TID-4500, UC-35 L5 LAWRENCE UVERMORE LABORATORY U*^ty&CaHoa&/UwmmCaltOtnitf/S4550 UCRL-51296 MECHANICAL PROPERTIES OF GRANITE FROM THE TAOURIRT TAN AFELLA MASSIF, ALGERIA fi. N. Schock A. E. Abey H. C. Heard II. Louis MS date: November ",, 1972 -NOTICC- Tliii report wos prepircd as on account of work sponsored by the United Stales Government. Neither the United States nor the United Slates Atomic Energy Commission, nor any of their employees, nor any of their contractors, subcontractors, or Ihcu employees, makes any warranty, cxircss or Implied, or assumes an;' legal liability or rcsponiiblllly for the accuracy, com pleteness or usefulness of any Information, apparatus, pjoduct or process disclosed, or represents that Its uso would not infringe privately owned rights. • i r- ";,;~'"-'r^i 1 1 ••', V • • -III I) \ Contents Abstract I introduction 1 Pressure-Volume Determinations 3 Determination of Shear Strength at High Pressure 5 Uniaxial Compression Tests 6 Torsion Tests 7 Brazil Tests 11 Acoustic Velocity Determinations 11 Three-Dimensional Stress-Strain Determinations 13 Uniaxial Stress 14 Uniaxial Strain 16 References 19 MECHANICAL PROPERTIES OF GRANITE FROM THE TAOURIRT TAN AFELLA MASSIF, ALGERIA Abstract The mechanical properties of a granite granites that have been studied extensively. from the French Hoggar test site in The failure envelope was determined to Algeria were measured to provide input 30-kbar mean stress with no evidence of for numerical codes seeking to predict ductile behavior. Stress-strain experiments rock response to a stress wave and to reveal the presence of long narrow cracks assist in formulating models on which which close at stress libels below 0.5 kbar. these codes are based. The measured The rock at atmospheric pressure was properties include pressure-volume found to have a bulk modulus of 330 kbnr behavior, failure envelope as a function and a shear modi'lus jf 290 kbar. These of mea.i pressure, compressional and yield an elastic compressional velocity of shear velocities as a function of pressure, 5.24 km sec" , in good agreement with and three-dimensional stress-strain laboratory measurements on small measurements along various loading and samples and with field experiments within unloading paths. This granite responds the massif over distances of several tens to stress in much the same way as other of meters. Introduction As part of an exchange program between test site and expe; Imental conditions Is the French Commissariat a L'Energie given by Stephens. Atomique (CEA) and the United States The Hoggar test site consists primarily Atomic Energy Commission, related to of Taourirt Tan Afella (24° 03' N, 5° 02' the peaceful use of nuclear explosives, E) and the surrounding plains. The we have received a suite of rock samples samples received (henceforth called from a 765-m borehole in the Taourirt Hoggar) were from a borehole drilled Tan Afella massif, on the Hoggar test into the massif to within 40 m of the shot site, in what was formerly French point, prior to the Monique explosion Algeria. The French have conducted (117 kT). A cross-section of the massif several underground nuclear explosions through the borehole is shown in Fig. i. in this massif. A summary of previous We received samples from every 20 or technical exchanges and a bibliography ot 30 m between the surface and 750 m. the French reports describing the Hoggar Each sample is approximately 10 cm in -l- AltituHo -— m SW NE 2000- — /"""•"^.^ Borehole T 71 1800- J IOOP"^*^. TAOURIRT TAN AFELLA 1600- 30o\- 1400- 500V- 1200- 700 m\- Projection of mino shaft \ = {extonding to the north from 11000000-- Point 0 point 0 for about 1230 m) Scalar 1/10,000 Fig. 1. Southwest-Noriheast section through Borehole T. 71. _j i_ 1_ 10 20 30 40 50 60 70 80 90 cm Fig. 2. French CEA photograph of granite samples. -2- Table 1. Properties of the granite of motion, and wave propagation. Since Taourirt Tan Afella.3 these calculational codes require mech Mineralogical analyses anical properties as input, ivo have chosen Quartz 3 57o Ch aye's to concentrate first on the rock samples index 64 Microcline 37% closest to the explosion. The deepest Plagioclase 25% sample (7 50 m) is from just outside the Biotite 2.1% region in which the cavity was produced, Muscovite 0.6% and where peak stresses are of the order of tens oC kilobars. Chemical analyses We have experimentally determined Si0 7 5.80% K0 4.7 9% 2 2 the pressure-volume loading behavior to AlO 12.49% Ti0 0.08% 2 s 2 35 kbar, the failure envelope to 50 kbar 1.30% o.oi/o Fe2°3 P2C5 mean pressure, and acoustic velocities to MnO 0.04% co 0.13% 2 10 kbar. In addition, the stress-atrain MgO 0.03% H0+ 0.48% 2 relationships in quasi-static loading have CaO 0.59% H0- 0.06% 2 bvi^n measured to 15 kbar to determine Na0 3.80% 2 such parameters as the stress and path dependence of the shear modulus, and the length by 5 cm in diameter, althougu the properties on unloading from peak stresses size and core diameter vary slightly below the failure envelope. The experi (Fig. 2). The samples were coherent, mental techniques used have been de- 4-8 appeared relatively unaltered and showed cribed in detail elsewhere. The aver little evidence of fracturing. Chemical age density of the material studied is -3 and mineralogical analysis of the granite 2.61 g cm and varied between 2.604 and body are given in Table 1. 2.617. All stresses are referred to a One of the primary goals of this ex cylindrical coordinate system witn a,, a„ change of rock samples is to compare and a„ the maximum, intermediate, and numerical simulation techniques that seek minimum principle stresses. Stress is to predict such explosion induced features taken as positive and strain as negative as cavity dimensions, fracturing, ground in compression. Pressure-Volume Determinations The pressure-volume relationship for volume relationship is determined from Hoggar granite was determined on four measurements of force and piston dis different samples from 700 m. Two of placement. The results from the two these samples (1.15 cm diam X 2.54 cm 3 5-kbar quasi-hydrostatic runs are shown cylinders) were compressed to 35 kbar by the symbols O and A in Fig. 3. The in a quasi-hydrostatic piston cylinder remaining two samples (1.91 cm diam apparatus. This apparatus uses tin as X 2.54 cm) were tested in a hydrostatic the pressure medium. The pressure- apparatus to 14 kbar. These sampies -3' 0.94 0.95 0.96 0.97 0 98 0.99 1.00 v/v 0 Fig. 3. Pressure-volume relationship for Hoggar granite. Climax Stock gronodiorite, and Westerly granite. Pressure-volume relationships are shown for com parison. were jacketed in 0.02-cm lead to prevent penetration of the pressure fluid into the v/v'o = - AZ ciCpi ,P•' , (i) n rock. Strain was measured as a function l»0 of pressure by foil strain gap that are where C, is a constant and P-> l Ii_s pressure bonded to the lead jacket. Tho results for in kbar. The bulk modulus, K, can be the hydrostatic tests are shown as D and expressed as a ratio of power series V in Fig. 3. For comparison. Fig. 3 also shows the pressure-volume relation- 9 C.P ships for Climax Stock granodiorlte and i K =-q-^ . (2) Westerly granite. I" i • C • P*1-1' The results from all four runs appear t to be in good agreement in the overlapping i=l region. A curve '«* drawn through the Table 2 gives the values for C,. Equa experimental data up to 35 kbar. These tion 2 gives a bulk modulus at P = 0 of data may be expressed as a power series, 326 kbar. -4- Table 2. Polynomial coefficients in Eq. 2 and derived pressure- volume data. [ Ct 0 1.000000000 1 -3.06201539X 10"3 2 1.50892659 X 10"4 3 -1.64618743 X 10"5 4 1.05764000 X 10"6 5 -3.22663929 X 10"8 6 1.45310915 X 10"10 7 1.86230791 X 10"11 8 -4.99569603 X 10-13 9 41 .12613182 X 10" 5 P v/v K (kb) 0 (kb) 0 1. 326 0.5 0.9985 342 1 0.9971 357 5 0.9872 436 10 0.9765 487 15 0.9672 56S 20 0.9594 675 25 0.9529 770 30 0.9468 795 35 0.9409 810 Determination of Shear Strength at High Pressure The differential stress-strain behavior 1.9 cm diam by 3.0 cm long at 1 bar of this granite was determined in three pressure. The compression tests were types of tests: 1) uniaxial compression carried out in a fluid medium using on cylinders 1.2 cm diam by 2.5 cm long jacketed samples. Pressures wrere under confining pressures ranging up to determined from the resistance change of 22 kbar, 2) torsion of solid disks 0.25 cm manganin wire coils and the axial loads diam by 0.7 cm long under pressures imposed on the sample were measured ranging up to 50 kbar, and 3) indirect within the pressure vessel with a force tensile tests (Brazil) on right cylinders gage placed in mechanical series with the -5- test sample. Changes in sample length Tabic 3. Compression,teats, Jloggar granodiorite. were determined from external piston displacements. Accuracies of measure •i ni r.i •'> " ~' <\ K ment are estimated at 0.5 to 1.0% after calibration. General descriptions of the 2007 n 0 0 I04T. 0 GftS 0 apparatus as well as discussions of gen 31(52 f) 0 o tono 0 f?0 0 eral techniques used are described else- s-r'.4n0o 42 210000 aa isoo 3:>(1.i0o 2.i7n 3;o0 1 r-"3r0. i 23<0>(1300 tiirnji where. The torsion tests were carried :o2ro «520 1000 toiio 4C40 I?20 (010 233d woo J4!>0 1000 1040 44*0 12.10 lifO Ifl (10 out in a solid-pressure medium appara 15030 C7C0 21.00 20110 6S20 3*40 tuso 3MO 14370 "310 3010 21.10 GlflO .10*0 nuo 4150 tus. The mean prersures as well as innri OliO 3000 :. n o coso 300O 7fi4.1 :<l 10 the torques and twists applied to the I 7340 i mo .TOM- :il -o "120 4040 7 7 SO Nl -10 1P020 14600 3C?'' 3840 7fi7r> 1.100 P7G0 ?+3P sample disk were measured externally. I 7*70 3430 3020 "MfJO 7330 3130 7fi30 5270 Accuracies for these tests are believed 1DP30 11470 4000 42:0 7P70 3G30 9.110 iCSO aieso 15050 soso 3? 10 0300 0 ion no S310' to be about 5%. The indirect tensile tests 31)70 13300 5100 MOO D040 .14 50 1-1-10 7700 23010 CSIO 60C0 (1510 (1700 0 11*110 r.ni 0 were made in a standard testing machine 25760 7300 70 BO 7.100 !>350 0 133PS 7.10.11 having accuracies of <0,S%. All three 2 MOO 7300 70GO 73P0 «00 y 1.1J !>0 7300 33020 12350 13350 1 23 SO 10750 0 I0-.20 12350 test types were carried out at room 37110 153(50 153C0 153G0 toono 0 2?r,m 153 GO •4 43700 202C0 202KO 30360 11370 0 2'7tV. 3^ .0 temperature and at stra'n rates of 10 4 3330 21030 21030 31^30 11700 0 30730 71M0 tto 10"5/sec. flntnn proooufo. All fallm 11, ir. >>v UriHlo fr -aclurc. T. 713toi it nnmpli en from COO to 7 5'0 rtl. UNIAXIAL COMPRESSION TESTS the single or occasionally conjugate shear Differential stress-axial strain curves fractures in these samples did not punc at each pressure were calculated from ture the thin-wall jacketing material. For the raw force-displacement data and the the highest pre93ure tests, displacements initial sample dimensions. Intercomparl- on the fracture surfaces were sufficient son of these curves over v .e range of to penetrate the jacket and allow the fluid pressures investigated along with visual pressure access to the rock with conse observations on the deformed test samples quent drop in stress to zero. Total then yielded an internally consistent pat permanent strains before onset of fracture tern of behavior with pressure for the were about 1 to 2% with the tendency to Hoggar granite. increase somewhat with pressure. Be In each ease, the stress-strain curve havior of all samples could thus be termed showed a quasi-elastic portion followed brittle. by a narrow region of yielding (both ir, The principal stresses at the point of stress-:as well as in strain) which finally fracture la., a,) as well as the stresses terminated in fracture. In most tests, supported by tl e granite ir mediately after with the exception of those at the highest fracture (aj, cri) are summarized inTable3. pressures, the stress after fracture did From this table it is apparent that a or not drop to zero but remained at about the shear stress -r, [a - o~'i/2, markedly one-half the ultimate (fracture) value. increases with confining pressure o„. The tensile fracture planes as well as Sucih btihavior Is to be expected if the -6- ."qiluro mechanism responsible <s depend- at which the dominant .'iiechynisn: of e it upon normal stress. Shear fracture deformation became plastic flow in the and frictional sliding of adjacent surfaces component crystals (ductile behavior) arc two such mechanisms. Figure -J prompted us to extend our measurement? illustrates this increase in strength with to tho highest preus<irt, * possible. Com pressure up to pressures of 22 kbar. pression testing i'ecomen very difficult 12 Results on the same roclt to S kbar are in fluido at pressure:; above about 25 kbar. also shown. Agreement between the two Thus, ~.-o initiated a limited pr< gram of sets of data is considered very good at the strength measurements in torsion in tho lower pressures but only fair in the 2 to pressure region 21 to 50 kbnr in a ."olid 4 kbar range. Discrepancies diminish at pressure medium apparatus. the highest comparable pressure and it Re-outta from the torsion tests in the >-.ppears the two curves might cross and form of torque-twist curvej as well as diverge if higher pressure data were the deformed samples had the same available. Also shown for comparison characteristics as the compression data are data for tw< similar rocks—tho discussed above. Values for the prlncip; Westerly grafjit"; to 20 kbar and the stresses at fracture, as calculated in Uv Climax Stock granodiorite to 8 libar. The outer flboru of the deformed disk, are esterly results are nearly parallel to oummcrli'.ed in Table -t for comparison that of the Hoggar to the highest pres with those for compression (Table 3). sures; the only significant difference is From these tables it appears the fracti.r the 3 to 4 kbar offset in fracture strength strength lu apparently still increasing t at pressures above about 10 kbar. Tho the highest pressures mea&ured. Gr: uc Hardhot granodioritc apparently la stronger comparison of both sets of results ar< than b ••) granites. Results for both the iloggar and Table 1. Torsion tests, Hoggar grano Westerly granites are also shown as diorite.3 failure envelopes in shear stress-mean pressure space (Fig. 5). In addition, tho strength of the Hoggar samples after fracture is shown for comparison. It is kb apparent that this granite retains con 41.2 21.0 0.8 10.1 21.0 siderable strength under pressure even 41.2 21.0 0.0 10.1 21.0 though all cohesion is destroyed. Avail 44.5 21.0 -2.5 11,8 21.0 able data ior the Hardhat and Westerly 56.2 29.0 1.8 13.5 ?9.0 rocks also indicate comparable strengths 56.6 29.0 1.4 13.8 29.0 after fracture. 63.2 35.0 6.8 14.1 35.0 dl.4 35.0 8.6 IS.2 3 5.0 TORSION TESTS 79.5 50.0 20.5 14.8 50.0 80.6 50.0 19.4 1 5.3 50.0 The desire to determine the limiting All failure is by brittle fracture. shear strength as well as the pressures T. 71 test samples from 600 to 7 50 -7- 0 5 10 15 20 25 a, — kbar Fig. 4. Axial stress difference at failure as a function of confining pressure for Hoggar and Westerly granites and Climax Stock granodiorite. -8-
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