IS 10130: Vulcanized Vegetable Oils (factice) for Rubber Industry

11 Pages·1992·1.2 MB·English

by  Bureau of Indian Standards

इंटरनेट मानक
Disclosure to Promote the Right To Information
Whereas the Parliament of India has set out to provide a practical regime of right to
information for citizens to secure access to information under the control of public authorities,
in order to promote transparency and accountability in the working of every public authority,
and whereas the attached publication of the Bureau of Indian Standards is of particular interest
to the public, particularly disadvantaged communities and those engaged in the pursuit of
education and knowledge, the attached public safety standard is made available to promote the
timely dissemination of this information in an accurate manner to the public.
“जान1 का अ+धकार, जी1 का अ+धकार” “प0रा1 को छोड न’ 5 तरफ”
Mazdoor Kisan Shakti Sangathan Jawaharlal Nehru
“The Right to Information, The Right to Live” “Step Out From the Old to the New”
IS 10130 (1992): Vulcanized Vegetable Oils (factice) for
Rubber Industry [PCD 13: Rubber and Rubber Products]
“!ान $ एक न’ भारत का +नम-ण”
Satyanarayan Gangaram Pitroda
““IInnvveenntt aa NNeeww IInnddiiaa UUssiinngg KKnnoowwlleeddggee””
“!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता हहहहै””ै”
Bhartṛhari—Nītiśatakam
“Knowledge is such a treasure which cannot be stolen”

( )
rfpT ~;rfbJT
h&an Standard
VULCANIZED VEGETABLEOILS(FAC77CE)
FORRUBBER INDUSTRY- SPECIFICATION
( First Revision )
UDC 678’4’046’72

0 BIS 1992
BUREAU OF INDIAN STANDARDS
MANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG
NEW DELHl 110002

March 1992 Price Group 2
rebbuR stcudorP lanoitceS ,eettimmoC PCD 13
FOREWORD
sihT naidnI dradnatS was detpoda yb eht uaeruB fo naidnI ,sdradratS retfa eht tfard dezilanif
yb eht rebbuR stcudorP lanoitceS eettimmoC had neeb devorppa yb eht ,muelorteP laoC and
detaleR stcudorP noisiviD .licnuoC
sihT standard was tsrif dehsilbup ni 289l and is gnieb desiver htiw emos segnahc ot suit eht
stnemeriuqer fo eht ,sresu srecudorp and ,osla gniredisnoc eht raw lairetam noitisop as gnitsixe ni
.aidnI ehT muelortep rehte tcartxe tset has neeb dedulcni ot ekat erac fo rotsac lio desab secitcaf
hcih-w evlossid yletelpmoc ni enoteca d.ra lliw ton evig eht eulav fo segatnecrep fo sevitidda hcus
as larenim .lio
dezinacluV elbategev ,slio osla nwonk as ECITCAF era decudorp using elbategev slio dezinacluv
htiw sul~phur, sulphur edirolhc ro rehto~yna elbatius sulphur gniniatnoc cinagro .dnuopmoc tI
is desu ni eht rebbur ,stcudorp htob larutan and citehtnys as a gnissecorp aid.
dezinacluV elbategev slio ( SECITCAF > era dedarg gnidrocca ot rieht ,ruoloc ,yleman ,nworb
nedlog and .etihw nworB and dedlog SECITCAF desab no rotsac lio era osla ,tnatsiser and
ecneh mrof an largetni trap fo this .noitacificeps gniredisnoC eht raw lairetam ytilibaliava and
snoitcirtser desopmi no elbide slio rof esu ni ,yrtsudui this noitacificeps lliw eb desab no eht raw
slairetam rof ,ecitcaf elbaliava ni eht ,yrtnuoc ,yleman rotsac .lio etihW secitcaf era yllareneg
edam morf mustard ,lio epar dees ,lio tundnuorg lio and ralimis .slio yehT era hgih tsoc
secitcaf tnaem rof srossare and ralimis .snoitacilppa
hgiH ash tnetnoc debircserp ni epyT 3 edarG 2 secitcaf is eud ot etihw larenim srellif tneserp ni
meht rof ysae noitalunarg and .gniredwop yehT era deilppus ni redwop ro ralunarg .smrof
roF eht esoprup fo gnidiced rehtehw a ralucitrap tnemeriuqer fo this standard is deilpmoc ,htiw
eht lanif ,eulav devresbo ro ,detaluclac gnisserpxe eht tluser fo a tset ro ,sisylana shall eb dednuor
ffo ni ecnadrocca htiw SI 2 : 1960 seluR‘ rof gnidnuor ffo laciremun seulav ( desiver .‘) ehT
rebmun fo tnacifingis secalp deniater ni eht dednuor ffo eulav dluohs eb eht emas as that fo eht
deificeps eulav ni this standard.
2991:03101SI
Indian Standard
VULCANIZED VEGETABLE OILS ( FACTICl? )
FOR RUBBER INDUSTRY - SPFC‘IEICATIOfi
( First Revision )
1 SCOPE epyT 2 nedloG dezinacluv elbategev ,slio
and
1.1 sihT standard sebircserp eht stnemeriuqer
etihW dezinacluv elbategev .slio
and sdohtem fo sampling and stset rof -zinacluv Type 3
de elbategev slio ( ecitcaf ) rof esu ni rebbur
.yrtsudni 3.2 Grades
1.1.1 sihT standard srevoc dezinacluv elbategev
slio ( secitcaF ) rof lio ecnatsiser and ytilaiceps gnidnepeD no lacimehc-ocisyhp ,stnemeriuqer
snoitacilppa .osla nworb ( epyT 1 ) and etihw dezinacluv -egev
elbat slio ( epyT 3 ) shall eb fo owt sedarg and
2 REFERENCES nedlog dezinacluv elbategev slio ( epyT 2 ) shall
ehT gniwollof naidnI Standards era yrassecen eb fo eno edarg as detacidni ni elbaT 1.
stcnujda ot this standard:
4 STNEMERIUQER
SI .oN Title
4.1 noitpircseD
1070 noitacificepS rof retaw rof
: 1977
lareneg yrotarobal esu (
first
epyT 1 dezinacluv elbategev slio era yllausu
revision )
elbaliava ni lumps ro ,mrofi’selunarg and sepyT
7086 sdohteM fo sampling and 2
and 3 dezinacluv elbategev slio era elbaliava ni
( traP 1 ) : 1973 tset rof rebbur gnidnuopmoc
,stneidergni traP 1 ralunarg ro redwop .mrof hcaE epyt shall evahs
yllaitnesse doog ytilibisrepsid htiw .rebbur ehT
lairetam shall eb eerf morf ngierof rettam ekil
3 TYPES AND GRADES
,doow dust .cte
1.3
Types
erehT shall eb gniwollof eerht sepyt fo dezinacluv 4.2 ehT lairetam shall ylpmoc htiw eht
elbategev slio gnidneped no rieht~ :ruoloc stnemeriuqer nevig ni elbaT 1 nehw detset
gnidrocca ot erudecorp deificeps rednu 1oc 8

Type 1 nworB dezinacluv elbategev ,slio fo eht .elbaT
1
Table Requirements for Vulcanized Vegetable Oils
( Clauses 3.2 and 4.2 )
ix. citsiretcarahC epyT 1 epyT 2 epyT 3 %k:;e;ohteM
----r ~---* ----r 7---
edarG 1 edarG 2 edarG 1 edarG 2
)14 )2( )3( )4( )5( )6( )7( )8(
0 ecnaraeppA nworB nworB etihW etihW V&al
deruoloc deruoloc Y%%eT redwop redwop
pmul ro pmul ro redwop ro
ralunarg ralunarg selunarg
evitaleR ytisned 1.05 f 0.05 1.05 & 0.05 1.05 & 0.05 1.05 & 0.05 1.10 -+ 0.05 4 fo SI 7086
ii)
at 21127°C ( traP 1 ) : 1973
enotecA tcartxe ro 20 40 15 10 15 xennA A
iii)
muelortep rehte ,tcartxe
tnecrep yb mass,
Max
-iv) eerF sulphur, tnecrep 1 1.5 1.0 0.5 5-*o xennA B
yb mass,
Max
Ash ,tnetnoc tnecrep 0.5 0.5 1.0 2.0 20 xennA C
v)
yb mass, Max
vi) el batinfieoocprasenUp yb ,%.am ,rettam 1.0 1.0 0.I 1.0 5 xennA D
Max
vii) ,enirolhC tnecrep yb 0.02 0.02 0.02 3 8 xennA B
mass, xaM
1
IS 10130 : 1992
5 PACKING AN-D MARKING 6.2 Number of Tests
5.1 Packing tseT rof all scitsiretcarahc shall eb detcudnoc
Unless esiwrehto deerga ot neewteb eht no etisopmoc .elpmas
resahcrup and eht ,reilppus eht lairetam shall
eb dekcap ni denil-enelyhteylop hesslan bags. 6.3 Criteria for Conformity
5.2 Marking ehT tol shall eb deredisnoc as gnimrofnoc ot
5.2.1 hcaE egakcap shall eb dekram :htiw eht noitacificeps fi eht etisopmoc elpmas seifsitas
hcae fo eht .stnemeriuqer
4 eman fo eht ,lairetam epyt and ,edarg
b) noitacidni fo eht ecruos fo eht
,erutcafunam 7 TSET SDOHTEM
c>
ten mass fo eht ,lairetam 7.1 stseT shall eb detcudnoc gnidrocca ot eht
4 htnom and raey fo ,erutcafunam and sdohtem debircserp ni sexennA A ot E and eht
e) hctab ro edoc .rebmun tnaveler esualc fo SI 7086 ( traP 1 ) : 1973 as
nevig ni 1oc 8 fo elbaT 1.
5.2.2 hcaE egakcap yam osla eb dekram htiw
7.2 Unless deificeps esiwrehto erup‘ ’slacimehc
eht dradnatS Mark.
and dellitsid retaw ( ees SI 1070 : 1977 ) shall eb
6 SAMPLING deyolpme ni eht .stset
6.1 evitatneserpeR samples fo eht lairetam shall ETON - eruP‘ ’slacimehc llahs naem slacimehc
eb drawn as debircserp ni 15 fo SI 7086 that do ton niatnoc seitirupmi hcihw affect the
( traP 1 ) : 1973. stluser of .sisylana
ANNEX A
]
[ Clause 4.2, Table 1, Sl No. (iii)
DETERMINATION OF ACETONE/PETROLEUM ETHER EXTRACT
deriuqer ot llif and ytpme eht nohpis puc is
A-l REAGENTS
neewteb 5’2 and 5’3 .setunim
A-l.1 Acetone 3.2-A etaropavE eht tnevlos revo a maets bath,
using a eltneg tnerruc ro deretlif ria ot tneverp
dellitsiD revo suordyhna muissatop ,etanobrac
.gniliob evomeR eht ksalf morf eht maets bath
gniliob neewteb 56 and 57°C.
just roirp ot eht ecnaraeppasid fo eht last secart

fo tnevlos ot tneverp ssol fo .tcartxe eunitnoC
2.l-A muelorteP rehtE
eht passage fo ria hguorht eht ksalf rof
10 setunim ot evomer eht gniniamer tnevlos
gnivaH gniliob tniop morf 40 ot 60°C.
and yrd eht ksalf rof owt sruoh ni a 70 tr 5°C
ria .nevo
2-A ERJTDECORP
4.2-A looC ni a rotaccised ot eht moor
1.2-A hgieW yletamixorppa 2 g fo elpmas ni a
erutarepmet and .hgiew
retlif .repap dloF eht repap ni a yaw that ti
stif ni eht gnitcartxe ,puc and suspend eht puc
ni a dehgiew noitcartxe ksalf gniniatnoc 50 ot 3-A NOITALUCLAC
75 lm fo muelortep/enoteca .rehte roirP ot eht
gnihgiew fo eht noitcartxe ,ksalf ti shall evah enotecA muelortep/tcartxe
neeb deird rof owt sruoh at 70 & 5°C and rehte ,tcartxe tnecrep $- x 100
delooc ni a rotaccised ot eht erutarepmet fo eht yb mass
.ecnalab erehw
2.2-A tcartxE eht elpmas ylsuounitnoc rof A = mass ni g fo ,tcartxe~eht and
8 ,sruoh gnitaeh at a etar hcus that emit mass ni g fo elpmas ,desu
B =

2
IS 10130 : 1992
ANNEX B
[ Clause 4.2, Table 1, Sl No. (iv) ]
DETERMINATION OF FREE SULPHUR
B-l REAGENTS muidos etihplus noitulos htiw eht noitidda
fo 5 lm fo .lonahte retfA gnilooc add 10 lm
B-l.1 Sodium Sulphite Solution - 10 .tnecrep fo enilamrof ot evomer ssecxe ,etihplus neht
add 10 lm fo muitnorts edirolhc noitulos as llew
B-l.2 Formaline - 40 tnecrep edyhedlamrof as 5 lm muimdac edirolhc noitulds ot etatipicerp
.noitulos eerf yttaf .sdica retfA standing rof 30 setunim
retlif eht elohw mass hguorht nottoc loow and
B-l.3 Cadmium Chloride Solution - 3 .tnecrep tcaer eht etartlif htiw 15 lm fo 20 tnecrep citeca
.dica etartiT eht etahplusoiht os demrof htiw
4.l-B muitnortS edirolhC noituloS - 10 tnecrep 1’0 N enidoi noitulos using hcarts as .rotacidni
.noitulos
B-3 CALCULATION
B-1.5 Iodine Solution - 1’0 N.
eerF sulphur, tnecrep = 2300’0 v x ool
yb mass M
B-2 PROCEDURE
tcartxE 5 g fo eht lairetam htiw /enoteca erehw
muelortep rehte as ni xennA A. lioB eht
/I = lm fo 1’0 N enidoi ;noitulos and
enoteca muelortep/tcartxe rehte tcartxe rednu
xulfer rof owt sruoh htiw 30 lm fo 10 tnecrep M = mass ni g fo eht elpmas .nekat
ANNEX C
[ Table 1, SZ No. (v) ]
DETERMINATION OF ASH CONTENT
C-l APPARATUS rotaccised retfa .noitingi hgieW eht elbicurc
and its .stnetnoc
1.l-C aciliS ro nialecroP elbicurC
C-3 NOITALUCLAC
C-1.2 elffuM ecanruF
Ash ,tnetnoc tnecrep = C - A x ool
yb mass,
C-2 PROCEDURE B

erehw
ekaT a nwonk mass fo eht lairetam ( ylsuoiverp mass ni g fo eht ytpme ,elbicurc
A =
deird at 105°C ) ni a acilis .elbicurc etingI
mass ni g fo eht nemiceps ,nekat and
eht emas ni a elffum ecanruf at 550°C f 25°C B =
rof 16 h. looC eht tnetnoc fo eht elbicurc ni a C = mass ni g fo eht elbicurc and eht ash.
ANNEX D
[ Clause 4.2, Table 1, Sl No. (vi) ]
DETERMINATION OF UNSAPONIFIABLE MATTER
D-l REAGENTS tsellams tnuoma fo toh ,retaw ,looc add ti
ot eht revlis etartin noitulos and ekahs
.ylhguoroht wollA eht noitulos ot stand rof
D-l.1 Alcoholic Potash Solution
24 ,sruoh retlif and .litsid
eraperP a 2 N cilohocla muissatop edixordyh
noitulos yb gnivlossid eht deriuqer tnuoma fo 2.1-D muelorteP rehtE
muissatop edixordyh ni etulosba lonahte that
gnivaH gniliob tniop morf 40 ot 60°C.
has neeb deifirup as :swollof
2-D PROCEDURE
evlossiD 5’1 g fo revlis etartin ni 3 lm fo
,retaw and add ti ot eno ertil fo .lohocla 1.2-D lioB enoteca tcartxe fo 5 g fo lairetam
evlossiD 3 g fo muissatop edixordyh ni eht rednu xulfer htiw 30 lm fo 2 N cilohocla
3
IS 10130 : 1992
muissatop edixordyh rof owt .sruoh Add 5 lm gnillitsid ffo eht muelortep ,rehte eht eudiser is
fo retaw and liob rof a rehtruf 20 .setunim detaeh no a retaw bath rednu muucav ot
tnatsnoc mass.
2.2-D esniR eht paos noitulos os demrof htiw
50 tnecrep lohocla ni a gnitarapes lennuf and
ekahs at tsael 3 semit htiw 50 lm muelortep 3-D NOITALUCLAC
.rehte kaerB up eht noislume yb eht noitidda
deifinopasnU ,rettam itecrep
fo a small tnuoma fo .lohocla Wash eht -moc x$= 100
yb mass
denib muelortep rehte tcartxe ecno htiw lohocla
hcihw is ylthgils enilakla ot ,nielahthplonehp erehw
and neht htiw 25 lm fo 50 tnecrep lohocla litnu
this is ou regnol der ot nielahthplonehp nehw A = mass ni g fo eht ,eudiser and
detulid htiw 3-2 semulov fo .retaw retfA B = mass ni g fo eht elpmas .nekat
ANNEX E
I Clause 4.2, Table 1, Sl No. )iiv( j
NOITANIMRETED FO ENIROLHC
E-l REAGENTS taeH eht erutxim .yllaudarg Raise eht -met
erutarep llit eht mass is desuf and .detlem looC
eht tlem and tcartxe htiw dellitsid .retaw
E-l.1 Silver Nitrate Solution
etatipicerP eht edirolhc as revlis edirolhc htiw
2.l-E Ferric Nitrate an ssecxe fo standard revlis .etartin enimreteD
eht ssecxe revlis etartin yb noitartit htiw -oiht
3.l-E muissatoP edixordyH etanayc noitulos using cirref etartin as eht
.rotacidni A elttil eneznebortin yam eb desu ot
4.l-E muidoS edixoreP sserped eht ytilibulos fo revlis .edirolhc
E-1.5 Standard Thiocyanate Solution E-3 CALCULATION
E-2 PROCEDURE etaluclaC eht tnuoma fo enirolhc morf eht
:alumrof
taeH 2’0 3.O-ot g fo eht lairetam htiw a erutxim
fo 10 g fo deredwop muissatop edixordyh and 1 lm fo lamron revlis =3 530’0 46 g fo .enirolhc
5 g fo muidos edixorep ni a lekcin .elbicurc etartin noitulos

4
Standard Mark

ehT esu fo eht dradnatS Mark is denrevog yb eht snoisivorp fo eht
Bureau of Zndian
and eht seluR and snoitalugeR edam .rednuereht ehT dradnatS Mark no
Standards Act, 1986
stcudorp derevoc yb an naidnI dradnatS syevnoc eht ecnarussa that yeht evah neeb decudorp
ot ylpmoc htiw eht stnemeriuqer fo that standard rednu a llew denifed metsys fo ,noitcepsni
gnitset and ytilauq lortnoc hcihw desived and desivrepus yb SIB and detarepo yb eht -orp
is
.recud dradnatS dekram stcudorp era osla ylsuounitnoc dekcehc yb SIB rof ytimrofnoc ot
that standard as a rehtruf .draugefas sliateD fo snoitidnoc rednu hcihw a ecnecil rof eht esu
fo eht dradnatS Mark yam eb detnarg ot srerutcafunam ro srecudorp yam eb deniatbo morf
eht uaeruB fo naidnI Standards.