMajiyeboAlemaka PreparationofFeMnAlSiCPowderbyCO -SteelSlagCooperative 2 ElectroDeoxidation ................................................ 109 ZhenweiJing, XiaofeiXing, JuMeng, HongyanYan, HuiLi, andJinglongLiang ThermodynamicAnalysisofBNPreparedbyElectrodeposition BNPower ......................................................... 119 JuMeng, ChaoLuo, ZhenweiJing, HongyanYan, HuiLi, andJinglongLiang UseofCeramicWasteinDifferentPercentagesasaReplacement oftheFineAggregateinMortars .................................... 131 M.G.P.Cherene,G.C.Xavier,A.R.G.Azevedo,andS.N.Monteiro PartII PowderMaterialsProcessingandFundamentalUnderstanding Combustion Synthesis of ZrC-TiC Composite Nanoparticle by Self-Propagating High Temperature Synthesis (SHS) inZrO –TiO –Mg/Al–CSystem .................................... 143 2 2 MehmetBugdayciandOzanCoban SinteringMechanismforPolycrystallineDiamond .................... 151 RandalM.German Combustion Synthesis of B C–TiB Composite Nanoparticle 4 2 by Self-Propagating High-Temperature Synthesis (SHS) inB O –TiO –Mg–CSystem ....................................... 161 2 3 2 OzanCoban,MehmetBugdayci,SerkanBaslayici,andM.ErcanAcma AuthorIndex ...................................................... 171 SubjectIndex ..................................................... 173 About the Editors Bowen Li is a Research Professor in the Depart- ment of Materials Science and Engineering and Insti- tute of Materials Processing at Michigan Technolog- ical University. His research interests include mate- rials characterization and analysis, metals extraction, ceramic process, antimicrobial additives and surface treatment, porous materials, applied mineralogy, and solid waste reuse. He has published more than 140 technical papers in peer-reviewed journals and confer- ence proceedings, authored/co-authored 3 books, and edited/co-edited12books.Healsoholds16patentsand has delivered more than 30 invited technical talks. Dr. LireceivedaPh.D.degreeinMineralogyandPetrology fromChinaUniversityofGeosciencesBeijingin1998 andaPh.D.degreeinMaterialsScienceandEngineering from Michigan Technological University in 2008. He hasbeenanactivememberinTheMinerals,Metals& Materials Society (TMS), Society for Mining, Metal- lurgy&Exploration(SME),andChinaCeramicSociety. At TMS, he has served as the chair of the Materials CharacterizationCommitteeandasamemberofTMS CDDC Committee, Powder Materials Committee, and the Biomaterials Committee. He has also served as an EPDAwardcommitteemember,JOM subjectadvisor, andkeyreaderforMetallurgicalandMaterialsTrans- actions A. He has been organizer/co-organizer of a numberofinternationalsymposiaandsessions.Healso served as an editorial board member of the Journal ofMineralsand MaterialsCharacterizationandEngi- neering, Reviews on Advanced Materials Science, and ix x AbouttheEditors FUTOJournalSeries.HeistherecipientofAIMEHal W.HardingeAward(2022). DipankarGhoshiscurrentlyanAssociateProfessorin theMechanicalandAerospaceEngineeringDepartment at Old Dominion University (ODU), Norfolk, VA and joined the MAE faculty in July 2014. Prior to joining ODU, Dr. Ghosh was a postdoctoral scholar in the Division of Engineering and Applied Science at Cali- fornia Institute of Technology. He also held a position of postdoctoral associate in the Materials Science and Engineering Department at University of Florida. He completedhisPh.D.inMechanicalEngineeringin2009 fromtheUniversityofFlorida,Gainesville.Dr.Ghosh directs the Laboratory of Advanced Manufacturing of Materials. His research is focused on the freezing of particulate suspensions to develop novel direction- allyporousmaterialsandmultilayeredcomposites.Dr. Ghosh is primarily working on advancing the freeze- castingtechnologyforthesynthesisanddesignofnovel hierarchical ceramics and composites with a multidis- ciplinary research approach. Dr. Ghosh has published 2 book chapters, 47 peer-reviewed articles in presti- giousjournals,andisauthor/co-authorinover50confer- encepresentations.Hisresearchhasbeenfundedbythe USNationalScienceFoundation(NSF),ThomasF.and Kate Miller Jeffress Memorial Trust, Office of Naval Research (ONR), 4Va program, private industry, and internalgrantsfromODUResearchFoundation. Eugene A. Olevsky is the Dean and Distinguished Professor of the College of Engineering at San Diego State University. He has two M.S. degrees in Mechan- icalEngineeringandAppliedMathematicsandaPh.D. in Materials Engineering. He is the author of over 500 publications and more than 150 invited presenta- tionsinsinteringresearch.Hehassupervisedmorethan 100postdoctoral,graduate,andundergraduatestudents. Prof. Olevsky is a Fellow of the American Ceramic Society,aFellowoftheAmericanSocietyofMechanical Engineers, a Fellow of ASM International, Humboldt Fellow, and a Fellow of the International Institute of ScienceofSintering.

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