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ADVANCES IN CERAMICS ARMOR VI: Ceramic Engineering and Science Proceedings, Volume 31 PDF

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Advances in Ceramic Armor VI Advances in Ceramic Armor VI A Collection of Papers Presented at the 34th International Conference on Advanced Ceramics and Composites January 24-29, 2010 Daytona Beach, Florida Edited by Jeffrey J. Swab Volume Editors Sanjay Mathur Tatsuki Ohji ) WILE Y A John Wiley & Sons, Inc., Publication Copyright © 2010 by The American Ceramic Society. All rights reserved. Published by John Wiley & Sons, Inc., Hoboken, New Jersey. Published simultaneously in Canada. No part of this publication may be reproduced, stored in a retrieval system, or transmitted in any form or by any means, electronic, mechanical, photocopying, recording, scanning, or otherwise, except as permitted under Section 107 or 108 of the 1976 United States Copyright Act, without either the prior written permission of the Publisher, or authorization through payment of the appropriate per-copy fee to the Copyright Clearance Center, Inc., 222 Rosewood Drive, Danvers, MA 01923, (978) 750-8400, fax (978) 750-4470, or on the web at www.copyright.com. Requests to the Publisher for permission should be addressed to the Permissions Department, John Wiley & Sons, Inc., 111 River Street, Hoboken, NJ 07030, (201) 748-6011, fax (201) 748-6008, or online at http://www.wiley.com/go/permission. Limit of Liability/Disclaimer of Warranty: While the publisher and author have used their best efforts in preparing this book, they make no representations or warranties with respect to the accuracy or completeness of the contents of this book and specifically disclaim any implied warranties of merchantability or fitness for a particular purpose. No warranty may be created or extended by sales representatives or written sales materials. The advice and strategies contained herein may not be suitable for your situation. You should consult with a professional where appropriate. Neither the publisher nor author shall be liable for any loss of profit or any other commercial damages, including but not limited to special, incidental, consequential, or other damages. For general information on our other products and services or for technical support, please contact our Customer Care Department within the United States at (800) 762-2974, outside the United States at (317) 572-3993 or fax (317) 572-4002. Wiley also publishes its books in a variety of electronic formats. Some content that appears in print may not be available in electronic format. For information about Wiley products, visit our web site at www.wiley.com. Library of Congres sCataloging-in-Publicati oDnata is available. ISBN 978-0-470-59470-4 Printed in the United States of America. 10 9 8 7 6 5 4 3 21 Contents Preface ix Introduction xi Inspecting Composite Ceramic Armor Using Advanced Signal 1 Processing Together with Phased Array Ultrasound J. S. Steckenrider, W. A. Ellingson, E.R. Koehl, and T. J. Meitzler A Comparison of NDE Methods for Inspection of Composite 13 Ceramic Armor W. A. Ellingson and E.R. Koehl, T. J. Meitzler, L. P. Franks, and J. S. Steckenrider NDT Characterization of Boron Carbide for Ballistic Applications 25 Dimosthenis Liaptsis, Ian Cooper, Nick Ludford, Alec Gunner, Mike Williams, David Willis, Colin Roberson, Lucian Falticeanu, and Peter Brown Advanced Nondestructive Ultrasound Characterization of 37 Transparent Spinel A. R. Portune and R. A. Haber Optimization of a Portable Microwave Interference Scanning System 47 for Nondestructive Testing of Multi-Layered Dielectric Materials K. F. Schmidt, Jr., J. R. Little, Jr., W. A. Ellingson, L. P. Franks, and W. Green Corrective Techniques for the Ultrasonic Nondestructive Evaluation 57 of Ceramic Materials S. Bottiglieri and R. A. Haber Quantitative Evaluation of Structural Damage in Lightweight Armor 69 Materials Via XCT William H. Green, Kyu C. Cho, Jonathan S. Montgomery, and Herbert Miller v Static and Dynamic Properties of Mg/Ceramic MMCs 79 M. K. Aghajanian, A. L. McCormick, A. L. Marshall, W. M. Waggoner, and P. K Karandikar Impact Study of AIN-AION Composite 87 Kakoli Das, Monamul Haque Dafadar, Rajesh Kumar Varma, and Sampad Kumar Biswas Ballistic Evaluation and Damage Characterization of Metal-Ceramic 97 Interpenetrating Composites for Light Armor Applications Hong Chang, Jon Binner, and Rebecca Higginson Effect of an Interface on Dynamic Crack Propagation 105 Hwun Park and Weinong Chen Dynamic Equation of State and Strength of Boron Carbide 115 Dennis E. Grady Multiscale Modeling of Armor Ceramics 143 Reuben H. Kraft, Iskander Batyrev, Sukbin Lee, A. D. Rollett, and Betsy Rice Future Transparent Materials Evaluated through Parametric 159 Analysis Costas G. Fountzoulas and James M. Sands Nano-Processing for Larger Fine-Grained Windows of Transparent 167 Spinel Andreas Krell, Thomas Hutzler, Jens Klimke, and Annegret Potthoff Experimental Methods for Characterization and Evaluation of 183 Transparent Armor Materials E. Strassburger, M. Hunzinger, J. W. McCauley, and P. Patel Method for Producing SiC Armor Tiles of Higher Performance at 199 Lower Cost Bhanu Chelluri, Edward Knoth, Edward Schumaker, and Lisa P. Franks Development of Biomorphic SiSiC- and C/SiSiC-Materials for 207 Lightweight Armor Bernhard Heidenreich, Matteo Crippa, Heinz Voggenreiter Elmar Straßburger, Heiner Gedon, and Marco Nordmann Influence of Impurities on Stacking Fault Dynamics in SiC under 221 External Loading Vladislav Domnich and Richard A Haber Evolution of the AIN Distribution during Sintering of Aluminium 231 Nitride Doped Silicon Carbide N. Ur-rehman, P. Brown, and L. J. Vandeperre vi · Advances in Ceramic Armor VI Microstructure, Mechanical Properties, and Performance of 239 Magnesium Aluminum Boride (MgAIB ) 14 Michael L. Whittaker, Raymond A. Cutler, James Campbell, and Jerry La Salvia Microstructural Development and Phase Changes in Reaction 251 Bonded Boron Carbide P. G. Karandikar, S. Wong, G. Evans, and M. K. Aghajanian Author Index 261 Advances in Ceramic Armor VI · vii Preface The Armor Ceramics Symposium was held January 25-27, 2010 in Daytona Beach, FL as part of the 34th International Conference and Exposition on Advanced Ceramics and Composites. The 8th edition of this symposium consisted of over 65 oral and poster presentations on topics such as Impact, Penetration and Material Modeling, Boron Carbide, Silicon Carbide, Dynamic Material Behavior, Transpar- ent Materials, and NDE Applications. The symposium continues to foster discus- sion and collaboration between academic, government and industry personnel from around the globe. On behalf of the organizing committee I would like to thank the presenters, au- thors, session chairs and manuscript reviewers for their efforts in making the sym- posium and the associated proceedings a success. As special thanks goes to Marilyn Stoltz and Greg Geiger of The American Ceramic Society who was always there to answer my questions and provide the guidance and administrative support neces- sary to ensure a successful symposium. JEFFREY J. SWAB IX Introduction This CESP issue represents papers that were submitted and approved for the pro- ceedings of the 34th International Conference on Advanced Ceramics and Compos- ites (ICACC), held January 24-29, 2010 in Daytona Beach, Florida. ICACC is the most prominent international meeting in the area of advanced structural, functional, and nanoscopic ceramics, composites, and other emerging ceramic materials and technologies. This prestigious conference has been organized by The American Ce- ramic Society's (ACerS) Engineering Ceramics Division (ECD) since 1977. The conference was organized into the following symposia and focused ses- sions: Symposium 1 Mechanical Behavior and Performance of Ceramics and Composites Symposium 2 Advanced Ceramic Coatings for Structural, Environmental, and Functional Applications Symposium 3 7th International Symposium on Solid Oxide Fuel Cells (SOFC): Materials, Science, and Technology Symposium 4 Armor Ceramics Symposium 5 Next Generation Bioceramics Symposium 6 International Symposium on Ceramics for Electric Energy Generation, Storage, and Distribution Symposium 7 4th International Symposium on Nanostructured Materials and Nanocomposites: Development and Applications Symposium 8 4th International Symposium on Advanced Processing and Manufacturing Technologies (APMT) for Structural and Multifunctional Materials and Systems Symposium 9 Porous Ceramics: Novel Developments and Applications Symposium 10 Thermal Management Materials and Technologies Symposium 11 Advanced Sensor Technology, Developments and Applications XI Focused Session 1 Geopolymers and other Inorganic Polymers Focused Session 2 Global Mineral Resources for Strategic and Emerging Technologies Focused Session 3 Computational Design, Modeling, Simulation and Characterization of Ceramics and Composites Focused Session 4 Nanolaminated Ternary Carbides and Nitrides (MAX Phases) The conference proceedings are published into 9 issues of the 2010 Ceramic En- gineering and Science Proceedings (CESP); Volume 31, Issues 2-10, 2010 as out- lined below: • Mechanical Properties and Performance of Engineering Ceramics and Com- posites V, CESP Volume 31, Issue 2 (includes papers from Symposium 1) • Advanced Ceramic Coatings and Interfaces V, Volume 31, Issue 3 (includes papers from Symposium 2) • Advances in Solid Oxide Fuel Cells VI, CESP Volume 31, Issue 4 (includes papers from Symposium 3) • Advances in Ceramic Armor VI, CESP Volume 31, Issue 5 (includes papers from Symposium 4) • Advances in Bioceramics and Porous Ceramics III, CESP Volume 31, Issue 6 (includes papers from Symposia 5 and 9) • Nanostructured Materials and Nanotechnology IV, CESP Volume 31, Issue 7 (includes papers from Symposium 7) • Advanced Processing and Manufacturing Technologies for Structural and Multifunctional Materials IV, CESP Volume 31, Issue 8 (includes papers from Symposium 8) • Advanced Materials for Sustainable Developments, CESP Volume 31, Issue 9 (includes papers from Symposia 6, 10, and 11) • Strategic Materials and Computational Design, CESP Volume 31, Issue 10 (includes papers from Focused Sessions 1, 3 and 4) The organization of the Daytona Beach meeting and the publication of these pro- ceedings were possible thanks to the professional staff of ACerS and the tireless dedication of many ECD members. We would especially like to express our sincere thanks to the symposia organizers, session chairs, presenters and conference atten- dees, for their efforts and enthusiastic participation in the vibrant and cutting-edge conference. ACerS and the ECD invite you to attend the 35th International Conference on Advanced Ceramics and Composites (http://www.ceramics.org/icacc-ll) January 23-28, 2011 in Daytona Beach, Florida. Sanjay Mathur and Tatsuki Ohji, Volume Editors July 2010 xii · Advances in Ceramic Armor VI Advances in Ceramic Armor VI Edited by Jeffrey J. Swab Copyright © 2010 The American Ceramic Society INSPECTING COMPOSITE CERAMIC ARMOR USING ADVANCED SIGNAL PROCESSING TOGETHER WITH PHASED ARRAY ULTRASOUND J. S. Steckenrider Illinois College Jacksonville, IL W. A. Ellingson and E.R. Koehl Argonne National Laboratory Argonne, Illinois USA T.J. Meitzler US Army, TARDEC Warren, MI ABSTRACT A series of 16-inch square by 2-inch thick, multi-layered ceramic composite armor specimens have been inspected using a 128 element, 10MHz immersion phased array ultrasound system. Some of these specimens had intentional design defects inserted interior to the specimens. Because of the very large changes in acoustic velocities of the various layered materials, ultrasonic wave propagation is problematic. Further, since the materials used in the layers were stacked such that a lower elastic modulus material was on one side and a higher elastic modulus material was on the other, the side selected for ultrasonic insonification became a significant parameter. To overcome some aspects of the issues with the acoustic wave propagation, two digital signal processing methods were employed. These were: 1)- use of fast Fourier transforms (FFT) and 2)-an integrated signal analysis. Each method has strengths and weaknesses with application in part dependent upon the side of sample used for insonification. The results clearly show that use of these methods significantly improves defect detection. This paper presents the details of the samples used, the issues with ultrasonic wave propagation, a discussion of the two digital signal processing algorithms and results obtained. INTRODUCTION Ceramic armor for vehicles offers significant potential improvement over historical materials as it provides a greater capacity for energy absorption and dissipation per unit mass, achieved through very high fracture toughness. However, unlike their metallic predecessors, ceramic materials are much more vulnerable to manufacturing defects, as any such flaws can dramatically reduce that high toughness, thereby compromising the armor's ability to protect military personnel. Thus, an efficient non-destructive evaluation (NDE) method which can identify these defects before the armor is placed into service is critical to their effectiveness1. Conventional ultrasonic techniques have been used to both locate and characterize such defects in the monolithic ceramic tiles that make up the "backbone" of these armor panels2'3. Furthermore, phased-array ultrasound4 (PA-UT) has demonstrated significant improvement over these methods5 as it offers both enhanced sensitivity and markedly improved throughput67. While PA-UT has clearly demonstrated its performance with regard to the monolithic tiles themselves, actual implementation of ceramic armor incorporates these monolithic tiles into 1

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